Method for additive manufacturing with modified powder

Patent metadata

Field	Value
Publication number	US-11602791-B2
Application number	US-201816131700-A
Country	US
Kind code	B2
Filing date	Sep 14, 2018
Priority date	Sep 14, 2018
Publication date	Mar 14, 2023
Grant date	Mar 14, 2023

Abstract

A process for additive manufacturing of a metal alloy material is provided that includes: a) providing a feedstock powder comprising base powder particles with nanoparticles attached to surfaces of the base powder particles; b) providing an additive manufacturing system with a laser power source relatively movable at a scan speed; c) wherein the additive manufacturing system has a process window for the feedstock powder; and d) exposing the feedstock powder to a predetermined power input from the laser power source at a predetermined scan speed to produce the metal alloy material. The concentration by volume of nanoparticles within the feedstock powder is such that independent first and second microstructures may be produced within the metal alloy material.

First claim

What is claimed is:

1. A process for additive manufacturing of a metal alloy material, said process comprising:
providing a feedstock powder comprising base powder particles with nanoparticles attached to surfaces of the base powder particles, the feedstock powder having a concentration by volume of nanoparticles;
providing an additive manufacturing system with a laser power source movable at a scan speed relative to the metal alloy material;
wherein the additive manufacturing system has a process window for the feedstock powder, the process window defined by a maximum power input from the laser power source and a maximum scan speed;

exposing the feedstock powder to a first predetermined power input from the laser power source at a first predetermined scan speed to produce a first portion of the metal alloy material having a columnar microstructure; and
exposing the feedstock powder to a second predetermined power input from the laser power source at a second predetermined scan speed to produce a second portion of the metal alloy material having an equiaxed microstructure, one or both of the second predetermined power input and the second predetermined scan speed being different than the respective first predetermined power input and the first predetermined scan speed;
wherein each of the steps of exposing the feedstock powder to the first predetermined power input from the laser power source at the first predetermined scan speed and exposing the feedstock powder to the second predetermined power input from the laser power source at the second predetermined scan speed are performed a plurality of times collectively adding layers of the metal alloy material on top of one another to produce the metal alloy material; and
wherein at least one of the layers of the metal alloy material is part of the first portion of the metal alloy material having the columnar microstructure, and at least one of the layers of the metal alloy material is part of the second portion of the metal alloy material having the equiaxed microstructure.

2. The process of claim 1 , further comprising exposing the feedstock powder to a third predetermined power input from the laser power source at a third predetermined scan speed to produce a third portion of the metal alloy material having a third microstructure, different than the columnar microstructure or the equiaxed microstructure.

3. The process of claim 2 , wherein the third microstructure is a mixed equiaxed and columnar microstructure.

4. The process of claim 1 , wherein the feedstock powder has a first reflectivity value for a given wavelength of light produced by the laser power source, and the base powder particles have a second reflectivity value for the given wavelength of light produced by the laser power source, and the first reflectivity value is less than the second reflectivity value.

5. The process of claim 1 , wherein the metal alloy material is a nickel alloy material.

6. The process of claim 1 , wherein the metal alloy material is an aluminum alloy material.

7. The process of claim 1 , wherein the base powder particles comprise a first material type and the nanoparticles comprise a second material type, and the first material type is different from the second material type.

8. The process of claim 1 , wherein the second predetermined power input is greater than the first predetermined power input.

9. The method of claim 1 , wherein the base powder particles comprise an AA7075 aluminum alloy and the nanoparticles comprise zirconium oxide (ZrO 2 ).

10. The method of claim 9 , wherein the concentration by volume of nanoparticles is one percent.

11. The method of claim 1 , wherein the base powder particles comprise a nickel alloy and the nanoparticles comprise yttria.

12. The method of claim 11 , wherein the concentration by volume of nanoparticles is three percent.

13. A method of additively manufacturing a metal alloy material, comprising:
providing a feedstock powder having a base powder with a plurality of surface attached nanoparticles, wherein the base powder has a first reflectivity value at a given wavelength, and the nanoparticles have a second reflectivity value at the given wavelength, and wherein the feedstock powder has a third reflectivity value at the given wavelength, and the third reflectivity value is less than the first reflectivity value; and
producing a metal alloy material using an additive manufacturing process with the feedstock powder by exposing the feedstock powder to a predetermined power input from a laser power source movable at a predetermined scan speed relative to the metal alloy material, including:
exposing the feedstock powder to a first predetermined power input from the laser power source at a first predetermined scan speed to produce a first portion of the metal alloy material having a columnar microstructure; and
exposing the feedstock powder to a second predetermined power input from the laser power source at a second predetermined scan speed to produce a second portion of the metal alloy material having an equiaxed microstructure, one or both of the second predetermined power input and the second predetermined scan speed being different than the respective first predetermined power input and the first predetermined scan speed;

wherein each of the steps of exposing the feedstock powder to the first predetermined power input from the laser power source at the first predetermined scan speed and exposing the feedstock powder to the second predetermined power input from the laser power source at the second predetermined scan speed are performed a plurality of times collectively adding layers of the metal alloy material on top of one another to produce the metal alloy material; and
wherein at least one of the layers of the metal alloy material is part of the first portion of the metal alloy material having the columnar microstructure, and at least one of the layers of the metal alloy material is part of the second portion of the metal alloy material having the equiaxed microstructure.

14. The method of claim 13 , wherein the additive manufacturing process has a process window for the feedstock powder, the process window defined by a maximum power input from a laser power source and a maximum scan speed; and
wherein the first predetermined power input from the laser power source and the first predetermined scan speed are within the process window, and the second predetermined power input from the laser power source and the second predetermined scan speed are within the process window.

15. The method of claim 13 , further comprising exposing the feedstock powder to a third predetermined power input from the laser power source at a third predetermined scan speed to produce a third portion of the metal alloy material having a third microstructure, different than the columnar microstructure or the equiaxed microstructure.

16. The method of claim 13 , wherein the second predetermined power input is greater than the first predetermined power input.

17. A process for additive manufacturing of a metal alloy material, the process comprising:
providing an additive manufacturing system with a laser power source movable at a scan speed relative to the metal alloy material;
providing a feedstock powder comprising base powder particles having a first process window defined by a first effective power input range and a first scan speed range, the feedstock powder further comprising nanoparticles attached to surfaces of the base powder particles so that the feedstock powder has a second process window defined by a seco

Assignees

• United Technologies Corp
• Raytheon Tech Corp

Inventors

• Sharon John A
• Sheedy Paul
• Acharya Ranadip
• Jagdale Vijay Narayan

Classifications

• B23K26/0006 Primary

  taking account of the properties of the material involved (B23K26/32, B23K26/40 take precedence) · CPC title

• B33Y10/00 Primary

  Processes of additive manufacturing · CPC title

• B22F1/16

  Metallic particles coated with a non-metal (coated with lubricating or binding agents or with organic material B22F1/10) · CPC title

• B22F1/056

  Submicron particles having a size above 100 nm up to 300 nm · CPC title

• B22F10/28

  Powder bed fusion, e.g. selective laser melting [SLM] or electron beam melting [EBM] · CPC title