Process-intensified flow reactor

Patent metadata

Field	Value
Publication number	US-11679368-B2
Application number	US-202117517104-A
Country	US
Kind code	B2
Filing date	Nov 2, 2021
Priority date	Jul 31, 2017
Publication date	Jun 20, 2023
Grant date	Jun 20, 2023

Abstract

A flow reactor has a module having a process fluid passage with an interior surface, a portion of the passage including a cross section along the portion having a cross-sectional shape, and a cross-sectional area with multiple minima along the passage. The cross-sectional shape varies continually along the portion and the interior surface of the portion includes either no pairs of opposing flat parallel sides or only pairs of opposing flat parallel sides which extend for a length of no more than 4 times a distance between said opposing flat parallel sides along the portion and the portion contains a plurality of obstacles distributed along the portion.

First claim

What is claimed is:

1. A module for a flow reactor, comprising:
a module body defining a fluid passage therein, the fluid passage having an interior surface and comprising a portion, the portion including (i) an input end and an outlet end at which process fluid is configured to flow into the portion and out of the portion, respectively, (ii) a plurality of successive chambers each with a nozzle-like entrance and a narrowing exit, and (iii) a cross section delimited by the interior surface of the fluid passage along the portion,
wherein the cross section has a cross-sectional shape that varies continually along the portion, wherein the interior surface includes no pairs of opposing flat parallel sides at least along portions other than one or more of the entrance and the exit to the successive chambers, and wherein a plurality of obstacles are positioned along the portion between the input end and the output end.

2. The module of claim 1 , wherein one chamber of said successive chambers is nested with a next-succeeding chamber of said successive chambers such that the narrowing exit of the one chamber forms the nozzle-like entrance of the next adjacent succeeding chamber.

3. The module of claim 1 , wherein at least one of the plurality of obstacles is located within a first chamber and intersects a straight line having a first endpoint located at a center of the entrance of the first chamber and a second endpoint locate at a center of the exit of the first chamber.

4. The module of claim 3 , wherein the at least one of the plurality of obstacles intersects every straight line having a first end point within the entrance of the first chamber and a second endpoint within the exit of the first chamber.

5. The module of claim 3 , further comprising one or more bypass paths, positioned between the at least one obstacle and an inside surface of the first chamber, around the at least one obstacle of the plurality of obstacles.

6. The module of claim 5 , wherein the one or more bypass paths have a total cross-sectional area greater than the total cross-sectional area of the exit of the first chamber.

7. The module of claim 5 , wherein the at least one obstacle has one or more openings extending through the at least one obstacle.

8. The module of claim 5 , wherein the at least one obstacle has no openings extending through the at least one obstacle.

9. The module of claim 3 , wherein the at least one obstacle of the plurality of obstacles comprises at least one obstacle per chamber.

10. The module of claim 3 , further comprising two or more obstacles in a single chamber.

11. The module of claim 10 , wherein the two or more obstacles in a single chamber extend from opposite sides of the interior surface.

12. The module of claim 3 , wherein the at least one obstacle has two or more bypass paths.

13. The module of claim 12 , wherein the bypass paths are separated by the obstacle by a distance of at least twice a maximum diameter of the exit of the chamber.

14. The module of claim 3 , wherein the at least one obstacle has a single bypass path.

15. The module of claim 3 , wherein the at least one obstacle has two bypass paths, the two bypass paths positioned on opposite sides of the fluid passage relative to one another.

16. The module of claim 1 , wherein the at least one of the plurality of obstacles comprises a flat or concave surface aligned generally perpendicularly to the fluid passage, the flat or concave surface facing in a downstream direction or an upstream direction.

17. The module of claim 1 , wherein the at least one of the plurality of obstacles comprises a tapering elongated end pointing in a downstream direction or an upstream direction.

18. The module of claim 1 , wherein the interior surface of the portion comprises a height that varies periodically along the portion.

19. The module of claim 18 , wherein one or more of:
the height varies periodically with a length of each of the successive chambers such that the successive chambers are essentially identical, and
a period of variation in the height of the portion is different than the length of each successive chamber such that the successive chambers are different.

20. The module of claim 1 , wherein at least one of the plurality of obstacles extends only partially across a height of the chamber and a cross section of the at least one obstacle varies along a height of the obstacle.

Assignees

• Corning Inc

Inventors

• Jean Patrick
• Lavric Elena Daniela

Classifications

• B01F2101/2204

  Mixing chemical components in generals in order to improve chemical treatment or reactions, independently from the specific application · CPC title

• B01J2219/00891

  Feeding or evacuation · CPC title

• B01J2219/00889

  Mixing · CPC title

• B01J19/0093 Primary

  Microreactors, e.g. miniaturised or microfabricated reactors (laboratory containers with capillary fluid transport in microfabricated channels or chambers B01L3/5027) · CPC title

• B01J2219/00813

  Fluidic connections · CPC title