Method for producing resin particle dispersion, method for producing toner for electrostatic image development, and toner for electrostatic image development

Patent metadata

Field	Value
Publication number	US-11760845-B2
Application number	US-202117465210-A
Country	US
Kind code	B2
Filing date	Sep 2, 2021
Priority date	Mar 25, 2021
Publication date	Sep 19, 2023
Grant date	Sep 19, 2023

Abstract

Producing a resin particle dispersion using an apparatus including: two or more resin particle dispersion production lines each including an emulsification tank in which a resin is subjected to phase inversion emulsification using two or more organic solvents and an aqueous medium to obtain a phase-inverted emulsion, a distillation tank in which the organic solvents are removed from the phase-inverted emulsion by reduced pressure distillation to obtain a resin particle dispersion, and plural distillate collection tanks that collect distillates formed during the reduced pressure distillation according to respective target distillate compositions; and a reusable storage tank that collects and stores a distillate collected in at least one collection tank among the distillates collected in the plural collection tanks in each of the two or more production lines, and delivering the distillate to the emulsification tank in at least one production line to reuse the distillate for producing a phase-inverted emulsion.

First claim

What is claimed is:

1. A method for producing a resin particle dispersion, the method comprising:
using a resin particle dispersion production apparatus including:
two or more resin particle dispersion production lines each including an emulsification tank in which a resin is subjected to phase inversion emulsification using two or more organic solvents and an aqueous medium to thereby obtain a phase-inverted emulsion, a distillation tank in which the organic solvents are removed from the phase-inverted emulsion by reduced pressure distillation to thereby obtain a resin particle dispersion, and a plurality of distillate collection tanks that collect distillates formed during the reduced pressure distillation according to respective target distillate compositions; and
a reusable distillate storage tank A that collects and stores a distillate collected in at least one distillate collection tank A among the distillates collected in the plurality of distillate collection tanks in each of the two or more resin particle dispersion production lines,
wherein the distillate collected in the reusable distillate storage tank A is delivered to the emulsification tank in at least one resin particle dispersion production line among the two or more resin particle dispersion production lines to reuse the distillate for production of a phase-inverted emulsion in the at least one resin particle dispersion production line.

2. The method for producing a resin particle dispersion according to claim 1 , wherein the reuse amount of the distillate to be reused is determined using the mixing ratio of the two or more organic solvents in the distillate stored in the reusable distillate storage tank A and the mixing ratio of the two or more organic solvents at the time of the production of the phase-inverted emulsion in the at least one resin particle dispersion production line, and
wherein the determined reuse amount of the distillate in the reusable distillate storage tank A is delivered from the reusable distillate storage tank A to the emulsification tank in the at least one resin particle dispersion production line to reuse the distillate for the production of the phase-inverted emulsion in the at least one resin particle dispersion production line.

3. The method for producing a resin particle dispersion according to claim 1 , wherein the distillate composition of each of the distillates formed during the reduced pressure distillation is analyzed using at least one type of measurement selected from the group consisting of weight measurement, gas chromatography measurement, liquid chromatography measurement, infrared spectroscopy measurement, ultrasonic propagation velocity measurement, neutralization titration, specific gravity measurement, and electric conductivity measurement, and
wherein each distillate is collected in one of the distillate collection tanks that is determined according to a target distillate composition.

4. The method for producing a resin particle dispersion according to claim 2 , wherein the distillate composition of each of the distillates formed during the reduced pressure distillation is analyzed using at least one type of measurement selected from the group consisting of weight measurement, gas chromatography measurement, liquid chromatography measurement, infrared spectroscopy measurement, ultrasonic propagation velocity measurement, neutralization titration, specific gravity measurement, and electric conductivity measurement, and
wherein each distillate is collected in one of the distillate collection tanks that is determined according to a target distillate composition.

5. The method for producing a resin particle dispersion according to claim 1 , wherein the mixing ratio of the two or more organic solvents in the distillate stored in the reusable distillate storage tank A is computed using the mixing ratio of the two or more organic solvents at the time of production of the phase-inverted emulsion in each of the two or more resin particle dispersion production lines, the amounts of the organic solvents at the time of production of the phase-inverted emulsion in each of the two or more resin particle dispersion production lines, the amount of the distillate collected in the distillate collection tank A in each of the two or more resin particle dispersion production lines, and the amount of the distillate stored in the reusable distillate storage tank A.

6. The method for producing a resin particle dispersion according to claim 2 , wherein the mixing ratio of the two or more organic solvents in the distillate stored in the reusable distillate storage tank A is computed using the mixing ratio of the two or more organic solvents at the time of production of the phase-inverted emulsion in each of the two or more resin particle dispersion production lines, the amounts of the organic solvents at the time of production of the phase-inverted emulsion in each of the two or more resin particle dispersion production lines, the amount of the distillate collected in the distillate collection tank A in each of the two or more resin particle dispersion production lines, and the amount of the distillate stored in the reusable distillate storage tank A.

7. The method for producing a resin particle dispersion according to claim 3 , wherein the mixing ratio of the two or more organic solvents in the distillate stored in the reusable distillate storage tank A is computed using the mixing ratio of the two or more organic solvents at the time of production of the phase-inverted emulsion in each of the two or more resin particle dispersion production lines, the amounts of the organic solvents at the time of production of the phase-inverted emulsion in each of the two or more resin particle dispersion production lines, the amount of the distillate collected in the distillate collection tank A in each of the two or more resin particle dispersion production lines, and the amount of the distillate stored in the reusable distillate storage tank A.

8. The method for producing a resin particle dispersion according to claim 4 , wherein the mixing ratio of the two or more organic solvents in the distillate stored in the reusable distillate storage tank A is computed using the mixing ratio of the two or more organic solvents at the time of production of the phase-inverted emulsion in each of the two or more resin particle dispersion production lines, the amounts of the organic solvents at the time of production of the phase-inverted emulsion in each of the two or more resin particle dispersion production lines, the amount of the distillate collected in the distillate collection tank A in each of the two or more resin particle dispersion production lines, and the amount of the distillate stored in the reusable distillate storage tank A.

9. The method for producing a resin particle dispersion according to claim 1 , wherein the mixing ratio of the two or more organic solvents in the distillate stored in the reusable distillate storage tank A is measured using at least one type of measurement selected from the group consisting of gas chromatography measurement, liquid chromatography measurement, infrared spectroscopy measurement, ultrasonic propagation velocity measurement, neutralization titration, specific gravity measurement, and electric conductivity measurement.

10. The method for producing a resin particle dispersion according to claim 2 , wherein the mixing ratio of the two or more organic solvents in the distillate stored in the reusable distillate storage tank A is measured using at least one type of measurement selected from the group consisting of gas chromatography measurement, liquid chromatography measurement, infrared spectroscopy measurement, ult

Assignees

• Fujifilm Business Innovation Corp

Inventors

• Higashi Kenji
• Yamamoto Keita
• Inukai Takashi
• Nakamura Kazuhiko
• Isshiki Yuji

Classifications

• G03G9/0804 Primary

  whereby the components are brought together in a liquid dispersing medium · CPC title

• C08J3/095 Primary

  Oxygen containing compounds · CPC title

• G03G9/09392

  Preparation thereof · CPC title

• C08J2367/02

  Polyesters derived from dicarboxylic acids and dihydroxy compounds; (C08J2367/06 takes precedence) · CPC title

• C08J3/07

  from polymer solutions · CPC title