System and rotating blade unit for preparing silica aerogel

Patent metadata

Field	Value
Publication number	US-11505657-B2
Application number	US-201715755513-A
Country	US
Kind code	B2
Filing date	Mar 7, 2017
Priority date	Mar 24, 2016
Publication date	Nov 22, 2022
Grant date	Nov 22, 2022

Abstract

The system for preparing silica aerogel according to the present invention comprises a raw material supply part transferring at least one raw material of de-ionized water, water glass, a surface modifier, an inorganic acid, and an organic solvent to a mixing part, the mixing part mixing the raw materials transferred from the raw material supply part to produce silica wet gel, a drying part drying the silica wet gel to produce the silica aerogel, a recovery part recovering a portion of the vaporized raw material of the raw materials used in at least one of the mixing part and the drying part, and a heat transfer part transferring heat to at least one of the mixing part and the drying part, wherein the system further comprises a pulverizing part that pulverizes the raw material from the row material supply part to the mixing part.

First claim

The invention claimed is:

1. A system for preparing silica aerogel, the system comprising:
a raw material supply part comprising a plurality of storage containers each separately containing a raw material of de-ionized water, water glass, a surface modifier, an inorganic acid, and an organic solvent, and further comprising tubes for transferring each raw material from the raw material supply part to a pulverizer;
the pulverizer comprising:
a jet mill and an impaction plate, configured so that the jet mill produces a jet stream that accelerates particles of a raw material and directs the accelerated particles to collide with the impaction plate thereby pulverizing the particles;
a rotating blade unit that reduces particle size and increases a reaction surface area, the rotating blade unit comprising:
a plate member having a flat plate shape;
a rotating protruding blade member protruding upward from a top surface of the plate member and rotating with respect to the top surface of the plate member, and
the rotating blade unit is disposed under the jet mill such that particles exiting the jet mill fall and accumulate by gravity on the top surface of the plate member and the rotating protruding blade member passes through the accumulation of particles of the raw material on the top surface of the plate member to perform a pulverizing operation, and the particles are further pulverized by the rotating protruding blade member as the plate member rotates with the rotating protruding blade member rotating with respect to the top surface of the plate member as the plate member is rotating; and

a homogenizer configured to mix together two liquids of the raw material supply part that do not dissolve with respect to each other to form an emulsion in which solids comprising the pulverized particles are dispersed;

a mixer comprising a mixing tank, a stirring blade in the tank and a motor for rotating the stirring blade in the tank for mixing the emulsion of the raw materials transferred from the homogenizer to produce a silica wet gel;
a dryer connected to the mixer for drying the silica wet gel to produce the silica aerogel in a powder form;
a recovery unit comprising a condenser attached to the mixer and the dryer for recovering a portion of the organic solvent vaporized in at least one of the mixer and the dryer by liquefying the vaporized organic solvent; and
a heater for transferring heat or a heated medium to at least one of the mixer and the dryer.

2. The system of claim 1 , wherein the inorganic acid is nitric acid (HNO 3 ),
the organic solvent is hexane, and
the surface modifier is hexamethyldisilazane (HMDS).

3. The system of claim 1 ,
further comprises a collector comprising a collection tube connected to the dryer and a container that collects the silica aerogel powder.

4. The system of claim 1 , further comprising a temperature sensor for measuring a temperature in the mixing tank of the mixer.

5. The system of claim 1 , wherein the recovery unit further comprises a storage tank for storing the organic solvent liquefied in the condenser.

6. The system of claim 5 , wherein the recovery unit further comprising a vacuum pump for controlling a pressure within each of the condenser and the storage tank.

Assignees

• Lg Chemical Ltd

Inventors

• Kim Ye Hon
• Lee Dong Kwon
• Lee Jong Ku
• Lee Je Kyun

Classifications

• B01J19/00

  Chemical, physical or physico-chemical processes in general; Their relevant apparatus · CPC title

• C01B33/1585 Primary

  Dehydration into aerogels · CPC title

• B02C19/06

  Jet mills · CPC title

• C08J3/075

  Macromolecular gels · CPC title

• B02C18/18

  Knives; Mountings thereof · CPC title