Method for preparing electrospraying particles to improve stability of polyphenol

Patent metadata

Field	Value
Publication number	US-11464746-B2
Application number	US-201916419323-A
Country	US
Kind code	B2
Filing date	May 22, 2019
Priority date	May 22, 2019
Publication date	Oct 11, 2022
Grant date	Oct 11, 2022

Abstract

This invention provides a method for preparing electrospraying particles to improve stability of polyphenol including the following steps: preparing a pectin-silica composite; adding polyphenolic compounds into the pectin-silica composite to prepare a core solution; and coaxial electrospraying the core solution and a shell solution to prepare electrospraying particles loaded polyphenol. This method utilizes a pectin-silica composite as a polyphenol loading carrier, improves the encapsulating efficiency of polyphenols, reduces the contact probability of polyphenols with oxygen and water, and improves the stability of polyphenols; and an acidic aqueous solution is used as a shell solution to synergize with the pectin-silica composite to further improve the stability of polyphenols.

First claim

What is claimed is:

1. A method for preparing electrospraying particles to improve stability of polyphenol comprising the following steps:
preparing a pectin-silica composite;
adding polyphenolic compounds into the pectin-silica composite to prepare a core solution; and
coaxial electrospraying the core solution and a shell solution to prepare electrospraying particles loaded polyphenol.

2. The method for preparing the electrospraying particles to improve the stability of the polyphenol according to claim 1 , wherein preparing the pectin-silica composite comprising the following steps:
preparing a pectin solution: adding deionized water into pectin and stirring until the pectin is completely dissolved, and the pectin solution in an amount of 5%-10% by weight is prepared;
preparing a silica suspension: adding the deionized water into a silica powder while stirring, and the silica suspension in an amount of 0.1%-0.5% by weight is prepared; and
preparing the pectin-silica composite: adding the silica suspension in the amount of 0.1%-0.5% by weight into the pectin solution in the amount of 5%-10% by weight drop by drop while stirring, and the pectin-silica composite being obtained.

3. The method for preparing the electrospraying particles to improve the stability of the polyphenol according to claim 2 , adding 0.1-0.5 g tea polyphenols into the pectin-silica composite and stirring, and the core solution being prepared.

4. The method for preparing the electrospraying particles to improve the stability of the polyphenol according to claim 1 , wherein the shell solution is an acidic aqueous solution.

5. The method for preparing the electrospraying particles to improve the stability of the polyphenol according to claim 4 , wherein the shell solution is the acidic aqueous solution of which pH is 4.

6. The method for preparing the electrospraying particles to improve the stability of the polyphenol according to claim 4 , wherein the shell solution is an acetic acid solution in an amount of 5%-10%.

7. The method for preparing the electrospraying particles to improve the stability of the polyphenol according to claim 1 , wherein electrospraying conditions comprise: electrostatic voltage: 16-18 kv; receiving distance: 13-16 cm; needle type of the core solution: inner diameter 0.6 mm, outer diameter 0.9 mm; needle type of the shell solution: inner diameter 0.12 mm, outer diameter 0.15 mm; room temperature: 20° C.-25° C.; and air humidity: 45%-65%.

8. The method for preparing the electrospraying particles to improve the stability of the polyphenol according to claim 1 , comprising the following steps:
preparing a pectin solution: adding deionized water into pectin and stirring until the pectin is completely dissolved, and the pectin solution in an amount of 10% by weight being prepared;
preparing a silica suspension: adding the deionized water into a silica powder while stirring, and the silica suspension in an amount of 0.5% by weight being prepared;
adding 0.5 g tea polyphenols into the pectin-silica composite and stirring for 2 hours in a magnetic stirrer, and the pectin-silica composite being prepared; and
placing the pectin-silica composite on an electrospraying device as the core solution, taking an acetic acid solution in an amount of 10% by weight as the shell solution, and electrospraying particles loaded polyphenol being prepared;
wherein electrospraying conditions comprise: electrostatic voltage: 18 kv; receiving distance: 16 cm; needle type of the core solution: inner diameter 0.6 mm, outer diameter 0.9 mm; needle type of the shell solution: inner diameter 0.12 mm, outer diameter 0.15 mm; room temperature: 25° C.; and air humidity: 65%.

Assignees

• Univ Zhejiang Technology

Inventors

• Shao Ping
• Niu Ben
• Jiang Ligang

Classifications

• A23L33/105

  Plant extracts, their artificial duplicates or their derivatives · CPC title

• B01J2/02

  by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops · CPC title

• A23L29/231

  Pectin; Derivatives thereof · CPC title

• A61K9/4816

  Wall or shell material · CPC title

• A23V2002/00

  Food compositions, function of food ingredients or processes for food or foodstuffs · CPC title