Freeze-dried coffee powder and a method for the manufacture thereof

Patent metadata

Field	Value
Publication number	US-11744261-B2
Application number	US-202117478677-A
Country	US
Kind code	B2
Filing date	Sep 17, 2021
Priority date	Apr 27, 2016
Publication date	Sep 5, 2023
Grant date	Sep 5, 2023

Abstract

The present invention provides a method for the manufacture of a freeze-dried coffee powder, the method comprising:providing a coffee extract having from 40 wt % to 55 wt % solids;adding gas to the coffee extract in an amount of from 1 NL/kg to 5 NL/kg of coffee extract, to provide a gas-containing coffee extract at above atmospheric pressure;depressurising the gas-containing coffee extract to form a foamed coffee extract;cooling the foamed coffee extract to below −40° C. without shear, or with low shear, to form a frozen coffee extract,grinding the frozen coffee extract to a powder; anddrying the powder,wherein the step of cooling the foamed coffee extract to below −40° C. comprises:(i) cooling the foamed coffee extract to a first temperature;(ii) cooling the foamed coffee extract from the first temperature to a second temperature lower than the first temperature; and(iii) cooling the foamed coffee extract from the second temperature to below −40° C.,wherein the first temperature is 1° C. above a freezing point of the foamed coffee extract and wherein the second temperature is 3° C. below the freezing point,wherein step (ii) has a duration of from 5 to 90 minutes, preferably 10 to 60 minutes.

First claim

The invention claimed is:

1. A freeze-dried coffee powder for providing a coffee beverage with a crema of at least 0.25 ml/g on reconstitution in water, the coffee powder comprising particles having open gas bubbles and ice-crystal voids and having a closed porosity of less than 15%, wherein the open gas bubbles and ice-crystal voids have low interconnectivity such that less than 92% intrusion is achieved under a pressure of 90 psia Hg when measured by Hg porosimetry where intrusion into the particles is considered to start at 2 psia.

2. The freeze-dried coffee powder of claim 1 , wherein an intrusion span of the particles is at least 2, wherein the intrusion span is defined as:
(the pressure required for 90% intrusion)−(the pressure required for 10% intrusion)/(the pressure required for 50% intrusion)

when measured by Hg porosimetry where the intrusion into the particles is considered to start at 2 psia.

3. The freeze-dried coffee powder of claim 1 , wherein the freeze-dried coffee powder consists of soluble coffee solids.

4. The freeze-dried coffee powder of claim 1 , wherein the particles have a particle size distribution with a D10 of at least 300 microns.

5. The freeze-dried coffee powder of claim 1 , wherein the ice-crystal voids have a mean pore diameter of from 6 to 10 microns and/or wherein the open gas bubbles have a mean pore diameter from 10-60 microns.

6. The freeze-dried coffee powder of claim 1 , wherein the open gas bubbles and ice-crystal voids have low interconnectivity such that less than 80% intrusion is achieved under a pressure of 40 psia Hg.

7. A freeze-dried coffee powder for providing a coffee beverage with a crema of at least 0.25 ml/g on reconstitution in water, the coffee powder comprising particles having open gas bubbles and ice-crystal voids and having a closed porosity of less than 15%, wherein the open gas bubbles and ice-crystal voids have low interconnectivity such that less than 80% intrusion is achieved under a pressure of 40 psia Hg.

8. The freeze-dried coffee powder of claim 1 , wherein the freeze-dried coffee powder consists of soluble coffee solids and less than 20 wt % of roast and ground coffee particles and/or cocoa powder.

Assignees

• Douwe Egberts Bv

Inventors

• Welsh Joe Christopher
• Jackson Tamsin Mikeala
• Mulvany Jonathan Patrick
• Rees Jack
• Kang Woncheal

Classifications

• A23F5/32 Primary

  by lyophilisation · CPC title

• A23F5/08

  Methods of grinding coffee (coffee mills A47J42/00) · CPC title

• A23F5/36

  Further treatment of dried coffee extract; Preparations produced thereby, e.g. instant coffee ({A23F5/246 takes precedence; } removing unwanted substances A23F5/18; flavouring A23F5/46) · CPC title

• A23F5/26 Primary

  Extraction of water soluble constituents {(A23F5/246 takes precedence)} · CPC title

• A23F5/28 Primary

  Drying or concentrating coffee extract {(A23F5/246 takes precedence)} · CPC title