Process for producing needle-punched nonwoven fabric
US-11186931-B2 · Nov 30, 2021 · US
US11525220B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11525220-B2 |
| Application number | US-201816605385-A |
| Country | US |
| Kind code | B2 |
| Filing date | Apr 18, 2018 |
| Priority date | Apr 19, 2017 |
| Publication date | Dec 13, 2022 |
| Grant date | Dec 13, 2022 |
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An object of the present invention is to provide a process for producing fiberous board with which fiberous board exhibiting high bending strength and high stiffness at a wide range of heating temperatures and a wide range of compressing and heating times. In the present invention, fiberous board having an initial flexural modulus of at least 300 MPa in three point bending test is obtained by forming a web by correcting sheath-core composite fibers of which a core component is formed from a copolymer of ethylene glycol and terephthalic acid and the sheath component is formed from ethylene glycol, adipic acid, terephthalic acid, isophthalic acid; and/or diethylene glycol. The web is then compressed in a direction of thickness and heated, so that the sheath component softens and melts and the sheath-core composite fibers are melt bonded together and molded into a flat plate shape.
Opening claim text (preview).
The invention claimed is: 1. A process for producing a fibrous board having an initial flexural modulus of not less than 300 MPa in a three point bending test, comprising: collecting sheath-core composite fibers, of which the core component is formed from a copolymer of ethylene glycol and terephthalic acid, and the sheath component is formed from ethylene glycol, adipic acid, terephthalic acid and isophthalic acid; and optionally diethylene glycol, to form a web, and then compressing the web in a direction of thickness direction and heating to soften or melt the sheath components so as to bond the sheath-core composite fibers with each other, wherein the web is shaped into a plate to form a fibrous board, and a molar ratio of isophthalic acid:adipic acid:terephthalic acid in the sheath component is within the range of 0.004 to 0.6:1:1 to 10. 2. The process of claim 1 , wherein the web is preliminarily heated and sandwiched by a pair of metal plates having normal temperature and then compressed in the direction of thickness. 3. The process of claim 1 , wherein the web having normal temperature is sandwiched by a pair of heated metal plates, and then compressed in the direction of thickness. 4. The process according to claim 1 , wherein the web is needle punched to have the sheath-core composite fibers three dimensionally interlaced prior to the compressing and heating. 5. The process according to claim 1 , wherein the fibrous board has a maximum bending strength of not less than 7.3 MPa in a three point bending test. 6. The process according to claim 1 , wherein the sheath-core composite fiber is sheath-core composite continuous filament or sheath-core composite staple fiber. 7. The process according to claim 1 , wherein the web is shaped into a plate to form a fibrous board by cooling after the compressing and heating. 8. The process according to claim 1 , wherein a weight ratio of core to sheath is 0.3-5:1. 9. The process according to claim 1 , wherein the collected web exhibits a mass of at least 150 g/m 2 . 10. The process according to claim 1 , wherein the compressing is carried out with a surface pressure of 1-500 kg/cm 2 and the heating is carried out at a temperature of 100-200° C. 11. The process according to claim 1 , wherein the collected fibers consist of said sheath-core composite fibers, of which the core component is formed from a copolymer of ethylene glycol and terephthalic acid, and the sheath component is formed from ethylene glycol, adipic acid, terephthalic acid and isophthalic acid; and optionally diethylene glycol.
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