Methods of forming dynamic cross-linked polymer compositions using functional chain extenders under batch process
US-2019270847-A1 · Sep 5, 2019 · US
US11618709B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11618709-B2 |
| Application number | US-202117376284-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jul 15, 2021 |
| Priority date | May 23, 2018 |
| Publication date | Apr 4, 2023 |
| Grant date | Apr 4, 2023 |
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A method of processing an optical fiber includes drawing the optical fiber from a heated glass source, reheating the optical fiber, and cooling the optical fiber under vacuum at a cooling rate less than the cooling rate of the optical fiber in air at 25° C. and 1 atm. Cooling the optical fiber under vacuum is conducted after reheating the optical fiber. Cooling the optical fiber under vacuum reduces the rate of heat transfer from the optical fiber, which may enable further relaxation of the glass and reduction in the fictive temperature of the optical fiber. A system for processing an optical fiber includes a furnace containing a fiber preform, a first positioner, a reheating device, and a treatment device downstream of the reheating device, the treatment device operable to cool the optical fiber under vacuum to reduce the rate of heat transfer from the optical fiber.
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What is claimed is: 1. A system for processing an optical fiber, the system comprising: a furnace having a fiber preform operable to produce an optical fiber; at least one positioner downstream of the furnace, the positioner operable to reduce variability in a process pathway of the optical fiber; a treatment device downstream of the positioner, the treatment device comprising a reheating zone and a treatment zone downstream of the reheating zone, the treatment device operable to maintain the reheating zone and the treatment zone at an operating pressure less than atmospheric pressure and to cool the optical fiber in the treatment zone under vacuum at a cooling rate less than a cooling rate of the optical fiber in air at 25° C. and 1 atm; and a reheating device coupled to or enclosed within the reheating zone of the treatment device. 2. The system of claim 1 , wherein the treatment device is operable to maintain the optical fiber at a pressure of from 0.005 atm to 0.8 atm in the treatment zone. 3. The system of claim 1 , wherein the treatment device comprises a chamber enclosing at least a portion of the process pathway of the optical fiber downstream of the reheating device. 4. The system of claim 3 , wherein the chamber has an inner diameter of from 4 cm to 40 cm. 5. The system of claim 1 , wherein the treatment device encloses the positioner upstream of the reheating device. 6. The system of claim 1 , wherein the treatment device comprises a heated internal surface in the treatment zone, wherein the heated internal surface is operable to reduce a temperature gradient between the optical fiber and the treatment device. 7. The system of claim 1 , further comprising a heated slow cooling device disposed between the furnace and the positioner.
Improving the yield, e-g- reduction of reject rates · CPC title
Annealing or re-heating · CPC title
Drawing at high speed, i.e. > 10 m/s · CPC title
to the outside of the preform or fibre · CPC title
for glass optical fibres · CPC title
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