Method of preparing a composite sheet

Patent metadata

Field	Value
Publication number	US-11787152-B2
Application number	US-201916712448-A
Country	US
Kind code	B2
Filing date	Dec 12, 2019
Priority date	Dec 13, 2018
Publication date	Oct 17, 2023
Grant date	Oct 17, 2023

Abstract

A composite sheet comprising two or more layers is described where the degree of abrasiveness of can be controlled. The sheet can comprise partially or wholly biodegradable or compostable materials or blends thereof. Methods of preparing the composite sheets are also described.

First claim

What is claimed is:

1. A method of preparing a biodegradable or compostable composite sheet, the method comprising:
providing a base layer, wherein the base layer comprises a polymeric web consisting of a first polymer, wherein the first polymer comprises or consists of cellulose, and
meltblowing a second polymer onto a first surface of the base layer to form a first abrasive layer comprising meltblown fibers of the second polymer, wherein the second polymer is polylactic acid (PLA), wherein the meltblown fibers have a diameter of about 0.3 microns (μm) to about 5 μm, and wherein abrasiveness of the first abrasive layer is controlled by the diameter of the meltblown fibers.

2. The method of claim 1 , wherein the method further comprises meltblowing a third polymer onto a second surface of the base layer to form a second abrasive layer comprising meltblown fibers of the third polymer, wherein the third polymer is the same or different than the second polymer, and wherein the meltblown fibers of the second abrasive layer have a diameter of about 0.3 μm to about 20 μm.

3. The method of claim 2 , wherein the meltblown fibers of the second abrasive layer have a different diameter than the meltblown fibers of the first abrasive layer.

4. The method of claim 1 , wherein the meltblowing is performed using nozzles having a diameter of about 180 μm to about 600 μm and/or a nozzle density of about 10 per inch to about 75 per inch.

5. The method of claim 1 , wherein the meltblowing is performed using a die to collector distance (DCD) of about 50 millimeters (mm) to 300 mm.

6. The method of claim 5 , wherein the meltblowing is performed at a temperature of about 200° C. to about 300° C.

7. The method of claim 1 , wherein the first abrasive layer comprises about 1 grams per square meter (g/m 2 ) to about 30 g/m 2 of the second polymer.

8. The method of claim 7 , wherein the first abrasive layer comprises about 5 g/m 2 to about 15 g/m 2 of the second polymer.

9. The method of claim 1 , wherein the base layer comprises about 10 g/m 2 to about 150 g/m 2 cellulose.

10. The method of claim 9 , wherein the base layer comprises about 25 g/m 2 to about 55 g/m 2 cellulose.

11. The method of claim 1 , wherein the first polymer is cellulose.

12. The method of claim 1 , wherein the cellulose comprises pulp, lyocell, cotton, or a blend thereof.

13. The method of claim 1 , wherein the meltblowing of the second polymer is performed using an air consumption of about 1600 m 3 /m/hr to about 1900 m 3 /m/hr.

Assignees

• Univ North Carolina State

Inventors

• Pourdeyhimi Behnam

Classifications

• B32B5/26 Primary

  another layer {next to it} also being fibrous or filamentary {(relative arrangement of fibres or filaments of different layers B32B5/12)} · CPC title

• B29C48/154

  Coating solid articles, i.e. non-hollow articles · CPC title

• B32B5/022

  Non-woven fabric · CPC title

• B32B37/24

  with at least one layer not being coherent before laminating, e.g. made up from granular material sprinkled onto a substrate (B32B37/15 takes precedence) · CPC title

• D01D4/025

  Melt-blowing or solution-blowing dies · CPC title