Method for manufacturing material powder for metal laminating modelling

Patent metadata

Field	Value
Publication number	US-11701711-B2
Application number	US-202016929130-A
Country	US
Kind code	B2
Filing date	Jul 15, 2020
Priority date	Jul 31, 2019
Publication date	Jul 18, 2023
Grant date	Jul 18, 2023

Abstract

Provided is a method for manufacturing material powder for metal laminating modelling, in which a virgin material is manufactured based on the particle size distribution of the virgin material being an unused material powder, and the fluidity of an unsintered reused material after the virgin material is reused a predetermined number of times by a metal laminating modelling device, so that the particle size distribution of the virgin material corresponds to the fluidity of the reused material that is equal to or greater than a predetermined standard value. Silica particles may be added to the virgin material.

First claim

What is claimed is:

1. A method for metal laminating modelling, comprising:
measuring a particle size distribution of a trial virgin material being a material powder that is unused;
performing a durability test comprising:
(a) supplying the trial virgin material to a metal laminating modelling device;
(b) recovering an unsintered material being at least a portion of the trial virgin material that is unsintered and discharge from the metal laminating modelling device after the step (a);
(c) re-supplying the unsintered material to the metal laminating modelling device;
(d) recovering the unsintered material discharged from the metal laminating modelling device after the step (c);
(e) repeating the (c) and (d) steps for n times, where n is more than 19 times;
(f) measuring a fluidity of the unsintered material after the step (e) by measuring a discharge time and an angle of repose of the unsintered material, wherein the discharge time of the unsintered material is a time from the start of the falling of the unsintered material from a discharge port of a funnel by its own weight to the completion of the falling, and the angle of repose of the unsintered material is an angle formed by a slope and a horizontal surface of a pile of the unsintered material when the unsintered material is made to fall from the funnel and the pile of the unsintered material does not collapse spontaneously;

obtaining a predetermined standard value of the fluidity by measuring a standard discharge time and a standard angle of repose of a standard material, being a material that forms a material powder layer having a uniform thickness and density, wherein the standard discharge time of the standard material is a time from the start of the falling of the standard material from the discharge port of the funnel by its own weight to the completion of the falling, and the angle of repose of the standard material is an angle formed by a slope and a horizontal surface of a pile of the standard material when the standard material is made to fall from the funnel and the pile of the standard material does not collapse spontaneously;
wherein, if the fluidity of the unsintered material obtained in the step (f) is equal to or greater than the predetermined standard value, setting the particle size distribution of the trial virgin material as a predetermined particle size distribution, and producing a virgin material being the material powder having the predetermined particle size distribution for metal laminating modelling, and performing the metal laminating modelling after the durability test by:
repeating a recoating step of forming a material powder layer by the material powder obtained, and a sintering step of irradiating the material powder layer with a laser light in the metal laminating modelling device; and
collecting an unsintered material from the metal laminating modelling device for reuse, and reusing the unsintered material collected for x times in the recoating step and the sintering step such that the fluidity of the unsintered material will not reduce below the predetermined standard value of the fluidity, wherein the x times is determined by a measurement result from the durability test, wherein if the fluidity of the unsintered material is determined by the measurement result to be equal to or greater than the predetermined standard value, then then times performed in step (e) of the durability test is set as the x times performed in the recoating and sintering step; and
if the fluidity of the unsintered material obtained in the step (f) is lower than the predetermined standard value,
producing a second trial virgin material, being the material powder that is unused and having another particle size distribution different from the particle size distribution of the trial virgin material, and performing the durability test again using the second trial virgin material, and confirming the fluidity of an unsintered material of the second trial virgin material measured from the durability test, or
adding silica particles to a new unused batch of the trial virgin material having the particle size distribution until the predetermined standard value of the fluidity is reached, and determining an addition amount of the silica particles as a predetermined addition amount, and producing a virgin material being the material powder having the predetermined addition amount of silica particles added thereto for metal laminating modelling, and performing the metal laminating modelling after the durability test by:
repeating a recoating step of forming the material powder layer by the material powder obtained, and a sintering step of irradiating the material powder layer with a laser light in the metal laminating modelling device; and
collecting an unsintered material from the metal laminating modelling device for reuse, and reusing the unsintered material collected for y times in the recoating step and the sintering step such that the fluidity of the unsintered material will not reduce below the predetermined standard value of the fluidity, wherein the y times is determined by a measurement result from the durability test, wherein if the fluidity of the unsintered material is determined by the measurement result to be equal to or greater than the predetermined standard value, then the n times performed in step (e) of the durability test is set as the y times performed in the recoating and sintering step.

2. The method for metal laminating modelling according to claim 1 , wherein
the durability test is implemented without performing the metal laminating modelling.

3. The method for metal laminating modelling according to claim 1 , wherein
in the particle size distribution, a frequency of the particles having a particle diameter of 17 μm or less is 4% or less.

4. The method for metal laminating modelling according to claim 3 , wherein
in the particle size distribution,
a median diameter indicating the particle diameter that accounts for 50% in a cumulative distribution is within a range of 17 μm or more and 53 μm or less,
a mode diameter indicating the particle diameter that has a maximum frequency in the frequency distribution is within a range of 17 μm or more and 53 μm or less, and
the frequency of the particles having a particle diameter of 17 μm or less is 3% or less.

5. The method for metal laminating modelling according to claim 1 , wherein
the silica particles have a particle diameter of 5 nm or more and 15 nm or less.

6. The method for metal laminating modelling according to claim 1 , wherein the method further comprises:
performing a second durability test, comprising:
(a′) supplying the virgin material being the material powder having the predetermined addition amount of silica particles to the metal laminating modelling device;
(b′) recovering a second unsintered material being at least a portion of the virgin material having the predetermined addition amount of silica particles that is unsintered and discharged from the metal laminating modelling device after the step (a′);
(c′) re-supplying the second unsintered material to the metal laminating modelling device;
(d′) recovering the second unsintered material discharged from the metal laminating modelling device after the step (c′);
(e′) repeating the (c′) and (d′) steps more than 19 times;
(f′) measuring a fluidity of the second unsintered material after the step (e′) by measuring a discharge time and an angle of repose of the second unsintered material, wherein the discharge time of the second unsintered material is a time from the start of the falling of the second unsintered material from the discharge port of the funnel by its own weight to the completion of the falling, and the angle of repose of the second unsintered material is an angle fo

Assignees

• Sodick Co Ltd

Inventors

• Muranaka Katsutaka

Classifications

• B22F10/73 Primary

  of powder · CPC title

• B22F1/052 Primary

  characterised by a mixture of particles of different sizes or by the particle size distribution · CPC title

• B22F9/04

  starting from solid material, e.g. by crushing, grinding or milling ({C22C1/1084 takes precedence}; crushing, grinding or milling, in general, see the relevant subclasses, e.g. B02C) · CPC title

• B22F10/00

  Additive manufacturing of workpieces or articles from metallic powder (apparatus or devices therefor B22F12/00) · CPC title

• B22F10/34

  of powder characteristics, e.g. density, oxidation or flowability · CPC title