Hydrogel encapsulations and methods of making the same
US-2024180220-A1 · Jun 6, 2024 · US
US11458105B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11458105-B2 |
| Application number | US-201314057127-A |
| Country | US |
| Kind code | B2 |
| Filing date | Oct 18, 2013 |
| Priority date | Dec 4, 2008 |
| Publication date | Oct 4, 2022 |
| Grant date | Oct 4, 2022 |
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A hybrid encapsulate formulation obtained by mixing a starch/fragrance emulsion with a core-shell capsule suspension is provided as is a method of using the formulation in a personal care product, a beauty care product, a fabric care product, a home care product, a personal hygiene product, an oral care product and a method for releasing an encapsulated fragrance by moisture, shear, or a combination thereof.
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What is claimed is: 1. A hybrid encapsulate formulation consisting of 41% to 50% starch, 2% to 3.5% hydrocolloid, 10% to 30% sol-gel capsules, and 25% to 38% of the first fragrance, based on the dry weight of the hybrid encapsulate formulation, wherein the dry weight totals 100%; and wherein the hybrid encapsulate formulation is obtained by a method consisting essentially of (a) preparing an aqueous starch solution; (b) preparing an oil phase containing a first fragrance; (c) emulsifying the oil phase with the aqueous starch solution to obtain an emulsion; (d) mixing the emulsion with a core-shell capsule suspension to obtain a mixture, wherein the core-shell capsule suspension consists essentially of (i) prepared sol-gel capsules that encapsulate a second fragrance, and (ii) a hydrocolloid selected from the group consisting of polyvinylpyrrolidone, polyvinyl alcohol, and a combination thereof; and (e) spray drying the mixture to obtain a hybrid encapsulate formulation. 2. The hybrid encapsulate formulation of claim 1 , wherein the second fragrance in the emulsion and the first fragrance in the sol-gel capsule are the same. 3. The hybrid encapsulate formulation of claim 1 , wherein the second fragrance in the emulsion and the first fragrance in the sol-gel capsule are different. 4. A personal care product comprising the hybrid encapsulate formulation of claim 1 . 5. The personal care product of claim 4 , wherein said product is an antiperspirant or deodorant. 6. The personal care product of claim 4 , wherein said product is a shampoo, hair conditioner, hair rinse, hair refresher, body wash or soap. 7. A beauty care product comprising the hybrid encapsulate formulation of claim 1 . 8. The beauty care product of claim 7 , wherein said product is a fine fragrance or Eau De Toilette product. 9. A fabric care product comprising the hybrid encapsulate formulation of claim 1 . 10. The fabric care product of claim 9 , wherein said product is a rinse conditioner, liquid detergent or powder detergent. 11. A home care product comprising the hybrid encapsulate formulation of claim 1 . 12. The home care product of claim 11 , wherein said product is an all-purpose cleaner or fabric refresher. 13. A personal hygiene product comprising the hybrid encapsulate formulation of claim 1 . 14. The personal hygiene product of claim 13 , wherein the product is a hand sanitizer. 15. An oral care product comprising the hybrid encapsulate formulation of claim 1 . 16. The oral care product of claim 15 , wherein the product is a tooth powder. 17. The hybrid encapsulate formulation of claim 1 , wherein the hydrocolloid is polyvinylpyrrolidone. 18. The hybrid encapsulate formulation of claim 1 , wherein the spray drying step is performed at a spray drying inlet temperature of 150 to 240° C.
Encapsulated compositions · CPC title
In situ polymerisation with all reactants being present in the same phase · CPC title
Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms · CPC title
Formulations or additives for perfume preparations (essential oils or perfumes per se C11B9/00) · CPC title
Washing or bathing preparations · CPC title
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