Method for controlling an ozone generating machine

Patent metadata

Field	Value
Publication number	US-11453586-B2
Application number	US-201816622907-A
Country	US
Kind code	B2
Filing date	Jun 29, 2018
Priority date	Jun 30, 2017
Publication date	Sep 27, 2022
Grant date	Sep 27, 2022

Abstract

A method for producing ozone in an ozone generating machine, including the steps of: supplying feed gas containing dioxygen at a gas inlet (O 2 IN) of an ozone generator (OzG), at a given feed gas flow and feed gas pressure; supplying an alternating electric current so as to create electric discharges to generate a given amount of ozone at a gas outlet (O 3 OUT) of the ozone generator (OzG); adjusting electric current power and at least one of a plurality of process parameters comprising; characterized in that the method includes, during ozone production, the steps of: monitoring electric power and said at least one parameter of the plurality of process parameters; and adjusting the feed gas pressure in response to the adjustment of the electric current power and said at least one process parameter.

First claim

What is claimed is:

1. A method for producing ozone in an ozone generating machine (OGM) comprising at least two electrodes (E 1 , E 2 ) separated by an ozonizing gap (OG) and a dielectric layer, and located in an ozone generator (OzG) comprising at least a gas inlet (O 2 IN) for receiving a feed gas containing dioxygen, and a gas outlet (O 3 OUT) for exhausting gas comprising ozone, the method comprising the steps of:
supplying the feed gas containing dioxygen at the gas inlet (O 2 IN) of the ozone generator (OzG), at a first feed gas flow rate and first feed gas pressure,
supplying an alternating electric current to said at least two electrodes (E 1 , E 2 ) of the ozone generator (OzG) so as to create electric discharges in the ozonizing gap (OG), to generate a given amount of ozone at the gas outlet (O 3 OUT) of the ozone generator (OzG),
adjusting an electric current power density and at least one process parameter selected from a plurality of process parameters comprising: (i) feed gas flow, (ii) frequency of the alternating electric current, (iii) voltage of the alternating electric current, or (iv) cooling temperature of the ozone generator (OzG), to adjust the amount of generated ozone at the gas outlet (O 3 OUT) of the ozone generator (OzG),
characterized in that the method comprises, during ozone production, the steps of:
monitoring electric power and the at least one process parameter,
adjusting the first feed gas pressure to a second feed gas pressure in response to the adjustment of at least one process parameter.

2. The method according claim 1 , wherein the step of adjusting the first feed gas pressure to the second feed gas pressure comprises:
a step of calculating a derivative with respect to feed gas pressure of a model predicting a performance of the ozone generator (OzG) based on the first feed gas pressure, the electric current power density and said at least one of the said process parameters, to determine an optimum feed gas pressure leading to an optimized efficiency of the ozone generator (OzG) operated with the adjusted value of the electric current power density and said at least one adjusted process parameter, and
adjusting the first feed gas pressure to the second feed gas pressure to reach the optimum gas feed pressure within the ozone generator (OzG).

3. The method according to claim 1 , further comprising a step of monitoring the generated amount of ozone at the gas outlet (O 3 OUT) of the ozone generator (OzG) by measuring an ozone concentration and/or measuring a flow of gas flowing through the ozone generator (OzG).

4. The method according to claim 2 , wherein the steps of calculating the optimum feed gas pressure and adjusting the first feed gas pressure to the second feed gas pressure are performed simultaneously to, or within a predetermined operating time following a change power of the alternating electric current or the at least one process parameter.

5. The method according to claim 1 , wherein:
during the step of adjusting the at least one process parameter, only the frequency of the alternating electric current and the feed gas flow are adjusted, and wherein:
an increase of the frequency of the alternating electric current leads to an increase of the first feed gas pressure, and a decrease of the electric current frequency of the alternating electric current leads to a decrease of the first feed gas pressure.

6. The method according to claim 1 , wherein:
during the step of adjusting the electric current power density and at least one process parameter, only the electric current voltage and the feed gas flow are adjusted, and wherein:
an increase of the electric current voltage leads to an increase of the first feed gas pressure, and a decrease of the electric current voltage leads to a decrease of the first feed gas pressure.

7. The method according to claim 1 , wherein the first feed gas pressure in the ozone generator (OzG) is varied to the second feed gas pressure within a range of 0.5 bar(a)-6 bar(a).

8. The method according to claim 1 , further comprising the steps of:
monitoring the generated amount of ozone,
monitoring the feed gas pressure,
monitoring an amount of electricity consumed,
calculating and monitoring an ozone yield based on the generated amount of ozone and the amount of electricity consumed,
comparing the ozone yield before and after the step of adjusting the first gas feed pressure to the second gas feed pressure, and
adjusting the second feed gas pressure to a third feed gas pressure if ozone yield is decreased so as to optimize the ozone yield.

9. The method according to claim 8 , further comprising the step of further adjusting the third feed gas pressure if ozone yield is increased or is the same after the step of adjusting the second gas feed pressure to the third feed gas pressure, so as to further increase the ozone yield.

10. The method according to claim 8 , further comprising the step of maintaining the third feed gas pressure if ozone yield is increased or is the same after the step of adjusting the second gas feed pressure to the third gas feed pressure.

Assignees

• Suez Groupe
• Suez Groupe Sas

Inventors

• Seyrling Sieghard
• Tremblay Marco
• Ramoino Luca

Classifications

• C01B2201/90

  Control of the process · CPC title

• C01B13/115 Primary

  characterised by the electrical circuits producing the electrical discharge · CPC title

• C01B13/11 Primary

  by electric discharge · CPC title

• C01B2201/32

  Constructional details of the dielectrics · CPC title

• H01T23/00

  Apparatus for generating ions to be introduced into non-enclosed gases, e.g. into the atmosphere · CPC title