Temperature-controlled centrifuge with protective gas release in case of rotor crash

Patent metadata

Field	Value
Publication number	US-11577257-B2
Application number	US-201816955310-A
Country	US
Kind code	B2
Filing date	Dec 3, 2018
Priority date	Dec 20, 2017
Publication date	Feb 14, 2023
Grant date	Feb 14, 2023

Abstract

A centrifuge (10) and a method for preventing the ignition of combustible temperature control media in centrifuges (10) after a crash of the centrifuge rotor are presented. Ignition is prevented by the release of a protective gas in the event of a crash. More precisely, the released protective gas forms a flow that displaces the oxygen, distributes the escaping temperature control medium and fundamentally changes the momentary ratio of the concentration of oxygen to temperature control medium in such a manner that no ignition can take place either inside or outside the centrifuge (10). Thereby, combustible temperature control media can be used without safety concerns for controlling the temperature of centrifuges (10).

First claim

The invention claimed is:

1. A centrifuge ( 10 ), comprising:
a centrifuge container ( 16 ) in which a centrifuge rotor ( 20 , 20 ′) can be accommodated;
a motor ( 18 ) for driving the centrifuge rotor ( 20 , 20 ′);
temperature control means ( 24 , 42 , 44 ) for controlling the temperature of the centrifuge rotor ( 20 , 20 ′); and
a housing ( 12 ) in which the centrifuge container ( 16 ), the centrifuge rotor ( 20 , 20 ′), the temperature control means ( 24 , 42 , 44 ) and the motor ( 18 ) are accommodated,
wherein the temperature control means ( 24 , 42 , 44 ) comprise a combustible temperature control medium that is guided in a temperature control medium line ( 24 ), and
wherein the centrifuge ( 10 ) comprises a protective gas and is adapted to release the protective gas in the event of a crash of the centrifuge rotor ( 20 , 20 ′), and
wherein the protective gas is guided in a protective gas line ( 26 ), which extends around the centrifuge container ( 16 ) with one or several windings ( 36 ), and
wherein the protective gas line ( 26 ) and the temperature control medium line ( 24 ) are connected to one another at least in some areas.

2. The centrifuge ( 10 ) according to claim 1 ,
wherein the protective gas is an inert gas.

3. The centrifuge ( 10 ) according to claim 1 ,
wherein the protective gas is at least one gas selected from the group consisting of argon, helium, carbon dioxide, krypton, neon, nitrogen and xenon.

4. The centrifuge ( 10 ) according to claim 1 ,
wherein the protective gas line ( 26 ) is connected to a protective gas source ( 34 ).

5. The centrifuge ( 10 ) according to claim 4 ,
wherein the protective gas source ( 34 ) contains the protective gas under a pressure above atmospheric pressure.

6. The centrifuge ( 10 ) according to claim 4 ,
further comprising a throttle element arranged between the protective gas line ( 26 ) and the protective gas source ( 34 ).

7. The centrifuge ( 10 ) according to claim 4 ,
wherein at least two sections ( 28 , 30 ) of the protective line ( 26 ) are connected in parallel with the protective gas source ( 34 ).

8. The centrifuge ( 10 ) according to claim 1 ,
wherein the protective gas line ( 26 ) is arranged at least in areas ( 36 ) with respect to the centrifuge container ( 16 ) next to and/or below the temperature control medium line ( 50 ).

9. The centrifuge ( 10 ) according to claim 1 ,
wherein the protective gas line ( 26 ) and the temperature control medium line ( 24 ) are soldered to one another at least over a quarter of their respective winding lengths.

10. The centrifuge ( 10 ) according to claim 1 ,
wherein the protective gas line ( 26 ) has, at least in some areas, a smaller wall thickness than the temperature control medium line ( 24 ).

11. The centrifuge ( 10 ) according to claim 1 ,
wherein the protective gas line ( 26 ) and/or the temperature control medium line ( 24 ) are arranged directly on the centrifuge container ( 16 ) or at least in some areas are at least a component of a wall of the centrifuge container ( 16 ).

