High-temperature high-entropy alloy with light weight and high strength in as-cast state and preparation method thereof
US-2024410035-A1 · Dec 12, 2024 · US
US11512369B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11512369-B2 |
| Application number | US-201917255277-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jun 24, 2019 |
| Priority date | Jun 26, 2018 |
| Publication date | Nov 29, 2022 |
| Grant date | Nov 29, 2022 |
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A method for manufacturing an ingot made of titanium-based metallic compound, includes providing raw material fragments; melting the raw material fragments into a liquid metal in at least one basin; keeping in the molten state the liquid metal in the at least one basin; pouring the liquid metal from the at least one basin into a crucible by overflow from the at least one basin into the crucible; forming an ingot by cooling of the liquid metal into the crucible; wherein the method further includes preheating the raw material fragments before the melting of the raw material fragments with a preheating temperature higher than or equal to 75% of the liquidus temperature of the raw material fragments, and lower less than the liquidus temperature of the raw material fragments.
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The invention claimed is: 1. A method for manufacturing an ingot ( 2 ) made of titanium-based metallic compound comprising: providing raw material fragments; melting the raw material fragments into a liquid metal in at least one basin; keeping in the molten state the liquid metal in said at least one basin; pouring the liquid metal from the at least one basin into a crucible by overflow from said at least one basin into said crucible; forming an ingot by cooling of the liquid metal into the crucible; wherein the method further comprises: preheating the raw material fragments before the melting of said raw material fragments with a preheating temperature higher than or equal to 75% of the liquidus temperature of said raw material fragments and strictly lower than the liquidus temperature of said raw material fragments. 2. The method according to claim 1 , wherein the preheating temperature is higher than or equal to the solidus temperature of the raw material fragments. 3. The method according to claim 2 , wherein the preheating temperature is higher than or equal to 93% of the liquidus temperature. 4. The method according to any claim 1 , wherein the titanium-based metallic compound comprises at least one element having a melting temperature higher than the melting temperature of the titanium. 5. The method according to any claim 1 , wherein the preheating of the raw material fragments ( 3 ) is carried out by induction. 6. The method according to any one of claim 1 , wherein the preheating of the raw material fragments is carried out by a generator of a heating beam. 7. The method according to claim 6 , wherein said method further comprises controlling the orientation of the generator of the heating beam. 8. The method according to claim l, wherein the method further comprises: melting the raw material fragments into a liquid metal in a first basin; keeping in the molten state the liquid metal in the first basin; pouring the liquid metal from the first basin in a second basin by overflow from said first basin in said second basin; keeping in the molten state the liquid metal in the second basin; pouring the liquid metal from the second basin into the crucible by overflow from said second basin into said crucible. 9. A system ( 1 ) for manufacturing an ingot made of titanium-based metallic compound comprising: at least one basin which is configured to receive the liquid metal; a conveyor which is configured to convey raw material fragments to said at least one basin; a crucible which is fed by overflow from said at least one basin and which is configured to cool and solidify the liquid metal; a heating system located opposite the at least one basin and the crucible and configured to melt and keep in the molten state raw material fragments in said at least one basin and in said crucible; wherein the system comprises a preheating device which is configured to heat on the conveyor said raw material fragments with a preheating temperature higher than or equal to 75% of the liquidus temperature of said raw material fragments and strictly lower than the liquidus temperature of said raw material fragments. 10. The system according to claim 9 , wherein the preheating device comprises a generator of a heating beam. 11. The system according to claim 9 , wherein the preheating device comprises an induction-preheating device.
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