Distillation trays

Patent metadata

Field	Value
Publication number	US-11738284-B2
Application number	US-202117646189-A
Country	US
Kind code	B2
Filing date	Dec 28, 2021
Priority date	Apr 16, 2021
Publication date	Aug 29, 2023
Grant date	Aug 29, 2023

Abstract

Distillation trays having improved efficiency and capacity are described. The improvement is accomplished with unique downcomer spout arrangements and bubble promoters which provide equal liquid distribution to all areas of the tray. The ratio of the open area of a contacting zone including part of a bubble promoter and associated deck zone over the open area of the downcomer spout zone on the adjacent tray for distributing liquid to the zone is essentially the same across the tray.

First claim

What is claimed is:

1. A tray comprising:
a perforated deck;
a plurality of parallel trough-shaped downcomers extending through the deck, each downcomer having at least one first spout zone on a first side of a bottom and at least one second spout zone on a second side of the bottom;
a plurality of perforated bubble promoters on the deck, each bubble promoter having a first side and a second side, the bubble promoters positioned to align with at least one first spout zone and at least one second spout zone on a plurality of parallel trough-shaped downcomers on an adjacent tray rotated 90 degrees from the tray;
an open area of the at least one first spout zone on the adjacent tray being proportional to an open area of a first contacting zone of the tray, the first contacting zone defined by the first side of the bubble promoter and an associated deck zone;
an open area of the at least one second spout zone on the adjacent tray being proportional to an open area of a second contacting zone of the tray, the second contacting zone defined by the second side of the bubble promoter and an associated deck zone; and
wherein a ratio of the open area of the first spout zone to the open area of the second spout zone of the adjacent tray is 0.95 to 1.05 times a ratio of the open area of the first contacting zone to the open area of the second contacting zone of the tray.

2. The tray of claim 1 wherein the bubble promoters have an inverted V-shape with vertical ends.

3. The tray of claim 1 wherein a length of the spout zones on the first tray is less than a length of the bubble promoters on the tray below, or a width of the spout zones on the first tray is less than a width of the bubble promoters on the tray below, or both.

4. The tray of claim 1 wherein a size of the perforations of the deck is different from a size of the perforations of the bubble promoters.

5. The tray of claim 1 wherein a pitch of the perforations of the deck is different from a pitch of the perforations of the bubble promoters.

6. The tray of claim 1 wherein a size of the perforations of the first spout zone is different from a size of the perforations of the second spout zone.

7. The tray of claim 1 wherein a shape of the perforations of the first spout zone is different from a shape of the perforations of the second spout zone.

8. The tray of claim 1 wherein an open area of the deck is in a range of 5 to 30% of a total area of the deck, or wherein an open area of one of the bubble promoters is in a range of 5 to 30% of a total area of the one bubble promoter, or both.

9. A pair of trays comprising:
the first tray comprising:
a perforated deck;
a plurality of parallel trough-shaped downcomers extending through the deck, each downcomer having a first spout zone on a first side of a bottom and a second spout zone on a second side of the bottom, and wherein there is a downcomer at an edge of the first tray;
a plurality of perforated bubble promoters on the deck, each bubble promoter having a first side and a second side, the bubble promoters positioned to align with at least one first spout zone and at least one second spout zone on a plurality of parallel trough-shaped downcomers on an adjacent tray;

the second tray comprising:
a perforated deck;
a plurality of parallel trough-shaped downcomers extending through the deck, each downcomer having a first spout zone and a second spout zone at a bottom;
at least one perforated bubble promoter on the deck, the at least one bubble promoter having a first side and a second side, the bubble promoter positioned to align with the first spout zone and the second spout zone on a plurality of parallel trough-shaped downcomers on an adjacent tray;
a half bubble promoter on an edge of the second tray;

wherein a ratio of an open area of a first spout zone to an open area of a second spout zone on a tray adjacent to the first tray is 0.95 to 1.05 times a ratio of the open area of the first contacting zone to the second contacting zone of the first tray or an average of the open area of a first contacting zone of the first tray and a first contacting zone of the second tray to an average of a second contacting zone of the first tray and a second contacting zone of the second tray; and
wherein the first contacting zone of the first tray is defined by one side of the bubble promoter and an associated deck zone, the first contacting zone of the second tray is defined by one side of the bubble promoter or the half bubble promoter and an associated deck zone, the second contacting zone of the first tray is defined by one side of the bubble promoter and an associated deck zone, and the second contacting zone of the second tray is defined by one side of the bubble promoter or the half bubble promoter and an associated deck zone.

10. The pair of trays of claim 9 wherein there are downcomers on the edge of both sides of the first tray.

11. The pair of trays of claim 9 wherein there are half bubble promoters on the edge of both sides of the second tray.

12. The pair of trays of claim 9 wherein the bubble promoters have an inverted V-shape with vertical ends.

13. The pair of trays of claim 9 wherein a length of the spout zones on the first tray is less than a length of the bubble promoters on the tray below, or a width of the spout zones on the first tray is less than a width of the bubble promoters on the tray below, or both.

14. The pair of trays of claim 9 wherein a size of the perforations of the deck is different from a size of the perforations of the bubble promoters.

15. The pair of trays of claim 9 wherein a pitch of the perforations of the deck is different from a pitch of the perforations of the bubble promoters.

16. The pair of trays of claim 9 wherein a size of the perforations of the first spout zone deck is different from a size of the perforations of the second spout zone.

17. The pair of trays of claim 9 wherein a shape of the perforations of the first spout zone is different from a shape of the perforations of the second spout zone.

18. The pair of trays of claim 9 wherein an open area of the deck is in a range of 5 to 30% of a total area of the deck, or wherein an open area of one of the bubble promoters is in a range of 5 to 30% of a total area of the one bubble promoter, or both.

19. A mass transfer column comprising:
at least two trays vertically spaced apart, each tray comprising:
a plurality of parallel trough-shaped downcomers extending through the deck, each downcomer having at least one first spout zone on a first side of a bottom and at least one second spout zone on a second side of the bottom;
a plurality of perforated bubble promoters on the deck, each bubble promoter having a first side and a second side, the bubble promoters of one tray positioned to align with at least one first spout zone and at least one second spout zone on a plurality of parallel trough-shaped downcomers on an adjacent tray rotated 90 degrees;
an open area of the at least one first spout zone on the first tray being proportional to an open area of a first contacting zone on the second tray, the first contacting zone defined by the first side of the bubble promoter and an associated deck zone;
an open area of the at least one second spout zone on the first tray being proportional to an open area of a second contacting zone of the second tray, the second contacting zone defined by the second side of the bubble promoter and an associated deck zone; and
wherein a ratio of the open area of the first spout zone to the open ar

Assignees

• Uop Llc

Inventors

• Xu Zhanping
• Nowak Brian J

Classifications

• B01D3/22

  with horizontal sieve plates or grids; Construction of sieve plates or grids · CPC title

• B01D3/20

  Bubble caps; Risers for vapour; Discharge pipes for liquid · CPC title

• B01D3/324 Primary

  Tray constructions · CPC title

• B01D3/18 Primary

  with horizontal bubble plates · CPC title