Calcium nitrate and potassium nitrate fertiliser particles

Patent metadata

Field	Value
Publication number	US-11485689-B2
Application number	US-201816476942-A
Country	US
Kind code	B2
Filing date	Jan 15, 2018
Priority date	Jan 16, 2017
Publication date	Nov 1, 2022
Grant date	Nov 1, 2022

Abstract

The present disclosure concerns fertilizer particles comprising calcium nitrate and potassium nitrate. It is found that fertilizer particles comprising 43 to 47% w/w calcium nitrate and 46 to 54% w/w potassium nitrate can be produced by melt granulation. Due to undercooling problems, such particles were not expected to be suitable for industrial production by melt granulation. However, the present disclosure provides a composition which forms a low viscosity melt with short solidification time. This was successfully achieved by reducing the water content of a fertilizer melt comprising 43 to 47% w/w calcium nitrate and 46 to 54% w/w potassium nitrate to less than 3% w/w of the melt.

First claim

The invention claimed is:

1. A method for producing solid fertilizer particles comprising the steps:
a. forming liquid drops from a homogeneous fertilizer melt comprising 43 to 47% w/w calcium nitrate and 46 to 54% w/w potassium nitrate and less than 3% w/w water;
b. cooling the liquid drops to form solid particles; and
c. coating the solid particles,
wherein the amount of coating applied is in the range of 0.05 to 0.3% w/w relative to the weight of the particles.

2. The method according to claim 1 , wherein the temperature of the fertilizer melt is in the range of 153 to 225° C.

3. The method according to claim 1 , wherein the liquid drops are solidified by falling through a cooling fluid.

4. The method according to claim 1 , wherein the fertilizer melt comprises about 45% w/w calcium nitrate and about 53% w/w potassium nitrate and wherein the temperature of the fertilizer melt is in the range of 200 to 225° C.

5. The method according to claim 1 , wherein the fertilizer melt comprises about 45% w/w calcium nitrate and about 49% w/w potassium nitrate and wherein the temperature of the fertilizer melt is in the range of 200 to 225° C.

Assignees

• Yara Int Asa

Inventors

• Myrstad Amund
• Chladek Petr
• Obrestad Torstein

Classifications

• C01D9/18

  Preparation in the form of shaped products, e.g. granules · CPC title

• C05C5/02 Primary

  containing sodium or potassium nitrate · CPC title

• C01D9/00 Primary

  Nitrates of sodium, potassium or alkali metals in general {(preparation as fertilizers or of fertilizers containing them C05D5/00)} · CPC title

• C05C5/04

  containing calcium nitrate · CPC title

• C05G5/30

  Layered or coated, e.g. dust-preventing coatings · CPC title