Method and apparatus for producing a glass component

Patent metadata

Field	Value
Publication number	US-11512017-B2
Application number	US-202016804760-A
Country	US
Kind code	B2
Filing date	Feb 28, 2020
Priority date	Mar 1, 2019
Publication date	Nov 29, 2022
Grant date	Nov 29, 2022

Abstract

In known methods for producing a glass component, a void-containing intermediate product containing doped or non-doped SiO2 is inserted into a sheath tube composed of glass, which has a longitudinal axis and an inner bore, and is thermally treated therein. In order to subject the intermediate product to a thermal and/or reactive treatment that is reproducible and uniform in its effect from this starting point, it is proposed in one embodiment that into the sheath tube's inner bore a first gas-permeable gas diffuser is inserted which is displaceable along the sheath tube's longitudinal axis and is pressed against the intermediate product during the thermal treatment.

First claim

The invention claimed is:

1. A method of producing a glass component, comprising:
preparing a void-containing intermediate product that contains doped or non-doped SiO 2 ;
introducing the intermediate product into a sheath tube composed of glass, which has a longitudinal axis and an inner bore; and
thermal treating the intermediate product in the sheath tube,
wherein a first gas-permeable gas diffuser is inserted into the sheath tube's inner bore, which first gas-permeable gas diffuser is displaceable along the sheath tube's longitudinal axis and is pressed against the intermediate product during the thermal treatment,
wherein a compression force is generated by means of a clamping device, which exerts a pressure on the first gas diffuser, and
wherein the clamping device comprises an elastically deformable spring element inserted in the sheath tube's inner bore, or a slide which is displaceable in the sheath tube's inner bore and having a first magnetic element composed of a magnetic material and a second magnetic element which is movable in the direction of the longitudinal axis outside the sheath tube's inner bore and which acts on the magnetic element.

2. The method according to claim 1 , wherein the first gas diffuser consists of a porous glass, which has a higher viscosity compared to the doped or non-doped SiO 2 .

3. The method according to claim 1 , wherein the intermediate product is heated in an electrically heated annular furnace for the thermal treatment.

4. The method according to claim 1 , wherein the intermediate product is in the form of a soot body, sintered body or compact and has an external cross-sectional shape that fills an inner cross-sectional shape of the sheath tube leaving a gap with a gap width of no more than 1 mm.

5. The method according to claim 1 , wherein at one end of the sheath tube a vacuum is applied in the sheath tube's inner bore and/or at an opposite end of the sheath tube a treatment gas is fed into the sheath tube.

6. The method according to claim 1 , wherein the elastically deformable spring element inserted in the sheath tube's inner bore is a bellows.

7. The method according to claim 1 , wherein the intermediate product is arranged between the first gas diffuser and a second gas-permeable gas diffuser.

8. The method according to claim 7 , wherein the first gas diffuser and the second gas diffuser are configured in a cylindrical shape and each of the first and second gas diffusers have a flat end face adjacent to the intermediate product.

9. The method according to claim 1 , wherein into the sheath tube's inner bore a first fixing element is inserted, in or on which at least one through-going gas channel is formed and which is displaced along the sheath tube's longitudinal axis and pressed against the first gas diffuser.

10. The method according to claim 9 , wherein the first fixing element consists of a gas-tight material, and quartz glass made from synthetically produced raw materials.

11. The method according to claim 9 , wherein the first fixing element, viewed in the direction of flow of a treatment gas, is arranged upstream of the first gas diffuser and that a second fixing element in the direction of flow is arranged downstream of the second gas diffuser and is adjacent thereto.

12. The method according to claim 11 , wherein the first fixing element, the first gas diffuser, the intermediate product to be treated, the second gas diffuser and the second fixing element are adjacent to each other in an abutting manner in this order.

13. An apparatus for producing a glass component comprising:
a sheath tube composed of glass for receiving a void-containing intermediate product;
wherein the sheath tube has a longitudinal axis and an inner bore; and
wherein a first gas-permeable gas diffuser is inserted into the sheath tube's inner bore, which is displaceable along the sheath tube's longitudinal axis towards the intermediate product, wherein a clamping device is inserted into the sheath tube inner bore, which exerts a pressure on the first gas diffuser, and
wherein the clamping device comprises an elastically deformable spring element inserted in the sheath tube's inner bore, or a slide which is displaceable in the sheath tube's inner bore and having a first magnetic element composed of a magnetic material and a second magnetic element which is movable in the direction of the longitudinal axis outside the sheath tube's inner bore and which acts on the magnetic elem.

14. The apparatus according to claim 13 , wherein into the sheath tube's inner bore a first fixing element is inserted, which is displaceable along the sheath tube's longitudinal axis and which presses against the first gas diffuser, and in or on which at least one through-going gas channel is formed.

Assignees

• Heraeus Quarzglas

Inventors

• Plass Jacqueline
• Schönfeld Dörte
• Schmitt Clemens
• Laaz Alexander
• Langner Andreas
• Schötz Gerhard
• Lehmann Walter
• Hünermann Michael
• Weidlich Stefan
• Schäfer Jürgen

Classifications

• C03B37/01211 Primary

  by inserting one or more rods or tubes into a tube · CPC title

• C03B2201/06

  Doped silica-based glasses · CPC title

• C03B37/01297

  by melting glass powder in a mould · CPC title

• C03B2205/63

  Ohmic resistance heaters, e.g. carbon or graphite resistance heaters · CPC title

• C03B37/01257

  Heating devices therefor · CPC title