Removable impingement basket for ethylene oxide (EO) reactors

Patent metadata

Field	Value
Publication number	US-11559799-B2
Application number	US-202017130961-A
Country	US
Kind code	B2
Filing date	Dec 22, 2020
Priority date	Dec 22, 2020
Publication date	Jan 24, 2023
Grant date	Jan 24, 2023

Abstract

An ethylene oxide (EO) reactor is provided in which a removable impingement basket is configured to be inserted into the reactor inlet pipe of the EO reactor. The removable impingement basket provides protection for the silver-based catalyst filled tubes and other components that are present inside the EO reactor as well as providing another access point into the EO reactor. The removable impingement basket also can provide better distribution of the inlet gas as compared to an EO reactor containing a non-removable impingement plate.

First claim

What is claimed is:

1. An ethylene oxide (EO) reactor comprising:
a removable impingement basket located at an upper portion of the EO reactor and affixed to inlet pipe flanges of an inlet pipe of the EO reactor, wherein the removable impingement basket comprises a non-perforated hollowed-wall section having an upper end and a lower end, a mounting flange located adjacent to the upper end of the non-perforated hollowed-wall section, and a perforated hollowed-wall section located at the lower end of the non-perforated hollowed-wall section, wherein the perforated hollowed-wall section contains a plurality of through-holes configured to permit inlet gas to flow from the inlet pipe into the upper portion of the EO reactor, and the mounting flange comprises a plurality of lifting fingers extending upward from a surface thereof.

2. The EO reactor of claim 1 , wherein the non-perforated hollowed-wall section, the perforated hollowed-wall section, and the mounting flange are cylindrical.

3. The EO reactor of claim 2 , wherein the perforated hollowed-wall section comprises a cylindrical outer wall and a convex bottom wall.

4. The EO reactor of claim 1 , wherein at least the non-perforated hollowed-wall section and the perforated hollowed-wall section are of integral construction.

5. The EO reactor of claim 1 , wherein the mounting flange has a surface that is flush with a topmost surface of the upper end of the non-perforated hollowed-wall section.

6. The EO reactor of claim 1 , wherein the mounting flange has a surface that is located beneath a topmost surface of the upper end of the non-perforated hollowed-wall section.

7. The EO reactor of claim 1 , wherein the inlet pipe flanges comprise a plurality of top inlet pipe flanges and bottom inlet pipe flanges affixed to an outer wall of the inlet pipe of the EO reactor, wherein each top inlet pipe flange is paired with one of the bottom inlet pipe flanges to provide a paired inlet pipe flange set.

8. The EO reactor of claim 7 , wherein the mounting flange is sandwiched between the top inlet pipe flanges and the bottom inlet pipe flanges.

9. The EO reactor of claim 8 , wherein the mounting flange has a surface containing a plurality of through holes, wherein each through-hole present in the surface of the mounting flange is configured to align with through-holes present in each paired inlet pipe flange set.

10. The EO reactor of claim 9 , wherein a single stud bolt is positioned in each of the through-holes present in the surface of the mounting flange and each through-holes present in each paired inlet pipe flange set.

11. The EO reactor of claim 1 , wherein the inlet pipe flanges comprise a plurality of bottom inlet pipe flanges affixed to an outer wall of the inlet pipe of the EO reactor.

12. The EO reactor of claim 11 , wherein the mounting flange has a surface containing a plurality of through holes, wherein the surface of the mounting flange containing the plurality of through-holes is seated atop each of the bottom inlet pipe flanges and wherein each through-hole present in the surface of the mounting flange is configured to align with through-holes present in each of the bottom inlet pipe flanges.

13. The EO reactor of claim 12 , wherein a single stud bolt is positioned in each of the through-holes present in the surface of the mounting flange and each through-holes present in each of the bottom inlet pipe flanges.

