Process for producing spheroidized powder from feedstock materials

Patent metadata

Field	Value
Publication number	US-11465201-B2
Application number	US-202017102244-A
Country	US
Kind code	B2
Filing date	Nov 23, 2020
Priority date	Jun 19, 2018
Publication date	Oct 11, 2022
Grant date	Oct 11, 2022

Abstract

Disclosed herein are embodiments of methods, devices, and assemblies for processing feedstock materials using microwave plasma processing. Specifically, the feedstock materials disclosed herein pertains to scrap materials, dehydrogenated or non-hydrogenated feed material, and recycled used powder. Microwave plasma processing can be used to spheroidize and remove contaminants. Advantageously, microwave plasma processed feedstock can be used in various applications such as additive manufacturing or powdered metallurgy (PM) applications that require high powder flowability.

First claim

What is claimed is:

1. A method for manufacturing a metal spheroidized powder, the method comprising:
providing a titanium feedstock material to a microwave plasma torch; and
subjecting the titanium feedstock material to a microwave plasma process within the microwave plasma torch to form the metal spheroidized powder,
the microwave plasma process comprising introduction of an ionized plasma into the microwave plasma torch,
the ionized plasma comprising nitrogen,
wherein the metal spheroidized powder comprises particles comprising at least two different microstructures or crystal structures.

2. The method of claim 1 , wherein the titanium feedstock material comprises titanium powder.

3. The method of claim 1 , wherein the titanium feedstock material has a particle size distribution between 15 microns and 150 microns.

4. The method of claim 1 , wherein titanium feedstock material comprises commercially pure titanium (cpTi).

5. The method of claim 1 , wherein titanium feedstock material comprises hydride-dehydride (HDH) titanium powder.

6. The method of claim 1 , further comprising entraining the titanium feedstock material with an inert gas within the microwave plasma torch.

7. The method of claim 1 , wherein subjecting the titanium feedstock material to a microwave plasma process comprises introducing the titanium feedstock material to a microwave generated plasma environment having a temperature profile between 4,000 K and 8,000 K.

8. The method of claim 7 , wherein introducing the titanium feedstock material to the microwave generated plasma environment melts at least a surface portion of the titanium feedstock material.

9. The method of claim 8 , wherein melting at least the surface portion of the titanium feedstock material allows for spheroidization of the titanium feedstock material.

10. The method of claim 1 , wherein the metal spheroidized powder comprises particles with a median sphericity of at least 0.75.

11. The method claim 1 , wherein the metal spheroidized powder has a particle size distribution of between 5 and 45 microns at a low end of the particle size distribution range and between 15 and 105 microns at a high end of the particle size distribution range.

12. The method of claim 1 , wherein the metal spheroidized powder comprises particles comprising a core microstructure proximate to an interior region of the particles and a shell microstructure proximate to an outer region of the particles.

13. The method of claim 1 , wherein the titanium feedstock material comprises particles comprising an average particle size between 1 micron and 300 microns.

14. The method of claim 1 , further comprising cooling the metal spheroidized powder.

15. The method of claim 14 , wherein the cooling comprises controlling one or more cooling process parameters selected from the group consisting of a composition of a cooling gas, a cooling gas flow rate, and a residence time of the metal spheroidized powder.

16. The method of claim 1 , further comprising selecting or analyzing the titanium feedstock material to determine the composition of the titanium feedstock material prior to providing the titanium feedstock material to the microwave plasma torch.

17. The method of claim 16 , further comprising determining a desired microstructure of the spheroidized metal powder based on the determined composition of the titanium feedstock material.

18. The method of claim 1 , wherein a particle size distribution of the titanium feedstock material is maintained in a particle size distribution of the metal spheroidized powder.

19. The method of claim 1 , further comprising collecting the metal spheroidized powder in sealed drums in an inert atmosphere.

Assignees

• 6K Inc

Inventors

• Barnes John
• Bent Aaron
• Hadidi Kamal
• Redjdal Makhlouf
• Turchetti Scott
• Ullal Saurabh
• Duanmu Ning
• Kozlowski Michael C

Classifications

• B22F1/142

  Thermal or thermo-mechanical treatment · CPC title

• B22F1/065 Primary

  Spherical particles · CPC title

• B22F8/00

  Manufacture of articles from scrap or waste metal particles · CPC title

• B33Y70/00 Primary

  Materials specially adapted for additive manufacturing · CPC title

• C22C19/07

  based on cobalt · CPC title