Guided wave-based system for cure monitoring of composites using piezoelectric discs and fiber Bragg gratings/phase-shifted Bragg gratings

Patent metadata

Field	Value
Publication number	US-11590676-B2
Application number	US-201816109313-A
Country	US
Kind code	B2
Filing date	Aug 22, 2018
Priority date	Aug 21, 2018
Publication date	Feb 28, 2023
Grant date	Feb 28, 2023

Abstract

System and method for in-process cure monitoring of a material utilizes one or more sensors such as fiber Bragg gratings (FBGs) or phase-shifted FBGs (PS-FBGs) and at least one optical line fiber connected to the sensor(s). The sensor(s) and the optical line may be embedded in the material prior to curing the material may comprise a fiber reinforced polymer. Waves are excited into the material during curing thereof to form guided waves that propagate through the material. At least one wave metric of the guided waves is measured utilizing the sensor(s).

First claim

The invention claimed is:

1. A method of in-process cure monitoring of a material, the method comprising;
embedding at least one sensor selected from the group consisting of fiber Bragg gratings (FBGS) and phase-shifted FBGS (PS-FBGS) at a first location, and at least one optical line that is operatively connected to the sensor, into the material to be cured;
exciting waves into the material during curing of the material at a second location that is spaced apart from the first location to form guided waves that propagate through the material from the second location to the first location;
causing light to propagate through the optical line to the sensor; and
measuring at least one wave metric of the guided waves at the first location by utilizing the sensor receiving the propagated light, including measuring a wavelength spectrum oscillation to determine local strain resulting from the guided waves at the first location induced by the guided waves propagating through the material; and
measuring chemical cure shrinkage strain by utilizing the sensor, wherein the chemical cure shrinkage strain is induced by curing of the material.

2. The method of claim 1 , wherein the at least one sensor comprises a plurality of sensors.

3. The method of claim 1 , further comprising utilizing the at least one measured wave metric to determine information for at least one of
a phase transition of the material; and
a material property of the material.

4. The method of claim 1 , wherein
measuring the at least one wave metric includes measuring at least one of
a time of arrival of the guided waves at the second location; and
an amplitude of the guided waves at the second location.

5. The method of claim 1 , further comprising
measuring at least one wave metric of the material at a third location that is spaced apart from the first location and the second location;
determining a group velocity for guided waves between the second and third locations;
utilizing the group velocity to determine a mechanical property of the material.

6. The method of claim 1 , wherein
exciting at least one wave into the material during curing of the material comprises
exciting guided waves having at least first and second center frequencies, and wherein
the first center frequency is not equal to the second center frequency.

7. The method of claim 1 , wherein
the material comprises a thermosetting polymer; and
the curing process comprises heating or cooling the thermosetting polymer material to a prescribed temperature.

8. The method of claim 1 , further comprising
adjusting at least one parameter of the curing process based, at least in part, on a wave metric measured at the second location.

9. The method of claim 3 , wherein
the material property comprises at least one of viscosity, degree of cure, cure rate, and mechanical properties.

10. The method of claim 1 , wherein
the measured wave metric comprises a measured wave amplitude at the second location.

11. The method of claim 1 , further comprising
comparing a measured wave amplitude to an expected wave amplitude;
adjusting at least one process parameter of the curing process based on differences between the measured wave amplitude and the expected wave amplitude.

12. The method of claim 11 , wherein
the at least one process parameter of the curing process is selected from the group consisting of a temperature, pressure, and time at an elevated temperature.

13. The method of claim 1 ,
wherein the wave metric comprises time of arrival at the second location; and further comprising
comparing the measured time of arrival to an expected time of arrival to determine a difference;
adjusting at least one curing process parameter based, at least in part on the difference.

14. The method of claim 1 , further comprising
utilizing empirical data to determine a correlation between the measured wave metric and a cure state of the material.

15. The method of claim 1 ,
wherein the material comprises a multi-layer sheet of fiber reinforced polymer matrix material having opposite first and second side surfaces forming acoustic boundaries; and
further comprising
positioning the fiber reinforced polymer matrix material on a support surface with the second side surface facing the support surface;
positioning an actuator on the first or second side of the fiber reinforced polymer matrix at the first location;
embedding the optical line and a plurality of the sensors in the fiber reinforced polymer matrix material prior to curing the fiber reinforced polymer matrix material.

16. A method of in-process cure monitoring of a material, the method comprising
operatively connecting at least one optical sensor to a fiber reinforced composite material at a first location, wherein the optical sensor is a phase-shifted fiber Bragg grating that reflects predefined wavelengths of light and transmits all other wavelengths of light;
operatively connecting at least one optical line to the optical sensor;
exciting waves into the fiber reinforced composite material during curing of the composite material at a second location that is spaced apart from the first location to form guided waves that propagate through the composite material from the second location to the first location;
causing light to propagate through the optical line to the sensor; and
measuring at least one wave metric of the guided waves at the first location utilizing the optical sensor receiving the propagated light, including measuring a wavelength spectrum oscillation to determine local strain resulting from the guided waves at the first location line induced by the guided waves propagating through the material; and
measuring chemical cure shrinkage strain by utilizing the sensor, wherein the chemical cure shrinkage strain is induced by curing of the material.

17. The method of claim 16 , wherein
the at least one optical sensor is configured to reflect and/or filter light having predefined wavelengths.

18. The method of claim 16 , further comprising
utilizing the measured wave matric to determine information concerning at least one of
a phase transition of the fiber reinforced composite material; and
a material property of the fiber reinforced composite material.

19. The method of claim 16 , wherein
measuring at least one wave metric includes measuring at least one of
a time of arrival of the guided waves at the second location; and
an amplitude of the guided waves at the second location.

20. The method of claim 16 , wherein
the optical sensor is bonded to a surface of the fiber reinforced composite material prior to curing.

Assignees

• Nasa

Inventors

• Hudson Tyler B
• Yuan Fuh-Gwo
• Auwaijan Nicolas
• Palmieri Frank L

Classifications

• B29K2105/0881

  unidirectional · CPC title

• B29C35/0288 Primary

  Controlling heating or curing of polymers during moulding, e.g. by measuring temperatures or properties of the polymer and regulating the process (controlling or regulating chemical, physical or physico- chemical processes in general B01J19/0006) · CPC title

• B29K2101/10

  Thermosetting resins · CPC title

• B29K2307/04

  Carbon · CPC title

• G01D5/35316

  using a Bragg gratings · CPC title