Liquid sulfur degassing

Patent metadata

Field	Value
Publication number	US-11713246-B2
Application number	US-202016816484-A
Country	US
Kind code	B2
Filing date	Mar 12, 2020
Priority date	Mar 15, 2019
Publication date	Aug 1, 2023
Grant date	Aug 1, 2023

Abstract

A method and system for liquid sulfur degassing is disclosed. The method and system generally involve degassing liquid sulfur in a degassing vessel, and the level of the liquid sulfur in the degassing vessel is controlled in the degassing vessel by determining the level of liquid sulfur in the degassing vessel.

First claim

What is claimed is:

1. A method of treating liquid sulfur containing polysulfides and hydrogen sulfide, comprising:
contacting the liquid sulfur with stripping gas in a contact zone of a degassing vessel, thereby froth is formed in the degassing vessel and there is a level of froth in the degassing vessel;
determining a level of the liquid sulfur in the degassing vessel, wherein the determining the level of the liquid sulfur in the degassing vessel comprises:
measuring a second level of the liquid sulfur via a sensor in a level bridle that is fluidly connected to the degassing vessel, wherein the sensor is configured to measure liquid level via differential pressure, radar, capacitance, or combinations thereof, where the second level is different than the level of froth present on the liquid sulfur within the degassing vessel; and
determining the level of the liquid sulfur in the degassing vessel based on the second level measured in the level bridle by analyzing and calculating the level of the liquid sulfur in the degassing vessel based on correlation data stored on the memory of a controller; and

controlling the level of the liquid sulfur in the degassing vessel based on the step of determining the level of the liquid sulfur in the degassing vessel.

2. The method of claim 1 , wherein the froth in the degassing vessel results from the contacting, wherein the controlling the level of the liquid sulfur is not affected by the froth in the degassing vessel.

3. The method of claim 1 , wherein the controlling the level of the liquid sulfur comprises:
actuating a control valve located in a conduit comprising degassed liquid sulfur.

4. The method of claim 1 , further comprising:
before contacting the liquid sulfur with the stripping gas, contacting the liquid sulfur with a decomposition catalyst.

5. The method of claim 4 , wherein the decomposition catalyst is in a catalyst bed.

6. The method of claim 5 , wherein the catalyst bed is placed in the degassing vessel and above the contact zone.

7. The method of claim 6 , wherein the catalyst bed is a ring-shaped catalyst bed.

8. The method of claim 5 , wherein the catalyst bed is attached to a portion side of the degassing vessel.

9. The method of claim 5 , wherein the catalyst bed is in a second vessel, the method further comprising:
receiving a liquid sulfur feed stream into the second vessel; and
flowing a hydrogen sulfide enriched liquid sulfur stream from the second vessel to the degassing vessel.

10. The method of claim 1 , wherein the level bridle is fluidly connected to the degassing vessel by a first conduit and a second conduit, wherein the first conduit is in fluid communication with the liquid sulfur in the degassing vessel, wherein the second conduit is in fluid communication with a vapor space of the degassing vessel.

Assignees

• Fluor Tech Corp

Inventors

• Fenderson Stephen N
• Chow Thomas K T

Classifications

• C01B17/0232 Primary

  Purification, e.g. degassing · CPC title

• B01D19/0005

  with one or more auxiliary substances · CPC title

• B01D19/0063

  Regulation, control including valves and floats (for construction and details of valves F16K) · CPC title