Device for dispensing a fluid, which device can be arranged in a reactor comprising a fixed catalytic bed

Patent metadata

Field	Value
Publication number	US-11465112-B2
Application number	US-201917258902-A
Country	US
Kind code	B2
Filing date	Jun 27, 2019
Priority date	Jul 10, 2018
Publication date	Oct 11, 2022
Grant date	Oct 11, 2022

Abstract

The invention relates to a device (D) for distributing a fluid, which is able to be arranged in a fixed catalytic bed (C1, C2) of a reactor (R), said device comprisingconveying means for conveying said fluid, comprising a plurality of pipes each directly receiving a distinct share of said fluid,distribution means for distributing said fluid,means for generating a local pressure drop in said fluid,such that:the device comprises manifold means (2a) for collecting said fluid together, and providing the fluidic connection between the pipes of said fluid conveying means and said fluid distribution means,said means for generating a local pressure drop are added on to said conveying or distribution or manifold (2a) means.

First claim

The invention claimed is:

1. A device (D) for distributing a fluid, wherein the device feeds a fixed catalytic bed (C 1 , C 2 ; C′ 1 , C′ 2 ) of a reactor (R) with a reactant, said device comprising:
an upstream fluid conveyer comprising a plurality of pipes ( 1 ) each directly receiving a distinct share of said fluid,
a downstream fluid distributer ( 3 ),
a pressure reducing member,
wherein the device comprises a manifold ( 2 a ; 2 b ) for collecting said fluid together, and providing a direct fluidic connection between the pipes of said fluid conveyer ( 1 ) and said fluid distributer ( 3 ),
wherein said pressure reducing member is added on to said fluid conveyer ( 1 ) or fluid distributer ( 3 ) or manifold ( 2 a ; 2 b ).

2. The device of claim 1 , additionally comprising a plurality of fluid distributers ( 3 ), a plurality of manifolds ( 2 a ; 2 b ), and a fluid connector ( 10 );
wherein said manifolds ( 2 a ; 2 b ) are arranged one below the other,
wherein said fluid connector ( 10 ) provide a fluidic connection between the plurality of the manifolds ( 2 a ; 2 b ).

3. The device of claim 1 , wherein the manifold for collecting said fluid comprise at least one tube or an array of tubes ( 2 b ), to which the pipes of the fluid conveyer ( 1 ) are connected, said tube or tubes ( 2 b ) being closed at their ends.

4. The device of claim 1 , wherein said array of tubes ( 2 b ) is arranged in the form of a cross, a network, a grid or a star.

5. The device of claim 1 , wherein the manifold for collecting said fluid comprise at least one ring ( 2 a ), to which the pipes ( 1 ) of the fluid conveyer are connected.

6. The device of claim 1 , wherein said fluid conveyer ( 1 ) and/or a fluid connector ( 10 ) extend along an axis (z) and each of said fluid-collecting manifolds ( 2 a ; 2 b ) extend in a plane (P), such that the axis (z) and the plane (P) form an angle (α) comprised between 60 and 120 degrees.

7. The device of claim 1 , wherein said pressure reducing member comprises a restriction in the cross section for passage of the fluid of the restriction orifice ( 5 ), local narrowing or bellows type.

8. The device of claim 1 , wherein said fluid distributer comprises a plurality of nozzles ( 3 ), connected to said manifold ( 2 a ; 2 b ).

9. The device of claim 1 , wherein the angle of connection (β) of the body of said nozzles with respect to the manifold is comprised between 60 and 120 degrees.

10. The device of claim 1 , wherein the pressure reducing member ( 5 ) is added on to the fluid distributer in the vicinity of the region of connection to said manifold ( 2 a ; 2 b ).

11. A reactor (R), comprising:
a fixed catalytic bed (C 1 , C 2 ; C′ 1 , C′ 2 )
a distribution device (D) as claimed in claim 1 , arranged in said bed in such a way that the inlet or at least one of the inlets of the pipes ( 1 ) of the fluid conveyer of said device are upstream of or flush with said bed, and the manifold ( 2 a ; 2 b ), fluid distributer ( 3 ) and optionally fluid connector ( 10 ) of said device are in said bed.

12. The reactor (R) of claim 11 , wherein said manifold of said device extend in a plane (P) orthogonal to the axis (z) of said reactor (R).

13. The reactor of claim 11 , wherein said fixed catalytic bed supports the device.

14. The reactor of claim 11 , wherein the catalytic bed contains catalytic elements and wherein the dimensions of the outlets of each of said fluid distributers are strictly smaller than the smallest dimension of said elements at the level of which the fluid is distributed.

15. A process wherein the device (D) of claim 1 is/are implemented, wherein a feedstock comprising naphtha, is hydrotreated, or wherein a cracked petroleum feedstock is selectively hydrogenated, or wherein a gas is cleaned of its impurities by adsorption.

16. The device of claim 2 wherein the plurality of manifolds comprise at least two superposed rings.

17. The device of claim 16 wherein the at least two superposed rings comprise an upper and lower ring wherein the upper ring extends in a plane (P 1 ) orthogonal to the axis (z), and the lower ring extends in a plane (P 2 ) which is parallel to (P 1 ).

18. The device of claim 17 wherein the upper and lower rings are connected by the fluid connector, wherein said fluid connector comprises cylindrical pipes extending along the axis (z).

19. A process wherein the reactor (R) of claim 11 is/are implemented, wherein a feedstock comprising naphtha, is hydrotreated, or wherein a cracked petroleum feedstock is selectively hydrogenated, or wherein a gas is cleaned of its impurities by adsorption.

Assignees

• Axens

Inventors

• Boutrot Catherine
• Le Coz Jean-Francois

Classifications

• B01J4/004 Primary

  Sparger-type elements · CPC title

• B01J8/025

  in a cylindrical shaped bed · CPC title

• B01J8/0085

  promoting uninterrupted fluid flow, e.g. by filtering out particles in front of the catalyst layer · CPC title

• B01J2204/002

  the feeding side being of particular interest · CPC title

• B01J8/0278

  Feeding reactive fluids (for solid material B01J8/0015) · CPC title