Method for producing a fibrous material

Patent metadata

Field	Value
Publication number	US-11535983-B2
Application number	US-201716307823-A
Country	US
Kind code	B2
Filing date	May 18, 2017
Priority date	Jun 17, 2016
Publication date	Dec 27, 2022
Grant date	Dec 27, 2022

Abstract

A method for producing a fibrous material from lignocellulose from wood, preferably in the form of wood chips. The lignocellulose material is impregnated with a mixture of sodium sulfite and sodium bisulfite and subsequently undergoes a comminution process in a refiner. Additional chemicals from a mixture of sodium sulfite and sodium bisulfite are directly introduced into the refiner, allowing optimal conditions to be set for both additive flows of chemicals such that the process can be operated in an energetically advantageous manner and corrosion and scale formation in the refiner and subsequent aggregates can be prevented as much as possible.

First claim

The invention claimed is:

1. A method for producing pulp from a lignocellulose material made from wood in a manner that avoids or reduces corrosion and coating in a refiner, where the lignocellulose material is impregnated with chemicals from a mixture of sodium sulfite and sodium bisulfite in a reactor and subsequently grinded in the refiner, comprising:
feeding chemicals to the reactor during impregnation of the lignocellulose material; and
feeding chemicals directly to the refiner, wherein
the chemicals comprise a mixture of sodium sulfite and sodium bisulfite,
the chemicals fed to the reactor during impregnation have a pH within a range of 6.0-7.5, and
the chemicals fed to the refiner have a pH within a range of 4.0-5.5 and that is sufficient to avoid or reduce corrosion and coating in the refiner.

2. The method according to claim 1 , wherein the chemicals fed to the refiner have a pH within the range of 4.2-4.5.

3. The method according to claim 2 , wherein chemicals fed to the reactor during impregnation have a pH within the range of 6.5-7.0.

4. The method according to claim 1 , wherein chemicals fed to the reactor during impregnation have a pH within the range of 6.5-7.0.

5. The method according to claim 1 , wherein the lignocellulose material is in the form of wood chips.

6. The method according to claim 1 , wherein the chemicals fed to the reactor during impregnation and the chemicals fed to the refiner combine to 100%, characterized in that 60-80% of said 100% are added to the reactor during impregnation.

7. The method according to claim 6 , characterized in that impregnation takes place at a temperature within a range of 80-170° C.

8. The method according to claim 7 , characterized in that impregnation takes place at a temperature within the range of 120-140° C.

9. The method according to claim 1 , characterized in that impregnation takes place at a temperature within a range of 80-170° C.

10. The method according to claim 9 , characterized in that impregnation takes place at a temperature within a range of 120-140° C.

11. The method according to claim 1 , characterized in that the total quantity of chemicals added amounts to 1-20 kg of chemicals per ton of wood.

12. The method according to claim 1 , characterized in that the total quantity of chemicals added amounts to 10-15 kg of chemicals per ton of wood.

13. A method of producing pulp from a lignocellulose material made from wood, where the lignocellulose material is impregnated with chemicals from a mixture of sodium sulfite and sodium bisulfite in a reactor and subsequently grinded in a refiner, comprising:
feeding a wood material to a reactor for impregnation and adding chemicals comprising sodium sulfite and sodium bisulfite having a pH adjusted to reduce or prevent corrosion and coating in the refiner and within a range of 6.0-7.5 to the reactor during impregnation to yield impregnated wood material;
transferring the impregnated wood material from the reactor to a refiner and adding chemicals comprising sodium sulfite and sodium bisulfite having a pH adjusted to reduce or prevent corrosion and coating in the refiner and within a range of 4.0-5.5 directly to the refiner, wherein
impregnation in the reactor occurs at a temperature within a range of 80-170° C.

14. The method according to claim 13 , wherein the chemicals fed to the refiner have a pH within the range of 4.2-4.5.

15. The method according to claim 13 , wherein chemicals fed to the reactor during impregnation have a pH within the range of 6.5-7.0.

16. A method of producing pulp from a lignocellulose material made from wood in a manner that avoids or prevents corrosion and coating in refiner plates of a refiner, where the lignocellulose material is impregnated with chemicals from a mixture of sodium sulfite and sodium bisulfite in a reactor and subsequently grinded in a refiner, comprising:
providing chemicals comprising a mixture of sodium sulfite and sodium bisulfite;
feeding a wood material to a reactor for impregnation and adding 60-80% of the chemicals at a pH within a range of 6.0-7.5 to the reactor during impregnation to yield impregnated wood material; and
transferring the impregnated wood material from the reactor to the refiner and adding the rest of the chemicals at a pH within a range of 4.0-5.5 directly to the refiner at a grinding zone,
wherein the impregnation in the reactor occurs at a temperature within a range of 80-170° C.,
wherein the chemicals added during impregnation amount to 60-80% of the chemicals used in the reactor and the refiner, and
wherein the chemicals added to the refiner amount to 20-40% of the chemicals used in the reactor and the refiner.

17. The method according to claim 16 , wherein the chemicals fed to the refiner have a pH within the range of 4.2-4.5.

18. The method according to claim 16 , wherein chemicals fed to the reactor during impregnation have a pH within the range of 6.5-7.0.

19. The method according to claim 1 , wherein the ranges of pH are sufficient to prevent or avoid deposits and coating of calcium sulfite on refiner plates of the refiner and any gaseous sulfer dioxide formed in a refiner zone of the refiner is condensed with steam.

20. The method according to claim 13 , wherein the ranges of pH are sufficient to prevent or avoid deposits and coating of calcium sulfite on refiner plates of the refiner and any gaseous sulfer dioxide formed in a refiner zone of the refiner is condensed with steam.

Assignees

• Andritz Ag Maschf

Inventors

• Shagaev Oleg

Classifications

• D21D1/20

  Methods of refining · CPC title

• D21C3/04

  with acids, acid salts or acid anhydrides {(D21C3/003 and D21C3/222 take precedence)} · CPC title

• D21B1/14

  Disintegrating in mills · CPC title

• D21B1/021 Primary

  by chemical means · CPC title

• D21C3/12 Primary

  sodium bisulfite · CPC title