High-strength concrete and preparation method thereof

Patent metadata

Field	Value
Publication number	US-11753339-B2
Application number	US-202318152145-A
Country	US
Kind code	B2
Filing date	Jan 9, 2023
Priority date	Aug 4, 2020
Publication date	Sep 12, 2023
Grant date	Sep 12, 2023

Abstract

The present disclosure relates to a high-strength concrete and a preparation method thereof. The high-strength concrete includes lignin, recycled fine powder, cement, water, sand, gravels and a water reducing agent. The recycled fine powder is recycled fine powder of discarded concrete, and is prepared by separating solid waste of discarded buildings, then performing impurity removal and crushing processing, and grinding same by a ball mill into dust with a particle size of less than 0.16 mm. The lignin is discarded wood lignin, which is prepared by crushing the wood, stirring and extracting a sodium hydroxide aqueous solution with a mass concentration of 5% for 1 to 2 hours at the temperature of 80 DEG C. to obtain a black lignin alkali solution, adding a hydrochloric acid solution with a mass concentration of 30% into the alkali solution for stirring, and making the pH reduced to 7.0 for standing and layering.

First claim

What is claimed is:

1. A concrete comprising lignin, recycled fine powder, P.042.5 grade cement, water, sand, gravels with a particle size of 6 mm to 10 mm, and a polycarboxylic acid water reducing agent; wherein
a weight ratio of the cement, water, sand, gravels and the polycarboxylic acid water reducing agent in the concrete is 1:0.3:1.2:2.8:0.01;
a weight ratio of the lignin to the cement in the concrete is 0.1-0.3:20;
a weight ratio of the lignin to the recycled fine powder in the concrete is 0.1:5-10;
the recycled fine powder is recycled powder of discarded concrete, and is prepared by: separating solid waste of discarded buildings, removing impurity and crushing, and grinding into dust with a particle size of less than 0.16 mm by a ball mill;
the lignin is discarded wood lignin, which is extracted by: crushing wood, stirring and extracting with a sodium hydroxide aqueous solution with a mass concentration of 5% for 1 to 2 hours at 80° C. to obtain a black lignin alkali solution, adding a hydrochloric acid solution with a mass concentration of 30% into the black lignin alkali solution while stirring, reducing pH to 7.0, and obtaining the lignin by standing and layer separation;
and the concrete is made by a method comprising the following steps:
(1) pouring the lignin and the recycled fine powder into a portion of water to obtain a first uniformly mixed mixture,
(2) pouring the cement into the remaining water with a cement mixer to obtain a second uniformly mixed mixture,
(3) pouring the first uniformly mixed mixture into the second uniformly mixed mixture to obtain a third mixture, and then adding the polycarboxylic water reducing agent to the third mixture to obtain a uniformed mixed mixture A, and
(4) pouring the gravels and sand into the uniformly mixed mixture A for thoroughly stirring to obtain the concrete.

2. The concrete of claim 1 , wherein a ratio of water in the step (1) and step (2) is 1:2.

Assignees

• Univ Shandong
• China Power Construction Municipal Construction Group Co Ltd
• Univ Northeast Electric Power
• Shandong Boshuo Geotechnical Eng Design Consulting Co Ltd

Inventors

• Wu Ke
• Yang Tao
• Wang Cao
• Li Guodong
• Chen Rong
• Zhao Jiahui
• Hao Dongxue
• Ma Mingyue
• Yang Hongna

Classifications

• C04B28/04 Primary

  Portland cements · CPC title

• C04B28/02 Primary

  containing hydraulic cements other than calcium sulfates · CPC title

• C04B18/16 Primary

  from building or ceramic industry · CPC title

• C04B24/24

  Macromolecular compounds (C04B24/14 takes precedence; macromolecular compounds comprising sulfonate or sulfate groups C04B24/16) · CPC title

• C08H6/00

  Macromolecular compounds derived from lignin, e.g. tannins, humic acids · CPC title