Method of manufacturing ceramic tape

Patent metadata

Field	Value
Publication number	US-11768032-B2
Application number	US-202318115852-A
Country	US
Kind code	B2
Filing date	Mar 1, 2023
Priority date	Jun 29, 2015
Publication date	Sep 26, 2023
Grant date	Sep 26, 2023

Abstract

A method of manufacturing ceramic tape includes a step of directing a tape of partially-sintered ceramic into a furnace. The tape is partially-sintered such that grains of the ceramic are fused to one another yet the tape still includes at least 10% porosity by volume, where the porosity refers to volume of the tape unoccupied by the ceramic. The method further includes steps of conveying the tape through the furnace and further sintering the tape as the tape is conveyed through the furnace. The porosity of the tape decreases during the further sintering step.

First claim

What is claimed is:

1. A method of manufacturing ceramic tape, comprising:
conveying a tape comprising polycrystalline ceramic through a furnace, wherein length of the tape is at least 10 m, width is at least 10 mm, and thickness is at least 10 μm;
sintering the tape as the tape is conveyed through the furnace,
wherein prior to the sintering, the tape is already partially-sintered such that grains of the ceramic are fused to one another yet the tape still includes at least 10% porosity by volume, where the porosity refers to volume of the tape unoccupied by the ceramic; and
applying tension to the tape during the sintering.

2. The method of claim 1 , further comprising holding the tape flat with the tension during the sintering.

3. The method of claim 1 , wherein the tension comprises 20 megapascals.

4. The method of claim 1 , wherein the width is no greater than 20 cm and the thickness is no greater than 500 μm.

5. The method of claim 1 , wherein, during the sintering, temperatures experienced by portions of the tape in the furnace are at least 800° C., while other portions of the tape outside the furnace are experiencing lower temperatures.

6. The method of claim 5 , wherein the other portions of the tape outside of the furnace are experiencing room temperature.

7. The method of claim 1 , wherein the ceramic comprises alumina, zirconia, lithium garnet, and/or spinel.

8. The method of claim 1 , wherein the tape is conveyed through the furnace at a rate of at least 1 inch per minute.

9. A method of manufacturing ceramic tape, comprising:
conveying a tape comprising polycrystalline ceramic through a furnace, wherein length of the tape is at least 10 m, width is at least 10 mm, and thickness is at least 10 μm;
sintering the tape as the tape is conveyed through the furnace,
applying tension to the tape during the sintering; and
following the sintering, further comprising winding the tape on a spool.

10. The method of claim 9 , wherein the spool has a diameter of at least 0.5 cm.

11. The method of claim 9 , further comprising holding the tape flat with the tension during the sintering.

12. A method of manufacturing ceramic tape, comprising:
conveying a tape comprising polycrystalline ceramic through a furnace, wherein length of the tape is at least 10 m, width is at least 10 mm, and thickness is at least 10 μm;
sintering the tape as the tape is conveyed through the furnace, and
applying tension to the tape during the sintering,
wherein porosity of the tape after the sintering is less than 1%, where the porosity refers to volume of the tape unoccupied by the ceramic.

13. The method of claim 12 , wherein, prior to the sintering, the tape is already partially-sintered such that grains of the ceramic are fused to one another yet the tape still includes at least 10% porosity by volume.

14. The method of claim 12 , further comprising directing the tape into the furnace prior to the conveying, wherein as the tape is directed into the furnace, the tape still includes at least 30% porosity by volume.

15. A method of manufacturing ceramic tape, comprising:
directing a tape comprising polycrystalline ceramic into a furnace and conveying the tape through a furnace, wherein length of the tape is at least 10 m, width is at least 10 mm, and thickness is at least 10 μm; and
sintering the tape as the tape is conveyed through the furnace,
applying tension to the tape during the sintering,
wherein, as the tape is directed into the furnace, the tape still includes at least 30% porosity by volume, where the porosity refers to volume of the tape unoccupied by the ceramic.

16. The method of claim 15 , wherein, prior to the sintering, the tape is already partially-sintered such that grains of the ceramic are fused to one another yet the tape still includes at least 10% porosity by volume.

17. A method of manufacturing ceramic tape, comprising:
conveying a tape comprising polycrystalline ceramic through a furnace, wherein the ceramic comprises alumina, zirconia, lithium garnet, and/or spinel, wherein length of the tape is at least 10 m, width is at least 10 mm, and thickness is at least 10 μm, wherein the width is no greater than 20 cm and the thickness is no greater than 500 μm; and
sintering the tape as the tape is conveyed through the furnace, wherein porosity of the tape after the sintering is less than 1%;
applying tension to the tape during the sintering.

18. The method of claim 17 , wherein the tension comprises 20 megapascals.

19. The method of claim 17 , wherein, during the sintering, temperatures experienced by portions of the tape in the furnace are at least 800° C., while other portions of the tape outside the furnace are experiencing lower temperatures.

20. The method of claim 17 , wherein, prior to the sintering, the tape is already partially-sintered such that grains of the ceramic are fused to one another yet the tape still includes at least 10% porosity by volume, where the porosity refers to volume of the tape unoccupied by the ceramic.

Assignees

• Corning Inc

Inventors

• Badding Michael Edward
• Bouton William Joseph
• Brown Jacqueline Leslie
• Curry Timothy Joseph
• Hurny Roman E
• Kester Lanrik Wayne
• Ketcham Thomas Dale
• Olenick John Albert
• Olenick Kathleen Ritter
• Paananen Jeremy
• Silverblatt Thomas
• St Julien Dell Joseph
• Venkateswaran Viswanathan
• Zink Nathan Michael

Classifications

• C04B2235/9653

  Translucent or transparent ceramics other than alumina · CPC title

• C04B2235/963

  Surface properties, e.g. surface roughness · CPC title

• C04B2235/9615

  Linear firing shrinkage · CPC title

• C04B2235/6025

  Tape casting, e.g. with a doctor blade · CPC title

• C04B35/64 Primary

  Burning or sintering processes (C04B33/32 takes precedence {; powder metallurgy B22F}) · CPC title