Permeable graphene and permeable graphene membranes
US-2020261858-A1 · Aug 20, 2020 · US
US11452973B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11452973-B2 |
| Application number | US-201916771091-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jan 24, 2019 |
| Priority date | Jan 24, 2018 |
| Publication date | Sep 27, 2022 |
| Grant date | Sep 27, 2022 |
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A reverse osmosis membrane of the present invention includes a porous support substrate (2) and a separation active layer (3) formed on a surface of the porous support substrate (2) and formed of a carbon film containing organized carbon.
Opening claim text (preview).
The invention claimed is: 1. A method for producing a reverse osmosis membrane, the method comprising: a coating film forming step of forming a coating film soluble in a predetermined solvent on a surface of a porous support substrate insoluble in the solvent; a pre-carbon film forming step of forming a pre-carbon film on the coating film by a physical vapor deposition method using carbon as a target material under an atmosphere containing nitrogen gas together with a noble gas, wherein a ratio of the noble gas:the nitrogen gas is 1:0.1 to 1:10; a coating film removal step of dissolving and removing the coating film with the solvent after the pre-carbon film is formed; and an organization step of compressing the pre-carbon film by applying a pressure to the pre-carbon film by using pure water of 5.5 MPa or greater for 20 hours or longer to form a separation active layer formed of a carbon film containing organized carbon. 2. The method according to claim 1 , wherein, in the coating film removal step, the coating film is dissolved and removed from a laminate of the porous support substrate, the coating film, and the pre-carbon film while being immersed in the solvent. 3. The method according to claim 2 , wherein, in the coating film removal step, the solvent with the laminate immersed therein is shaken. 4. The method according to any one of claim 1 , wherein the porous support substrate includes a nonwoven backing layer and a porous plastic layer on a surface of the backing layer, and wherein, in the coating film forming step, the coating film is formed on the porous plastic layer. 5. The method according to any one of claim 2 , wherein the porous support substrate includes a nonwoven backing layer and a porous plastic layer on a surface of the backing layer, and wherein, in the coating film forming step, the coating film is formed on the porous plastic layer. 6. The method according to any one of claim 3 , wherein the porous support substrate includes a nonwoven backing layer and a porous plastic layer on a surface of the backing layer, and wherein, in the coating film forming step, the coating film is formed on the porous plastic layer.
by deposition from the gaseous phase, e.g. sputtering, CVD, PVD · CPC title
Separation of the coating from the substrate · CPC title
Specific pressure applied · CPC title
Preparation or purification of carbon not covered by groups C01B32/15, C01B32/20, C01B32/25, C01B32/30 · CPC title
Carbon · CPC title
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