12. The centrifuge according to claim 1 , wherein a multi-channel system exists to an effect that there is at least one separate said winding for the protective gas and at least one separate winding for the combustible temperature control medium.

13. The centrifuge ( 10 ) according to claim 1 , further comprising monitoring means ( 38 ) with regard to a condition of the protective gas which are adapted to limit a rotational speed of the centrifuge rotor ( 20 , 20 ′) to a value that is not critical for a crash of the centrifuge rotor ( 20 , 20 ′) if predetermined values far the condition of the protective gas are not reached.

14. The centrifuge ( 10 ) according to claim 13 ,
wherein the monitoring means ( 38 ) measure a pressure and/or a quantity of protective gas.

15. The centrifuge ( 10 ) according to claim 1 ,
further comprising a fan that, during operation of the centrifuge ( 10 ), continuously guides air from an interior of the housing into an environment of the centrifuge ( 10 ).

16. A method for preventing ignition of combustible tempering media in centrifuges ( 10 ) after a crash of a centrifuge rotor ( 20 , 20 ′),
wherein the centrifuge ( 10 ) comprises
a centrifuge container ( 16 ), in which a centrifuge rotor ( 20 , 20 ′) can be accommodated,
a motor ( 18 ) for driving the centrifuge rotor ( 20 , 20 ′),
temperature control means ( 24 , 42 , 44 ) for controlling the temperature of the centrifuge rotor ( 20 , 20 ′),
a protective gas line ( 26 ) which extends around the centrifuge container ( 16 ) with one or several windings ( 36 ), and
a housing ( 12 ) in which the centrifuge container ( 16 ), the centrifuge rotor ( 20 , 20 ′), the temperature control means ( 24 , 42 , 44 ) and the motor ( 18 ) are accommodated, and

wherein the temperature control means ( 24 , 42 , 44 ) comprises a combustible temperature control medium that is guided in a temperature control medium line ( 24 ), the method comprising:
causing fragments of the centrifuge rotor to destroy the protective gas line ( 26 ) and thereby release a protective gas guided therein into the centrifuge in the event of a crash of the centrifuge rotor ( 20 , 20 ′) before the fragments can destroy the temperature control medium line ( 24 ).

17. A centrifuge ( 10 ), comprising:
a centrifuge container ( 16 ) in which a centrifuge rotor ( 20 , 20 ′) can be accommodated;
a motor ( 18 ) for driving the centrifuge rotor ( 20 , 20 ′);
temperature control means ( 24 , 42 , 44 ) for controlling the temperature of the centrifuge rotor ( 20 , 20 ′); and
a housing ( 12 ) in which the centrifuge container ( 16 ), the centrifuge rotor ( 20 , 20 ′), the temperature control means ( 24 , 42 , 44 ) and the motor ( 18 ) are accommodated,
wherein the temperature control means ( 24 , 42 , 44 ) comprise a combustible temperature control medium that is guided in a temperature control medium line ( 24 ), and
wherein the centrifuge ( 10 ) comprises a protective gas and is adapted to release the protective gas in the event of a crash of the centrifuge rotor ( 20 , 20 ′), and
wherein the protective gas is guided in a protective gas line ( 26 ), which extends around the centrifuge container ( 16 ) with one or several windings ( 36 ), and
wherein the protective gas line ( 26 ) is arranged such that, in case of a crash, fragments of the rotor break the protective gas line ( 26 ), thereby causing the release of the protective gas into the centrifuge, before the fragments can break the temperature control medium line ( 24 ).

Assignees

• Eppendorf Ag

Inventors

• Müller Heiko

Classifications

• B04B15/02 Primary

  for cooling, heating, or heat insulating · CPC title

• B04B2007/065

  Devices and measures in the event of rotor fracturing, e.g. lines of weakness, stress regions · CPC title

• B04B7/06 Primary

  Safety devices {; Regulating} · CPC title