14. The EO reactor of claim 1 , wherein the EO reactor is a shell-and-tube heat exchange reactor.

15. The EO reactor of claim 1 , further comprising a plurality of elongated tubes located in the EO reactor and positioned beneath the removable impingement basket.

16. The EO reactor of claim 15 , wherein each elongated tube is filled with a silver-based epoxidation catalyst comprising an alumina support and at least a catalytically effective amount of silver or a silver-containing compound.

17. The EO reactor of claim 16 , wherein the silver-based epoxidation catalyst comprises an alumina support and at least a catalytically effective amount of silver or a silver-containing compound.

18. An ethylene oxide (EO) reactor comprising:
a removable impingement basket located at an upper portion of the EO reactor and affixed to inlet pipe flanges of an inlet pipe of the EO reactor, wherein the removable impingement basket comprises a non-perforated hollowed-wall section having an upper end and a lower end, a mounting flange located adjacent to the upper end of the non-perforated hollowed-wall section, and a perforated hollowed-wall section located at the lower end of the non-perforated hollowed-wall section, wherein the perforated hollowed-wall section contains a plurality of through-holes configured to permit inlet gas to flow from the inlet pipe into the upper portion of the EO reactor, and wherein the mounting flange has a surface that is located beneath a topmost surface of the upper end of the non-perforated hollowed-wall section.

19. An ethylene oxide (EO) reactor comprising:
a removable impingement basket located at an upper portion of the EO reactor and affixed to inlet pipe flanges of an inlet pipe of the EO reactor, wherein the removable impingement basket comprises a non-perforated hollowed-wall section having an upper end and a lower end, a mounting flange located adjacent to the upper end of the non-perforated hollowed-wall section, and a perforated hollowed-wall section located at the lower end of the non-perforated hollowed-wall section, wherein the perforated hollowed-wall section contains a plurality of through-holes configured to permit inlet gas to flow from the inlet pipe into the upper portion of the EO reactor, the inlet pipe flanges comprise a plurality of top inlet pipe flanges and bottom inlet pipe flanges affixed to an outer wall of the inlet pipe of the EO reactor, each top inlet pipe flange is paired with one of the bottom inlet pipe flanges to provide a paired inlet pipe flange set, the mounting flange is sandwiched between the top inlet pipe flanges and the bottom inlet pipe flanges, and the mounting flange has a surface containing a plurality of through holes, and wherein each through-hole present in the surface of the mounting flange is configured to align with through-holes present in each paired inlet pipe flange set.

20. An ethylene oxide (EO) reactor comprising:
a removable impingement basket located at an upper portion of the EO reactor and affixed to inlet pipe flanges of an inlet pipe of the EO reactor, wherein the removable impingement basket comprises a non-perforated hollowed-wall section having an upper end and a lower end, a mounting flange located adjacent to the upper end of the non-perforated hollowed-wall section, and a perforated hollowed-wall section located at the lower end of the non-perforated hollowed-wall section, wherein the perforated hollowed-wall section contains a plurality of through-holes configured to permit inlet gas to flow from the inlet pipe into the upper portion of the EO reactor, the inlet pipe flanges comprise a plurality of bottom inlet pipe flanges affixed to an outer wall of the inlet pipe of the EO reactor, and the mounting flange has a surface containing a plurality of through holes, and wherein the surface of the mounting flange containing the plurality of through-holes is seated atop each of the bottom inlet pipe flanges and wherein each through-hole present in the surface of the mounting flange is configured to align with through-holes present in each of the bottom inlet pipe flanges.

Assignees

• Scient Design Co

Inventors

• Ganjvar Mohammad

Classifications

• B01J23/50

  Silver · CPC title

• B01J2204/00

  Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices · CPC title

• B01J37/0201 Primary

  Impregnation · CPC title

• B01J37/08

  Heat treatment {(B01J37/0009, B01J37/0018 take precedence)} · CPC title

• B01J2208/00938

  Flow distribution elements · CPC title