Coated optical fiber and method of making same

Patent metadata

Field	Value
Publication number	US-11655185-B2
Application number	US-202016839281-A
Country	US
Kind code	B2
Filing date	Apr 3, 2020
Priority date	May 6, 2019
Publication date	May 23, 2023
Grant date	May 23, 2023

Abstract

A method is disclosed of making a coated optical fiber. The method may involve drawing a preform through a furnace to create a fiber having a desired diameter and cross sectional shape. The fiber is then drawn through a slurry, wherein the slurry includes elements including at least one of metallic elements, alloy elements or dielectric elements, and the slurry wets an outer surface of the fiber. As the fiber is drawn through the slurry, it is then drawn through a forming die to impart a wet coating having a desired thickness on an outer surface of the fiber. The wet fiber is then drawn through an oven or ovens configured to heat the wet coating sufficiently to produce a consolidated surface coating on the fiber as the fiber exits the oven or ovens.

First claim

What is claimed is:

1. A method of making a coated fiber, comprising:
drawing a preform through a furnace to create a fiber having a desired diameter and cross sectional shape;
continuing to draw the fiber through a slurry, wherein the slurry includes a plurality of elements, the plurality of elements including at least one of metallic elements, alloy elements or dielectric elements, and the slurry wets an outer surface of the fiber;
as the fiber is drawn through the slurry, drawing the fiber though a funnel-shaped forming die having an aperture at a lower end thereof, with a diameter of the aperture selected based on a viscosity of the slurry and a desired thickness of a wet coating to be imparted on an outer surface of the fiber, to create a wet fiber; and
continuing to draw the wet fiber into and through an oven configured to heat the wet coating sufficiently to produce a consolidated surface coating on the fiber as the fiber exits the oven; and
controlling a rheology of the slurry in part by controlling a temperature of the slurry as the fiber is drawn through the funnel-shaped forming die, and in part by at least one of:
adding at least one chemical compound to the slurry; or
subtracting at least one chemical compound from the slurry; or
modifying a concentration of at least one constituent of the slurry; and

wherein controlling the rheology of the slurry helps to control the viscosity of the slurry, to in turn control leakage of the slurry through the aperture while the fiber is being drawn through the aperture.

2. The method of claim 1 , wherein the plurality of elements includes metal particles comprised of at least one of metal powder particles or granular metal particles.

3. The method of claim 1 , wherein drawing the fiber through a slurry comprises using a vertically arranged draw tower to draw the fiber through the slurry.

4. The method of claim 1 , wherein the plurality of elements comprises at least one of: a naturally occurring metal which is not pyrophoric.

5. The method of claim 4 , wherein the slurry comprises a solvent which is evaporated during heating of the wet coating.

6. The method of claim 1 , wherein the plurality of elements comprises metallic elements including at least one of copper (CU), chromium (Cr), Titanium (Ti), gold (Au) or nickel (Ni).

7. The method of claim 1 , wherein the plurality of elements further comprise a dielectric, and the dielectric comprises magnesium fluoride (MgF 2 ).

8. The method of claim 1 , wherein the elements comprise gallium, and the slurry comprises liquid gallium.

9. The method of claim 8 , wherein the liquid gallium, when heated using the oven, forms the consolidated surface coating as a gallium oxide coating (Ga 2 O 3 ).

10. The method of claim 1 , wherein drawing the fiber through a slurry comprises drawing the fiber through a die element, wherein the die element holds a quantity of the slurry.

11. The method of claim 1 , wherein drawing the fiber into and through an oven comprises drawing the fiber into and through an oven filled with at least one of:
an inert gas to prevent oxidation;
a reactive gas to promote a desired characteristic of the consolidated surface; or
an inert gas to enable the use of metals or dielectrics that are pyrophoric.

12. The method of claim 1 , wherein drawing the fiber into and through an oven comprises drawing the fiber into and through an oven formed by a plurality of spaced apart oven units such that at least one of:
the fiber passes past each of the oven units and is evenly heated by the oven units; or
the fiber passes past each of the oven units and is exposed to different temperatures by each oven unit, at least one of the different temperatures being sufficient to melt the elements.

