Methods of fabricating vacuum housings with hermetic solder seals using capillary solder wicks
US-11194059-B2 · Dec 7, 2021 · US
US11715616B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11715616-B2 |
| Application number | US-202017082292-A |
| Country | US |
| Kind code | B2 |
| Filing date | Oct 28, 2020 |
| Priority date | Oct 31, 2019 |
| Publication date | Aug 1, 2023 |
| Grant date | Aug 1, 2023 |
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Systems and methods for the batch production of large numbers of highly uniform multichannel-plate photomultiplier tubes (MCP-PMTs) for large-scale applications are provided. The systems and methods employ dual, nested low-vacuum (LV) and UHV processing in a rapid-cycling, small-footprint, scalable, batch-production facility that is capable of fabricating many MCP-PMTs simultaneously.
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What is claimed is: 1. A system for fabricating a plurality of microchannel plate photomultiplier tube (MCP-PMT) detectors, the system comprising: a low-vacuum vessel comprising a housing and a seal, wherein the housing and the seal define an interior volume; a low-vacuum pumping system comprising at least one pump connected to the low-vacuum vessel, the low-vacuum pumping system configured to evacuate the interior volume of the low-vacuum vessel to a pressure in the range from 10 −5 to 10 −8 Torr; a plurality of detector modules contained within the low-vacuum vessel, each detector module comprising: a window; a base, wherein the window and the base define an internal volume of the detector module; and a microchannel-plate photomultiplier tube detector disposed within the internal volume of the detector module; one or more heaters in thermal communication with the detector modules; an ultrahigh-vacuum manifold connected to the internal volumes of the detector modules; and an ultrahigh-vacuum system comprising at least one pump connected to the ultrahigh-vacuum manifold, the ultrahigh-vacuum system configured to evacuate the ultrahigh-vacuum manifold to a pressure of 10 −9 Torr or lower. 2. The system of claim 1 , wherein the seal is an elastomeric O-ring or an elastomeric gasket. 3. The system of claim 1 , further comprising an alkali metal vapor source connected to the ultrahigh-vacuum manifold and configured to introduce an alkali metal vapor into the internal volumes of the detector modules. 4. The system of claim 1 , further comprising: an inert gas source connected to the ultrahigh-vacuum manifold and configured to introduce an inert gas into the internal volumes of the detector modules; and a residual gas analyzer connected to the ultrahigh-vacuum manifold and configured to sample gases present in the internal volumes of the detector modules. 5. The system of claim 1 , wherein the plurality of detector modules comprises at least 100 detector modules. 6. The system of claim 1 , wherein the plurality of detector modules comprises at least 500 detector modules. 7. A method for fabricating a plurality of microchannel plate photomultiplier tube (MCP-PMT) detectors using a system comprising: a low-vacuum vessel comprising a housing and a seal, wherein the housing and the seal define an interior volume; a low-vacuum pumping system comprising at least one pump connected to the low-vacuum vessel; a plurality of detector modules contained within the low-vacuum vessel, each detector module comprising: a window; a base, wherein the window and the base define an internal volume of the detector module; and a microchannel-plate photomultiplier tube detector disposed within the internal volume of the detector module; one or more heaters in thermal communication with the detector modules; an ultrahigh-vacuum manifold connected to the internal volumes of the detector modules; and an ultrahigh-vacuum system comprising at least one pump connected to the ultrahigh-vacuum manifold, the method comprising: placing solder into a gap between the window and the base of the detector modules or adjacent to a gap between the window and the base of the detector modules; evacuating the internal volume of the low-vacuum vessel to a low vacuum pressure in the range from 10 −5 to 10 −8 Torr; evacuating the ultrahigh-vacuum manifold and the internal volumes of the detector modules to an ultrahigh vacuum pressure of 10 −9 Torr or lower; heating the detector modules to a temperature at which the solder melts to fill the gaps between the windows and the bases, while the low vacuum pressure is maintained in the internal volume of the low-vacuum vessel and the ultrahigh vacuum pressure is maintained in the internal volumes of the detector modules; cooling the detector modules to a temperature at which the solder solidifies to form a solder seal between the windows and the bases, while the low vacuum pressure is maintained in the internal volume of the low-vacuum vessel and the ultrahigh vacuum pressure is maintained in the internal volumes of the detector modules; and releasing the vacuum in the internal volume of the low-vacuum vessel. 8. The method of claim 7 , wherein the low vacuum pressure is in the range from 1×10 −5 to 1×10 −7 Torr. 9. The method of claim 7 , further comprising leak testing all or selected detector modules by introducing a tracer gas into the low-vacuum vessel while maintaining the ultrahigh-vacuum pressure in the ultrahigh vacuum manifold and the internal volumes of the detector modules. 10. The method of claim 7 , further comprising forming a photocathode material on cathode surfaces of the microchannel plate detectors while maintaining the ultrahigh-vacuum pressure in the ultrahigh vacuum manifold and the internal volumes of the detector modules. 11. The method of claim 7 , further comprising testing a performance parameter of one or more of the microchannel plate detectors. 12. The method of claim 7 , wherein fabricating the plurality of microchannel plate photomultiplier tube (MCP-PMT) detectors is conducted without heating the low vacuum vessel.
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