Surface property inspection method, surface property inspection apparatus, and surface property inspection system

Patent metadata

Field	Value
Publication number	US-11442033-B2
Application number	US-201816628525-A
Country	US
Kind code	B2
Filing date	Jun 27, 2018
Priority date	Jul 10, 2017
Publication date	Sep 13, 2022
Grant date	Sep 13, 2022

Abstract

A surface property evaluation method includes a measurement step for acquiring the distribution of impedance in the depth direction of a test piece, and an evaluation step for evaluating the surface treatment state in the depth direction and wherein the evaluation step includes: a step for creating a reference measurement value group by preparing untreated sample, good sample, and sample to be evaluated, and calculating an impedance ratio γ1 at each frequency for the untreated sample and good sample impedances; a step for creating an evaluation measurement value group by calculating an impedance ratio γ2 for the impedances of untreated sample at each frequency relative to the sample to be evaluated impedances; and a step for evaluating the surface treatment state of a sample to be evaluated by comparing a reference measurement value group with the evaluation measurement value group.

First claim

The invention claimed is:

1. A surface property evaluation method for evaluating surface treatment state of a metal product, comprising:
a preparation step for preparing three test pieces consisting of a comparative sample whose surface is not treated, a reference sample whose surface is appropriately treated, and a test subject product for evaluation of performed surface treatment;
an impedance distribution acquisition step for acquiring impedance distributions of the three test pieces; and
an impedance distribution analysis step for evaluating surface treatment state of the test subject product, based on the impedance distributions acquired in the impedance distribution acquisition step;
wherein the impedance distribution acquisition step comprises:
a step for disposing each of the three test pieces inside a coil and applying an AC current to the coil to cause an AC magnetism excited by the coil to penetrate into each of the three test pieces;
a step for varying the frequency of the AC current applied to the coil, thereby varying a penetration depth of the AC magnetism into each of the three test pieces; and
a data acquisition step for acquiring the impedance distribution in a surface of each of the three test pieces by measuring coil impedances at multiple frequencies;
wherein the impedance distribution analysis step comprises:
a step for calculating an impedance ratio γ1 (Z 1 /Z 0 ) at each frequency, wherein the impedance ratio γ1 of an impedance Z 0 of the comparative sample and an impedance Z 1 of the reference sample is acquired at each of the multiple frequencies in the data acquisition step to create a reference measurement value group Gγ1;
a step for calculating at each frequency for the same multiple frequencies as in the reference measurement value group Gγ1 an impedance ratio γ2 (Z 2 /Z 0 ), wherein the impedance ratio γ2 of an impedance Z 2 of the test subject product and the impedance Z 0 of the comparative sample is acquired in the data acquisition step to create an evaluation measurement value group Gγ 2 ; and
a step for evaluating the surface treatment state of the test subject product by comparing certain evaluation criteria, set based on the reference measurement value group Gγ1, with the evaluation measurement value group Gγ2;
wherein the evaluation criteria are selected from among:
an area width criterion in which the surface treatment state of the test subject product is evaluated by setting an allowable impedance ratio range at each frequency based on the impedance ratio γ1 at each frequency of the reference measurement value group Gγ1 and comparing said allowable impedance ratio range to the impedance ratio γ2;
a peak criterion in which the surface treatment state of the test subject product is evaluated by setting an allowable peak position range based on the peak position of the reference measurement value group Gγ1 relative to frequency and comparing said allowable peak position range to the peak position in the impedance ratio γ2; and
an integral area criterion in which the surface treatment state of the test subject product is evaluated by setting an allowable integral value range based on the integral value of the impedance ratio γ1 of the reference measurement value group Gγ1 in a predetermined frequency range, and comparing said allowable integral value range to the integral value of the impedance ratio γ2 in said frequency range.

2. The surface property evaluation method of claim 1 , wherein the impedance distribution analysis step comprises a step for calculating the penetration depth of the AC magnetism into the test subject product based on the frequency of AC current applied to the coil, and the surface treatment state is evaluated by respectively producing a reference 2D map displaying the impedance ratio T1 relative to depth from the surface for the reference sample based on the reference measurement value group Gγ1, and an evaluation 2D map displaying the impedance ratio γ2 relative to depth from the surface of the sample to be evaluated based on the evaluation measurement value group Gγ 2 .

3. The surface treatment evaluation method of claim 1 , wherein in the impedance distribution analysis step, when evaluating the surface treatment state of the test subject product to which multiple surface treatments have been applied, different evaluation criteria are selected according to the depth from the surface of the test subject product.

4. The surface property evaluation method of claim 1 , wherein when the surface treatment applied to the test subject product includes shot peening, the peak criterion or the integral area criterion is selected to evaluate the surface treatment close to the surface of the test subject product.

5. The surface property evaluation method of claim 4 , wherein in the impedance distribution analysis step, the state of surface treatment by shot peening is evaluated.

6. The surface property evaluation method set forth in claim 1 , wherein the allowable ranges for the area width criterion, the peak criterion, and the integral area criterion are set based on the variability of multiple reference measurement value groups Gγ1.

7. A surface property evaluation apparatus for evaluating surface treatment of a metal product, comprising:
an oscillator comprising an AC power supply and a variable frequency circuit capable of varying a frequency of AC current output by the AC power supply;
a detector connected to the oscillator, comprising a coil for exciting AC magnetism by the AC current applied from the variable frequency circuit, for causing the AC magnetism to penetrate each of three test pieces, wherein the three test pieces consist of a comparative sample whose surface is not treated, a reference sample whose surface is appropriately treated, and a test subject product for evaluation of performed surface treatment;
a measurement instrument, connected to the variable frequency circuit and the detector, for acquiring an impedance distribution for each of the three test pieces; and
an evaluation device that evaluates the surface treatment state of the test subject product based on the impedance distribution acquired for the test subject product, wherein the evaluation device is configured to implement:
a preparation step for preparing the three test pieces;
an impedance distribution acquisition step for acquiring impedance distributions of each of the three test pieces; and
an impedance distribution analysis step for evaluating surface treatment state of the test subject product, based on the impedance distributions acquired in the impedance distribution acquisition step;
wherein the impedance distribution acquisition step comprises:
a step for disposing each of the three test pieces inside a coil and applying an AC current to the coil to cause an AC magnetism excited by the coil to penetrate into each of the three test pieces;
a step for varying the frequency of the AC current applied to the coil, thereby varying a penetration depth of the AC magnetism into each of the three test pieces; and
a data acquisition step for acquiring the impedance distribution in a surface of each of the three test pieces by measuring coil impedances at multiple frequencies;
wherein the impedance distribution analysis step comprises:
a step for calculating an impedance ratio γ1 (Z 1 /Z 0 ) at each frequency, wherein the impedance ratio γ1 of an impedance Z 0 of the comparative sample and an impedance Z 1 of the reference sample is acquired at each of the multiple frequencies in the data acquisition step to create a reference measurement value group Gγ1;
a step for calculating at each frequency for the same multiple frequencies as in the reference measurement value group Gγ1 an impedance ratio γ2 (Z 2 /Z 0 ), where

Assignees

• Sintokogio Ltd

Inventors

• Makino Yoshiyasu

Classifications

• G01N27/80 Primary

  for investigating mechanical hardness, e.g. by investigating saturation or remanence of ferromagnetic material · CPC title

• G01N27/023 Primary

  where the material is placed in the field of a coil · CPC title

• G01N33/204

  Structure thereof, e.g. crystal structure · CPC title

• G01N27/90

  using eddy currents · CPC title

• Y02P10/25

  Process efficiency · CPC title