Cubic boron nitride sintered material, tool comprising cubic boron nitride sintered material and method for manufacturing cubic boron nitride sintered material

Patent metadata

Field	Value
Publication number	US-11773030-B2
Application number	US-202118015298-A
Country	US
Kind code	B2
Filing date	Oct 26, 2021
Priority date	Oct 28, 2020
Publication date	Oct 3, 2023
Grant date	Oct 3, 2023

Abstract

A cBN sintered material comprising cBN particles and a binder phase, in which the binder phase contains AlN and AlB 2 , a content proportion of cBN particles is 70 to 97 vol %, cBN sintered material has a volume resistivity up to 5×10 −3 Ωcm, a rate of a peak intensity derived from Al with respect to a peak intensity derived from cBN particles is less than 1.0%, cBN particles include fine particles and coarse particles, coarse particles optionally include ultra-coarse particles, with respect to the entire cBN particles, a content proportion α of fine particles is from 10 vol %, a content proportion β of coarse particles is from 30 vol %, a content proportion γ of ultra-coarse particles is 25 vol % or less, and a total of the content proportion α of fine particles and the content proportion β of coarse particles is 50 to 100 vol %.

First claim

The invention claimed is:

1. A cubic boron nitride sintered material comprising:
cubic boron nitride particles; and
a binder phase,
wherein the binder phase contains aluminum nitride and aluminum diboride,
a content proportion of the cubic boron nitride particles is 70 vol % or more and 97 vol % or less with respect to the entire cubic boron nitride sintered material,
wherein the cubic boron nitride sintered material has a volume resistivity of 5×10 −3 Ωcm or less,
in a case where X-ray diffraction measurement is performed on an arbitrary surface or arbitrary cross section of the cubic boron nitride sintered material, a rate of a peak intensity derived from metallic aluminum with respect to a peak intensity derived from the cubic boron nitride particles is less than 1.0%,
wherein the cubic boron nitride particles include fine particles having a particle diameter of 2 μm or less and coarse particles having a particle diameter of 5 μm or more,
wherein the coarse particles optionally include ultra-coarse particles having a particle diameter of more than 12 μm, and
wherein with respect to the entire cubic boron nitride particles,
a content proportion α of the fine particles is 10 vol % or more,
a content proportion β of the coarse particles is 30 vol % or more,
a content proportion γ of the ultra-coarse particles is 25 vol % or less, and
a total of the content proportion α of the fine particles and the content proportion β of the coarse particles is 50 vol % or more and 100 vol % or less.

2. The cubic boron nitride sintered material according to claim 1 , wherein
with respect to the entire cubic boron nitride particles,
the content proportion α of the fine particles is 10 vol % or more and 20 vol % or less,
the content proportion β of the coarse particles is 30 vol % or more and 90 vol % or less, and
the content proportion γ of the ultra-coarse particles is more than 0 vol % and 25 vol % or less.

3. The cubic boron nitride sintered material according to claim 1 , wherein, in a case where X-ray diffraction measurement is performed on the arbitrary surface or arbitrary cross section of the cubic boron nitride sintered material, the rate of the peak intensity derived from aluminum diboride with respect to the peak intensity derived from the cubic boron nitride particles is 3.9% or more.

4. The cubic boron nitride sintered material according to claim 1 , wherein an area rate of voids that are observed in the arbitrary surface or arbitrary cross section of the cubic boron nitride sintered material is 0.05% or less.

5. A tool comprising:
the cubic boron nitride sintered material according to claim 1 .

6. The tool according to claim 5 , further comprising:
a coating that is provided on the cubic boron nitride sintered material,
wherein a peeling load is 20 N or more, in a case where a scratch test is performed on the coating with a diamond indenter having R of 200 μm and a cone angle of 120°.

7. The tool according to claim 6 , wherein the coating includes a coated layer composed of a compound represented by Ti x M 1-x C y N 1-y ,
wherein M represents one or more elements selected from the group consisting of Group IV elements except titanium, Group V elements and Group VI elements in the periodic table, aluminum, silicon and boron,
x is 0.2 or more and 1 or less, and
y is 0 or more and 0.6 or less, in Ti x M 1-x C y N 1-y .

8. The tool according to claim 6 , wherein the coating has a thickness of 0.5 μm or more and less than 6.0 μm.

Assignees

• Sumitomo Electric Hardmetal Corp

Inventors

• Miyamoto Keita
• Kukino Satoru
• Ueda Akihiko
• Matsukawa Michiko

Classifications

• C04B35/5831 Primary

  based on cubic boron nitrides {or Wurtzitic boron nitrides, including crystal structure transformation of powder} · CPC title

• C04B35/62836

  Nitrides · CPC title

• C04B35/62892

  with a coating layer consisting of particles · CPC title

• C04B41/0072

  Heat treatment · CPC title

• C04B2235/3804

  Borides · CPC title