System and method for producing hollow fibre membranes

Patent metadata

Field	Value
Publication number	US-11813577-B2
Application number	US-202017437427-A
Country	US
Kind code	B2
Filing date	Mar 17, 2020
Priority date	Mar 20, 2019
Publication date	Nov 14, 2023
Grant date	Nov 14, 2023

Abstract

The invention relates to an apparatus and a method for the manufacture of at least one hollow fiber membrane, wherein a spinning mass is extruded via a spinning unit to form a spinning thread and precipitated in a precipitation bath to form a hollow fiber membrane and the hollow fiber membrane is optionally rinsed in a rinsing bath, wherein furthermore the hollow fiber membrane is passed through at least one drying unit, wherein the drying unit comprises a pressure section which is constructed in such a way that a positive pressure compared with atmospheric pressure can be set in the pressure section, and at least part of the precipitating agent or rinsing agent contained in the at least one hollow fiber membrane (104) is separated from the at least one hollow fiber membrane.

First claim

The invention claimed is:

1. An apparatus for the manufacture of at least one hollow fiber membrane, comprising
a spinning unit comprising at least one annular gap nozzle which is fluidically connected to a source of a spinning mass and a source of a coagulation medium in order to extrude at least one hollow spinning thread from the spinning mass, the cavity of which hollow spinning thread is filled with the coagulation medium,
a precipitation bath for precipitating the at least one spinning thread to form at least one hollow fiber membrane,
optionally, at least one rinsing unit for rinsing the at least one hollow fiber membrane,
at least one drying unit for drying the at least one hollow fiber membrane,
optionally, a receiving unit for receiving the at least one hollow fiber membrane on a support, wherein
the at least one drying unit comprises a pressure section which is constructed in such a way that a positive pressure compared with atmospheric pressure can be set in the pressure section,
the pressure section comprises a pressure chamber which comprises an interior space, an inlet for introducing the at least one hollow fiber membrane into the interior space of the pressure chamber, an outlet for discharging the at least one hollow fiber membrane from the interior space of the pressure chamber and at least one gas inlet, wherein the at least one gas inlet is in fluid communication with a gas source and the pressure section is further constructed in such a way that a positive pressure can be generated in the interior space of the pressure chamber via the gas source, the positive pressure removing liquid from the at least one hollow fiber membrane without the liquid being evaporated,
the drying unit further comprises a tempering section which has a heating device which is arranged so that a temperature of 50 to 230° C. is capable of being set in the tempering section,
the tempering section comprises a tempering chamber which has an inlet for introducing the at least one hollow fiber membrane and an outlet for discharging the at least one hollow fiber membrane, and
the pressure chamber and the tempering chamber are separate chambers, and the apparatus is further constructed in such a way that the at least one hollow fiber membrane or several hollow fiber membranes obtained from the precipitation bath or, optionally, from the rinsing bath is/are first passed through the pressure chamber and then through the tempering chamber.

2. The apparatus according to claim 1 , wherein the apparatus is constructed in such a way that the pressure in the pressure section of the drying apparatus is 1100 hPa to 10,000 hPa.

3. The apparatus according to claim 1 , wherein a cross-sectional area of the inlet for introducing the at least one hollow fiber membrane into the interior space of the pressure chamber, and of the outlet for discharging the at least one hollow fiber membrane from the pressure chamber is less than 30 times, and at least 1.1 times or more the cross-sectional area of the hollow fiber membrane or the total of the cross-sectional areas of the several hollow fiber membranes.

4. The apparatus according to claim 1 , wherein the pressure chamber of the pressure section is divided into several compartments.

5. The apparatus according to claim 1 , wherein the clear width of the interior space of the pressure chamber has, in the cross section parallel to the direction of travel of the at least one hollow fiber membrane, at least one enlargement of the cross section and at least one reduction of the cross section, wherein the enlargement of the cross section and the reduction of the cross section result in a conical shape of the inner side of the pressure chamber.

6. The apparatus according to claim 5 , wherein the at least one gas inlet of the pressure chamber is arranged at a position where the cross section of the clear width of the interior space of the pressure chamber has a maximum, centrally between the inlet for introducing the at least one hollow-fiber membrane into, and the outlet for discharging the at least one hollow-fiber membrane out of, the pressure chamber.

7. The apparatus according to claim 1 , wherein the pressure chamber has one or more outlets for discharging the liquid, wherein the outlets are arranged at a position where the cross section of the clear width of the interior space of the pressure chamber has a maximum.

Assignees

• Fresenius Medical Care Deutschland Gmbh

Inventors

• Paul Michael

Classifications

• B01D69/0871

  Fibre guidance after spinning through the manufacturing apparatus · CPC title

• B01D63/0233

  forming the bundle · CPC title

• B01D2323/081

  Heating · CPC title

• B01D67/0018 Primary

  Thermally induced processes [TIPS] · CPC title

• B01D69/088 Primary

  Co-extrusion; Co-spinning · CPC title