Methods and apparatuses for making compositions comprising an acid and an acid degradable component and/or compositions comprising a plurality of selectable components
US-10631558-B2 · Apr 28, 2020 · US
US11644353B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11644353-B2 |
| Application number | US-201917273982-A |
| Country | US |
| Kind code | B2 |
| Filing date | Sep 6, 2019 |
| Priority date | Sep 6, 2018 |
| Publication date | May 9, 2023 |
| Grant date | May 9, 2023 |
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A flow control module with a thermal mass flow meter is provided. The thermal mass flow meter facilitates measuring both a flow rate and a temperature of a fluid passing through the flow control module. Fluids may experience different flow characteristics at different temperature ranges. The flow control module includes a proportional control valve for selectively adjusting the flow rate of the fluid passing through the flow control module. Upon detecting that the temperature of the fluid is outside of a temperature range for the fluid, a controller is configured to load a different set of calibration parameters for controlling the operation of the proportional control valve to accommodate the different flow characteristics of the fluid at that temperature. Additionally, the controller is configured to detect bubbles using the thermal mass flow meter based upon the difference in thermal conductivity of gasses and liquids.
Opening claim text (preview).
What is claimed is: 1. A flow control module, comprising: a housing having an inlet and an outlet and a passageway extending between the inlet and the outlet, the passageway defining a flow path through the flow control module; a thermal mass flow meter, the thermal mass flow meter located between the inlet and the outlet along the flow path, wherein the thermal mass flow meter is configured to communicate a first signal based on a flow rate of a fluid along the flow path; a first solenoid assembly mounted to the housing, the first solenoid assembly configured as an on/off solenoid assembly such that the first solenoid assembly is operable to allow the fluid to flow along the flow path in an on position and prevent the fluid from flowing along the flow path in an off position; and a second solenoid assembly mounted to the housing, the second solenoid assembly configured as a proportional solenoid assembly such that the second solenoid assembly is operable to receive a second signal in response to communication of the first signal and to proportionally control a flow rate of the fluid along the flow path through the flow control module based on the second signal, wherein the thermal mass flow meter is further configured to communicate a third signal based on a measured temperature of the fluid, wherein the second solenoid assembly is further configured to proportionally control the flow rate of the fluid based on a new set of calibration parameters upon a determination that the measured temperature of the fluid is outside a temperature range for the fluid. 2. The flow control module of claim 1 , wherein the new set of calibration parameters change one or more of a location of an armature of the second solenoid assembly for a given flow rate, how often the second solenoid assembly makes adjustments made to proportionally control the flow rate, or how fast the armature of the second solenoid assembly moves to proportionally control the flow rate. 3. The flow control module of claim 1 , wherein the thermal mass flow meter comprises a heater and a temperature sensor located at a distance toward the outlet relative to the heater. 4. The flow control module of claim 3 , wherein the thermal mass flow meter further comprises a second temperature sensor located at the distance toward the inlet relative to the heater. 5. The flow control module of claim 3 , wherein the thermal mass flow meter is configured to generate the first signal based on a measured amount of heat transferred from the heater to the temperature sensor. 6. The flow control module of claim 5 , wherein the first signal is a voltage or current value of the measured amount of heat transferred or a flow rate value determined by the thermal mass flow meter based on the measured amount of heat transferred. 7. The flow control module of claim 3 , wherein the temperature sensor comprises a thermocouple, a thermopile, or thermistor. 8. A fluid dispenser, comprising: a controller; and a flow control module, the flow control module comprising: a housing having an inlet and an outlet and a passageway extending between the inlet and the outlet, the passageway defining a flow path through the flow control module; a thermal mass flow meter, the thermal mass flow meter located between the inlet and the outlet along the flow path, wherein the thermal mass flow meter is configured to communicate a first signal to the controller based on a flow rate of a fluid along the flow path; a shut-off valve configured to allow the fluid to flow along the flow path in an open position and prevent the fluid from flowing along the flow path in a closed position; and a proportional control valve configured to receive a second signal from the controller in response to communication of the first signal and to proportionally control a flow rate of the fluid along the flow path through the flow control module based on the second signal, wherein the controller is further configured to detect a change in phase of the fluid based on a comparison of the first signal to a threshold value indicative of the change in phase of the fluid. 9. The fluid dispenser of claim 8 , wherein the controller is configured to determine the flow rate of the fluid based on the first signal. 10. The fluid dispenser of claim 9 , wherein the first signal is a voltage or current value produced by the thermal mass flow meter or a flow rate value determined by the thermal mass flow meter. 11. The fluid dispenser of claim 9 , wherein the controller is further configured to compare the determined flow rate of the fluid to a predetermined flow rate and to generate the second signal based on the comparison. 12. The fluid dispenser of claim 11 , wherein the controller is further configured to receive the predetermined flow rate from a database. 13. The fluid dispenser of claim 8 , wherein the controller is further configured to detect a bubble based on the change in phase of the fluid. 14. The fluid dispenser of claim 13 , wherein the controller is configured to detect the bubble based upon detection of the change in phase for more than a predetermined threshold amount of time. 15. The fluid dispenser of claim 13 , wherein the controller is further configured to generate a maintenance alert or a sold-out alert upon detection of a threshold number of bubbles or a threshold number of bubbles within a predetermined time period. 16. A sold-out detection system, comprising: a sold-out sensor comprising: a housing comprising an inlet and an outlet and a passageway extending between the inlet and the outlet, the passageway defining a flow path through the sold-out sensor; and a thermal mass flow meter comprising a heater and a temperature sensor located at a distance toward the outlet relative to the heater, wherein the thermal mass flow meter is configured to generate a first signal based on a measured amount of heat transferred from the heater to the temperature sensor by a flow of a fluid along the flow path; and a controller configured to receive the first signal and detect a change in phase of the fluid based on a comparison of the first signal to a threshold value indicative of the change in phase of the fluid, wherein the controller is further configured to detect a bubble based on the detected change in phase of the fluid, and wherein the controller is further configured to detect a sold-out condition upon detection of a threshold number of bubbles or a threshold number of bubbles within a predetermined time period.
Structural arrangements; Mounting of elements, e.g. in relation to fluid flow · CPC title
using a particular type of heating, cooling or sensing element {(G01F1/6847 takes precedence)} · CPC title
by action on throttling means (G05D7/0688, G05D7/0694 take precedence) · CPC title
Circuits therefor, e.g. constant-current flow meters · CPC title
characterised by the set value given to the control element · CPC title
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