Process for manufacturing a ceramic composite material part by pressurized injection of a loaded slurry into a porous mould
US-2018297901-A1 · Oct 18, 2018 · US
US11655193B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11655193-B2 |
| Application number | US-201816648427-A |
| Country | US |
| Kind code | B2 |
| Filing date | Sep 18, 2018 |
| Priority date | Sep 19, 2017 |
| Publication date | May 23, 2023 |
| Grant date | May 23, 2023 |
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A method for injecting a loaded suspension into a fibrous texture having a three-dimensional or multilayer weaving includes the injection of a suspension containing a powder of solid particles into the volume of the fibrous texture. The injection of the loaded suspension is carried out by at least one hollow needle in communication with a loaded suspension supply device, each needle being movable in at least one direction extending between a first face and a second opposite face of the fibrous texture so as to inject the loaded suspension at one or more determined depths in the fibrous texture.
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The invention claimed is: 1. A method for injecting a loaded suspension into a fibrous texture having a three-dimensional or multilayer weaving in which at least some of weft yarns link warp yarns on several layers of warp yarns or vice versa, said method comprising injecting a suspension containing a powder of solid particles into a volume of the fibrous texture, wherein the injecting of the loaded suspension is carried out by means of at least one hollow needle in communication with a loaded suspension supply device, each needle being configured to cross a thickness of the fibrous texture and move in at least one direction extending between a first face and a second opposite face of the fibrous texture so as to inject the loaded suspension at a plurality of determined depths in the fibrous texture as a result of the movement of the needle. 2. The method according to claim 1 , wherein each hollow needle has an external diameter of between 0.4 mm and 0.8 mm. 3. The method according to claim 1 , wherein each hollow needle has a beveled end. 4. The method according to claim 1 , wherein the needle(s) is/are moved sequentially between the first face and the second opposite face of the fibrous texture, the needle(s) being stopped at intermediate positions between these two faces, a determined dose of loaded suspension being injected into the texture at each intermediate position. 5. The method according to claim 1 , wherein the at least one needle is moved continuously between the first face and the second opposite face of the fibrous texture, the loaded suspension being injected continuously at a determined flow rate into the fibrous texture. 6. The method according to claim 1 , wherein, during the injecting of the loaded suspension, the fibrous texture is placed in a compaction tooling comprising at least on one face one or more through holes for the needle(s). 7. The method according to claim 1 , wherein the injecting of the loaded suspension into the fibrous texture is carried out without draining a liquid phase of the suspension. 8. A method for manufacturing a part made of composite material comprising: forming a fibrous texture by three-dimensional or multilayer weaving between a plurality of yarns, injecting a loaded suspension into the fibrous texture according to claim 1 , the loaded suspension comprising at least one liquid or solid precursor of a matrix, compacting the injected fibrous texture, transforming said at least one precursor into a matrix. 9. The method according to claim 8 , wherein the yarns of the fibrous texture are formed of refractory ceramic fibers, the loaded suspension containing refractory ceramic particles as a solid precursor of a ceramic matrix, the method comprising heat treating the refractory ceramic particles present in the fibrous texture in order to form a refractory ceramic matrix in said texture. 10. The method according to claim 9 , wherein the refractory ceramic particles are made of a material chosen from: alumina, mullite, silica, an aluminosilicate, an aluminophosphate, zirconia, a carbide, a boride and a nitride. 11. The method according to claim 8 , wherein the yarns of the fibrous texture are formed of fibers consisting of one or more of the following materials: alumina, mullite, silica, an aluminosilicate, a borosilicate, silicon carbide and carbon.
based on silicon carbide · CPC title
obtaining fibres · CPC title
based on silica · CPC title
Silica or silicates other than aluminosilicates, e.g. quartz · CPC title
Silicon carbide · CPC title
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