Methods for mixing products using acoustic mixing
US-10046287-B2 · Aug 14, 2018 · US
US11801959B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11801959-B2 |
| Application number | US-201615754763-A |
| Country | US |
| Kind code | B2 |
| Filing date | Aug 26, 2016 |
| Priority date | Aug 26, 2015 |
| Publication date | Oct 31, 2023 |
| Grant date | Oct 31, 2023 |
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A multilayer container for elevated temperature, high pressure processing of a material within the container, using a pressure transmission liquid within the container, the multilayer container having a container wall having an inner layer formed of a plastic for containing the liquid in contact with the inner side thereof and at least one further layer outboard of the inner layer and formed of different plastic from the inner layer, wherein the inner layer has a compression heating coefficient at least as high as the compression heating coefficient of the pressure transmission liquid in contact with the inner side thereof and the at least one further layer has a lower thermal conductivity at ambient pressure and temperature than the inner layer.
Opening claim text (preview).
The invention claimed is: 1. A multilayer container configured to be used in a pressure vessel operating at elevated temperature for high pressure elevated temperature processing of a material within the container, using an aqueous pressure transmission liquid within the container and a pressurization medium in the pressure vessel outside the multilayer container, the multilayer container having a container wall comprising as contiguous plastics layers, an inner layer formed of a plastic for containing the aqueous pressure transmission liquid in contact with an inner side of the inner layer, an intermediate layer and a layer outboard of the intermediate later layer, wherein (a) the inner layer is of polyethylene having a compression heating coefficient greater than a compression heating coefficient of the aqueous pressure transmission liquid in contact with the inner side of the inner layer to transfer heat from the inner layer to the aqueous pressure transmission liquid during high pressure processing; (b) the intermediate layer is of polypropylene or ABS and the intermediate layer having a lower thermal conductivity than the inner layer, a lower compression heating coefficient than the inner layer and a higher compression heating coefficient than the aqueous pressure transmission liquid; and (c) the outboard layer, which is free of PVC, has a compression heating coefficient that is lower than the compression heating coefficient of the inner layer and, the outboard layer having a thermal conductivity of no more than 0.25 W·m −1 ·K −1 to provide thermal insulation to reduce heat loss from the container; and wherein the container wall comprises a cylindrical side wall and an end wall, that is sealed to the cylindrical side wall, is provided with a piston having a peripheral edge which seals with the container cylindrical side wall whereby the aqueous pressure transmission liquid and the material are separated from the pressurization medium outside the container, the piston being movable within the container cylindrical side wall in response to a change in pressure applied to the piston by the pressurization medium outside of the container to apply pressure to the aqueous pressure transmission liquid within the container during high pressure processing. 2. The multilayer container according to claim 1 , wherein the inner layer has a compression heating coefficient at ambient temperature and ambient pressure of at least 6×10 −11 Pa −1 . 3. The multilayer container according to claim 1 , wherein the compressibility of the outboard layer is no more than 2.0×10 −10 Pa −1 . 4. The multilayer container according to claim 1 , wherein the inner layer is formed of high density polyethylene. 5. The multilayer container according to claim 4 , wherein the outboard layer is selected from the group consisting of polypropylene, PTFE, PMMA, and PVDF. 6. The multilayer container according to claim 1 , wherein the intermediate layer has a thermal conductivity, compressibility and compression heating coefficient that is higher than the outboard layer. 7. The multilayer container according to claim 1 , wherein the inner layer is formed of HDPE and the intermediate layer is formed of polypropylene. 8. The multilayer container according to claim 1 , wherein each of the inner, intermediate and outboard layers are of thickness in the range of from 1 mm to 50 mm. 9. The multilayer container according to claim 1 , wherein the material to be processed is a food material. 10. The multilayer container according to claim 1 , wherein there is no ohmic or electrical heating within the container or from outside of the container. 11. The multilayer container according to claim 1 , wherein the piston is of single or multilayer construction and comprises the same material as the inner layer of the container. 12. The multilayer container according to claim 1 , wherein the contiguous layers are different diameter cylindrical side wall layers which are separable and slidably engaged. 13. A system for high pressure thermal processing of a material, comprising the multilayer container according to claim 1 , wherein the aqueous pressure transmission liquid and the material are within the container. 14. The system according to claim 13 , wherein the container is housed within the pressure vessel for applying pressure to the aqueous pressure transmission liquid, and wherein the pressure vessel contains the liquid pressurization medium separated from the aqueous pressure transmission liquid within the container by the piston and the piston is responsive to pressure exerted by the pressurization medium to transfer pressure to the aqueous pressure transmission liquid. 15. A process for high pressure thermal processing of a material comprising: (i) providing the multilayer container according to claim 1 ; (ii) providing the aqueous pressure transmission liquid and the material; (iii) preheating the multilayer container, the aqueous pressure transmission liquid and the material; (iv) placing the material to be processed within the container and providing the aqueous pressure transmission liquid within the container in association with the material for applying pressure to the material; and (v) applying pressure to the aqueous pressure transmission liquid within the container; wherein the inner and intermediate layers together provide compression heating to the aqueous pressure transmission liquid and the outboard layer reduces heat loss from the container. 16. The process according to claim 15 , wherein the multilayer container, the aqueous pressure transmission liquid and the material are preheated to a temperature in the range of from 40° C. to 150° C. and the pressure applied is in the range of from 100 to 1000 MPa. 17. The process according to claim 16 , wherein the pressure is maintained in the range for a period of 1 second to 30 minutes. 18. The process according to claim 15 , wherein the material is a food material.
by heating materials in packages which are not progressively transported through the apparatus · CPC title
using sub- or super-atmospheric pressures, or pressure variations transmitted by a liquid or gas · CPC title
by heat · CPC title
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