Method of manufacturing ceramic tape

Patent metadata

Field	Value
Publication number	US-11629915-B2
Application number	US-202117468752-A
Country	US
Kind code	B2
Filing date	Sep 8, 2021
Priority date	Jun 29, 2015
Publication date	Apr 18, 2023
Grant date	Apr 18, 2023

Abstract

A method of manufacturing ceramic tape includes a step of directing a tape of partially-sintered ceramic into a furnace. The tape is partially-sintered such that grains of the ceramic are fused to one another yet the tape still includes at least 10% porosity by volume, where the porosity refers to volume of the tape unoccupied by the ceramic. The method further includes steps of conveying the tape through the furnace and further sintering the tape as the tape is conveyed through the furnace. The porosity of the tape decreases during the further sintering step.

First claim

What is claimed is:

1. A method of manufacturing ceramic tape, comprising:
directing a tape of partially-sintered ceramic into a furnace, wherein the tape is partially-sintered such that grains of the ceramic are fused to one another yet the tape still includes at least 10% porosity by volume, where the porosity refers to volume of the tape unoccupied by the ceramic;
conveying the tape through the furnace; and
further sintering the tape as the tape is conveyed through the furnace, wherein the porosity of the tape decreases during the further sintering.

2. The method of claim 1 , further comprising drawing the tape of partially-sintered ceramic from a source prior to directing the tape into the furnace.

3. The method of claim 2 , wherein the source is a spool of the tape of partially-sintered ceramic.

4. The method of claim 1 , further comprising applying tension to the tape during the further sintering.

5. The method of claim 4 , further comprising holding the tape flat with the tension during the further sintering.

6. The method of claim 5 , wherein the tension comprises 20 megapascals.

7. The method of claim 1 , following the further sintering, further comprising winding the tape on a spool.

8. The method of claim 7 , wherein the spool has a diameter of at least 0.5 cm.

9. The method of claim 8 , wherein length of the tape on the spool is at least 10 m, width is at least 10 mm, and thickness is at least 10 μm.

10. The method of claim 9 , wherein the width is no greater than 20 cm and the thickness is no greater than 500 μm.

11. The method of claim 1 , wherein, during the further sintering, temperatures experienced by portions of the tape in the furnace are at least 800° C., while other portions of the tape outside the furnace are experiencing lower temperatures.

12. The method of claim 11 , wherein the other portions of the tape outside of the furnace are experiencing room temperature.

13. The method of claim 1 , wherein the porosity of the tape after the further sintering is less than 1%.

14. The method of claim 1 , wherein the ceramic comprises alumina, zirconia, lithium garnet, and/or spinel.

15. The method of claim 1 , wherein the tape is conveyed through the furnace at a rate of at least 1 inch per minute.

16. The method of claim 1 , wherein, as the tape is directed into the furnace, the tape still includes at least 30% porosity by volume.

17. A method of manufacturing ceramic tape, comprising:
drawing a tape of partially-sintered ceramic from a source, wherein the tape is partially-sintered such that grains of the ceramic are fused to one another yet the tape still includes at least 10% porosity by volume, where the porosity refers to volume of the tape unoccupied by the ceramic;
directing the tape of partially-sintered ceramic into a furnace,
conveying the tape through the furnace;
further sintering the tape as the tape is conveyed through the furnace, wherein the porosity of the tape decreases during the further sintering; and
applying tension to the tape during the further sintering.

18. The method of claim 17 , wherein the tension comprises 20 megapascals.

19. A method of manufacturing ceramic tape, comprising:
directing a tape of partially-sintered ceramic into a furnace, wherein the tape is partially-sintered such that grains of the ceramic are fused to one another yet the tape still includes at least 10% porosity by volume, where the porosity refers to volume of the tape unoccupied by the ceramic, wherein the ceramic comprises alumina, zirconia, lithium garnet, and/or spinel;
conveying the tape through the furnace; and
further sintering the tape as the tape is conveyed through the furnace, wherein the porosity of the tape decreases during the further sintering, wherein length of the tape is at least 10 m, width of the tape is at least 10 mm, and thickness of the tape is at least 10 μm.

20. The method of claim 19 , wherein the width is no greater than 20 cm and the thickness is no greater than 500 μm.

Assignees

• Corning Inc

Inventors

• Badding Michael Edward
• Bouton William Joseph
• Brown Jacqueline Leslie
• Curry Timothy Joseph
• Hurny Roman E
• Kester Lanrik Wayne
• Ketcham Thomas Dale
• Olenick John Albert
• Olenick Kathleen Ritter
• Paananen Jeremy
• Silverblatt Thomas
• St Julien Dell Joseph
• Venkateswaran Viswanathan
• Zink Nathan Michael

Classifications

• C04B2235/9653

  Translucent or transparent ceramics other than alumina · CPC title

• C04B2235/963

  Surface properties, e.g. surface roughness · CPC title

• C04B2235/9615

  Linear firing shrinkage · CPC title

• C04B2235/6025

  Tape casting, e.g. with a doctor blade · CPC title

• C04B35/64 Primary

  Burning or sintering processes (C04B33/32 takes precedence {; powder metallurgy B22F}) · CPC title