Capillary tube connection

Patent metadata

Field	Value
Publication number	US-11714067-B2
Application number	US-202117218018-A
Country	US
Kind code	B2
Filing date	Mar 30, 2021
Priority date	Oct 30, 2015
Publication date	Aug 1, 2023
Grant date	Aug 1, 2023

Abstract

A plug for connecting capillaries includes at least one capillary tube, at least one sealing, and at least one pressure piece. The capillary tube includes a first inner diameter and an open end section. The sealing includes a second inner diameter, a first end section and a shape adapted to seal the open end section of the capillary tube when connected. The pressure piece is adapted to exert at least axial pressure and/or force to at least a part of the sealing. The pressure piece is also adapted to host the first end section of the sealing in abutment with the open end section of the capillary tube so that the capillary tube and the sealing are aligned.

First claim

What is claimed is:

1. A plug for connecting capillaries, the plug comprising:
a) a capillary tube comprising a first inner diameter and an open end section;
b) a supporting structure disposed on a portion of an outer surface of the capillary tube;
c) a sealing comprising a second inner diameter, a first end section, a second end section, and a convex shape, wherein the second end section is oriented opposite to the first end section; and
d) a pressure piece configured to exert an axial force to at least a part of the sealing towards the second end section, the pressure piece including an aperture, wherein the pressure piece is configured to host at least the first end section in the aperture, wherein an end face of the first end section is in abutment with the open end section of the capillary tube so that the first inner diameter of the capillary tube and the second inner diameter of the sealing are aligned, wherein the pressure piece is crimped onto the capillary tube.

2. The plug of claim 1 , wherein the supporting structure abuts the sealing.

3. The plug of claim 1 , wherein the pressure piece is crimped onto the sealing in order to hold the sealing.

4. The plug of claim 1 , in which the open end section includes a flat face, and the first end section further comprises a flat face.

5. The plug of claim 1 , in which the second inner diameter is at least in part larger than the first inner diameter of the capillary tube when the sealing is in an uncompressed state.

6. The plug of claim 1 , in which the sealing includes a maximum diameter being larger than a maximum axial length.

7. A plug for connecting capillaries, the plug comprising:
a) a capillary tube comprising a first inner diameter and an open end section;
b) a supporting structure disposed on a portion of an outer surface of the capillary tube;
c) a sealing comprising a second inner diameter, a first end section, a second end section, an annular shape, and a radial groove, wherein the second end section is oriented opposite to the first end section; and
d) a pressure piece configured to exert an axial force to at least a part of the sealing towards the second end section, the pressure piece including an aperture and a radial ridge configured to engage the radial groove of the sealing, wherein the pressure piece is configured to host at least the first end section in the aperture, wherein an end face of the first end section is in abutment with the open end section of the capillary tube so that the first inner diameter of the capillary tube and the second inner diameter of the sealing are aligned, wherein the pressure piece is crimped onto the capillary tube.

8. The plug of claim 7 , wherein the supporting structure abuts the sealing.

9. The plug of claim 7 , in which the second end section of the sealing extends axially past an end section of the pressure piece by at least 0.2 mm and at most 0.6 mm.

10. The plug of claim 7 , in which the first inner diameter of the capillary tube is at least 10 μm and is at most 500 μm.

11. The plug of claim 7 , in which the second inner diameter of the sealing, in an uncompressed state, is at least 3% in part larger than the first inner diameter of the capillary tube and at most 100% larger than the first inner diameter of the capillary tube.

12. The plug of claim 7 , in which the second inner diameter of the sealing opens to an end face of the second end section with an outwardly flared portion.

13. The plug of claim 12 , in which a largest diameter of the outwardly flared portion of the sealing, in an uncompressed state, is at least 3% in part larger than the first inner diameter of the capillary tube and at most 100% larger than the first inner diameter of the capillary tube.

14. The plug of claim 7 , in which a maximum diameter of the sealing is at least 1.1 times larger than a maximum axial length of the sealing.

15. The plug of claim 7 , in which the second end section of the sealing comprises a larger average diameter than an average diameter of the first end section of the sealing being hosted in the pressure piece.

16. The plug of claim 15 , in which the larger average diameter of the second end section of the sealing is at least 3% larger than the average diameter of the first end section of the sealing.

17. The plug of claim 7 , in which the first end section of the sealing is crimped into an end section of the pressure piece by reducing a diameter of the end section of the pressure piece.

18. The plug of claim 7 , in which the first end section of the sealing is fixed into an end section of the pressure piece by a friction fit of the first end section of the sealing in the end section of the pressure piece.

19. The plug of claim 7 , in which the first end section of the sealing is fixed into an end section of the pressure piece by an adhesive between the first end section of the sealing and the end section of the pressure piece.

20. The plug of claim 7 , in which the first end section of the sealing is injection molded into an end section of the pressure piece.

21. The plug of claim 7 , in which an average diameter of the first end section of the sealing is at most 30% larger than an outer diameter of the capillary tube.

22. The plug of claim 7 , in which the sealing comprises a material selected from the group consisting of a PEEK (Polyetheretherketone) material and a PAEK (Polyaryletherketone) material.

23. The plug of claim 7 , in which the sealing is configured to abut and seal an inner face of a bushing by the second end section, and the bushing is adapted to connect the capillary tube and a bushing capillary.

24. A plug for connecting capillaries, the plug comprising:
a) a capillary tube comprising a first inner diameter and an open end section;
b) a supporting structure disposed on a portion of an outer surface of the capillary tube;
c) a sealing comprising a second inner diameter, a first end section, a second end section, an annular shape, and a radial ridge, wherein the second end section is oriented opposite to the first end section; and
d) a pressure piece configured to exert an axial force to at least a part of the sealing towards the second end section, the pressure piece including an aperture and a radial groove configured to engage the radial ridge of the sealing, wherein the pressure piece is configured to host at least the first end section in the aperture, wherein an end face of the first end section is in abutment with the open end section of the capillary tube so that the first inner diameter of the capillary tube and the second inner diameter of the sealing are aligned, wherein the pressure piece is crimped onto the capillary tube.

25. The plug of claim 24 , wherein the pressure piece is crimped onto the sealing in order to hold the sealing.

26. A method for connecting capillaries, the method comprising:
inserting a plug into a cavity of a bushing, the plug comprising:
a) a capillary tube comprising a first inner diameter and an open end section;
b) a supporting structure disposed on a portion of an outer surface of the capillary tube;
c) a sealing comprising a second inner diameter, a first end section, a second end section, and a convex shape, wherein the second end section is oriented opposite to the first end section; and
d) a pressure piece configured to exert an axial force to at least a part of the sealing towards the second end section, the pressure p

Assignees

• Dionex Softron Gmbh

Inventors

• Wachinger Thomas
• Buerger Daniel

Classifications

• G01N30/6026 Primary

  Fluid seals · CPC title

• F16L19/0206

  the collar not being integral with the pipe · CPC title

• F16L19/0212

  using specially adapted sealing means · CPC title

• G01N30/6039

  in series · CPC title