High-strength welding process for making heavy glass preforms with large cross sectional areas

Patent metadata

Field	Value
Publication number	US-11739019-B2
Application number	US-202016746180-A
Country	US
Kind code	B2
Filing date	Jan 17, 2020
Priority date	Jan 22, 2019
Publication date	Aug 29, 2023
Grant date	Aug 29, 2023

Abstract

An apparatus and related process for producing a high-strength weld between two glass components. Chucks clamp and move respective first ends of the glass components toward each other inside an enclosure, where the second ends are heated, softened, and welded together in a weld zone. The enclosure has layers of stacked quartz glass bricks and allows the weld zone to cool slowly and avoid stress. A propane quartz melting torch directs a flame inside the enclosure and toward the second ends as the glass components move toward each other. The flame softens the second ends and creates substantially smooth polished surfaces in the weld zone having an increased hydroxide content. At least 80% of the weld zone has a hydroxide content greater than about 10 ppm average in a 10 μm depth from the surface and the tensile strength of the weld zone is above about 10 MPa.

First claim

What is claimed:

1. A process for creating a high-strength weld seam in the center of a weld zone between two glass components of a welded assembly, the process comprising:
(a) providing two glass cylinder components each having a first end, an opposing second end, a central bore, and a ground surface, wherein each of the two glass cylinder components has an outside diameter and an inside diameter and wherein a ratio of the outside diameter to the inside diameter of each of the two glass cylinder components is greater than 3.0;
(b) clamping the first end of each glass cylinder component in the respective chucks of a lathe;
(c) moving the glass cylinder components towards each other using the lathe into an enclosure in which the second end of the first glass cylinder component and the second end of the second glass cylinder component are heated, softened, and welded together to form the weld seam in the weld zone, the enclosure having layers of stacked quartz glass bricks and allowing the weld zone to cool slowly and avoid stress in the weld zone;
(d) jointly and simultaneously heating and softening the second end of the first cylinder glass component and the second end of the second glass cylinder component in the enclosure using at least one propane quartz melting torch directing a flame inside the enclosure and toward the second ends of the glass cylinder components as the glass cylinder components move toward each other, the flame creating substantially smooth polished surfaces in the weld zone proximate the second end of each glass cylinder component having an increased hydroxide content;
(e) pressing the softened second ends of the glass cylinder components against each other to form the weld seam in the weld zone of the welded assembly; and
(f) cooling the welded assembly to ambient temperature,
wherein at least a portion of the cooling is done at a rate of about 60° C. per minute, and
wherein at least 80% of the weld zone has a hydroxide content greater than about 10 ppm average in a 10 μm depth from the surface and the tensile strength of the weld zone is greater than about 10 MPa.

2. The process of claim 1 , further comprising the step, after the step (e) of pressing the softened second ends of the glass cylinder components against each other to form the weld seam in the weld zone, the step of pressing a paddle against the outer surface of the weld zone to shape the weld zone.

3. The process of claim 1 , wherein during the step (d) of jointly and simultaneously heating and softening the second end of the first glass cylinder component and the second end of the second glass cylinder component, introducing a purging gas into the central bore to prevent the flame from entering the central bore, thereby assuring that the hydroxide content on the inside surface of the cylinder is less than on the outside surface of the cylinder.

4. The process of claim 1 , further comprising the step, after the step (f) of cooling, of removing the 10 μm depth from the surface of the weld zone.

5. The process of claim 1 , wherein the roughness of the ground surfaces of the cylinders is R z <6 μm and the roughness of the smooth polished surfaces is R z <0.3 μm.

6. The process of claim 1 , wherein at least 80% of the weld zone has a hydroxide content between about 20 and about 100 ppm average in a 10 μm depth from the surface.

7. The process of claim 1 , wherein the step (a) of providing two glass cylinder components includes providing a chamfered second end on at least one of the two glass cylinder components.

8. The process of claim 1 , wherein the enclosure further comprises a base layer made of graphite upon which the layers of stacked quartz glass bricks are disposed.

Assignees

• Heraeus Quartz North America Llc
• Heraeus Quarzglas

Inventors

• Ganz Oliver
• Koch Kenneth Robert
• Pontsler Tim Alan

Classifications

• C03B23/207 Primary

  Uniting glass rods, glass tubes, or hollow glassware (C03B23/24 takes precedence) · CPC title

• C03B23/043 Primary

  Heating devices specially adapted for re-forming tubes or rods in general, e.g. burners · CPC title

• C03B37/02736 Primary

  Means for supporting, rotating or feeding the tubes, rods, fibres or filaments to be drawn, e.g. fibre draw towers, preform alignment, butt-joining preforms or dummy parts during feeding (uniting rods or tubes C03B23/207) · CPC title

• C03B37/012

  Manufacture of preforms for drawing fibres or filaments · CPC title

• C03B37/01211

  by inserting one or more rods or tubes into a tube · CPC title