13. The method of claim 12 , wherein at least one of the oven units is operated to reach a temperature of at least 300 degrees C.

14. The method of claim 1 , wherein drawing the preform through a furnace comprises drawing a telecom-grade fused silica rod through the furnace.

15. The method of claim 1 , wherein the furnace produces a temperature of at least about 700 degrees C.

16. The method of claim 1 , further comprising using a puller wheel structure having a spool, the spool receiving the fiber after the fiber exits the oven.

17. A method of making a coated fiber, comprising:
drawing a preform through a furnace using a vertical draw tower to create a fiber having a desired diameter and a cross sectional shape;
continuing to draw the fiber through an aperture of a funnel-shaped die element containing a slurry, the slurry containing at least one of metal elements or dielectric elements, the die element disposed elevationally below the furnace such that the slurry coats the fiber with a portion of the slurry to form a wet coating on the fiber as the fiber passes through the aperture, thus creating a wet fiber, and the aperture being dimensioned such that the wet coating has a desired thickness;
controlling a rheology of the slurry by controlling a temperature of the slurry as the fiber is drawn through the funnel-shaped die element, wherein controlling the rheology of the slurry further includes at least one of:
adding at least one chemical compound to the slurry; or
subtracting at least one chemical compound from the slurry; or
modifying a concentration of at least one constituent of the slurry; and

wherein controlling the rheology of the slurry helps to control a viscosity of the slurry, to in turn control leakage of the slurry through the aperture while the fiber is being drawn through the aperture;
continuing to draw the wet fiber into an oven disposed elevationally below the funnel-shaped die element;
using the oven to evenly heat the wet fiber such that the wet coating is consolidated to form a consolidated surface on the fiber; and
further comprising using an inert gas within the oven to prevent oxidation.

18. The method of claim 17 , wherein drawing a preform through the furnace comprises drawing a telecom-grade fused silica rod through the furnace.

19. The method of claim 17 , wherein the at least one of metal elements or dielectric elements comprise naturally occurring metals which are not pyrophoric.

20. The method of claim 17 , wherein the at least one of metal elements comprises at least one of copper, chromium, titanium, gold or nickel.

21. A system for creating a metallic coated fiber, comprising:
a vertically arranged draw tower having a furnace, the vertically arranged draw tower configured to draw a preform through the furnace to create a fiber having a desired diameter and a cross sectional shape as the fiber leaves the furnace;
a funnel shaped die element having an aperture at a lower end, the aperture having a diameter configured based on a desired thickness of a wet coating and a viscosity of a slurry being used to form a wet coating on the fiber, the funnel shaped die element containing the slurry, the slurry containing at least one of metal elements or dielectric elements, the funnel shaped die element disposed elevationally below the furnace such that the slurry coats the fiber with a portion of the slurry to form the wet coating on the fiber as the fiber passes through the aperture, and wherein a rheology of the slurry is controlled at least in part by controlling the temperature of the slurry to further control the viscosity to prevent leakage from the aperture, and in part by at least one of:
adding at least one chemical compound to the slurry; or
subtracting a

Assignees

• L Livermore Nat Security Llc

Inventors

• Messerly Michael
• Calta Nicholas
• Elhadj Selim
• Lange Andrew
• Mart Cody Wren
• Mellors Robert
• Schenkel Nick
• Yu Charles Xiao

Classifications

• C03C25/1063 Primary

  Metals · CPC title

• C03C25/1061 Primary

  Inorganic coatings · CPC title

• C03C25/18

  Extrusion · CPC title

• C03B37/15

  with heat application, e.g. for making optical fibres (fusion-splicing of light guides G02B6/255; treatment of light guides to shape optical elements {G02B6/2835, G02B6/2856}) · CPC title

• C03B2205/40

  Monitoring or regulating the draw tension or draw rate · CPC title