Managing wellbore cement compositions based on material characteristics

Patent metadata

Field	Value
Publication number	US-11441415-B2
Application number	US-201916629076-A
Country	US
Kind code	B2
Filing date	Feb 12, 2019
Priority date	Feb 12, 2019
Publication date	Sep 13, 2022
Grant date	Sep 13, 2022

Abstract

Wellbore cement compositions can be managed based on material characteristics determined from a cement sample. For example, a cement sample can be retrieved from a wellbore. The cement sample can be analyzed using a plurality of sensors to generate a three-dimensional mapping of particles in the cement sample. The three-dimensional mapping can represent three-dimensional spatial relationships between the particles in the cement sample. The three-dimensional mapping can be compared to baseline three-dimensional mappings in a database. The comparison of the three-dimensional mappings can be used to identify at least one material characteristic of the cement sample. Based on the at least one material characteristic of the cement sample, a cement mixture can be prepared or information related to the cement mixture can be output.

First claim

What is claimed is:

1. A method comprising:
retrieving a cement sample from a wellbore;
analyzing the cement sample using a plurality of sensors to generate a three-dimensional mapping of particles in the cement sample, the three-dimensional mapping representing three-dimensional spatial relationships between the particles in the cement sample;
comparing the three-dimensional mapping to a plurality of baseline three-dimensional mappings in a database to identify at least one material characteristic of the cement sample; and
preparing a cement mixture based on the at least one material characteristic of the cement sample from the wellbore.

2. The method of claim 1 , wherein:
the cement sample is a cement cutting from a casing shoe; and
the plurality of sensors include any combination of: a first sensor configured to perform X-Ray Computing Tomography on the cement sample, a second sensor configured to perform Focused Ion-Beam Scanning Electron Macroscopy with X-Ray Diffraction on the cement sample, a third sensor configured to perform X-Ray Fluorescence on the cement sample, a fourth sensor configured to perform Energy Dispersive Spectroscopy on the cement sample, or a fifth sensor configured to perform Nuclear Magnetic Resonance on the cement sample.

3. The method of claim 1 , wherein the at least one material characteristic comprises one or more physical properties selected from the group consisting of: a porosity of the cement sample, density of the cement sample, CSH content in the cement sample, degree of crystallinity, a volume fraction of a chemical component in the cement sample, a total surface area of a chemical component in the cement sample, a given geometric shape factor of a chemical component in the cement sample, and an amount of unreacted bulk blend component in the cement sample.

4. The method of claim 1 , further comprising generating the database by:
preparing a plurality of slurry mixtures;
curing the plurality of slurry mixtures under combinations of conditions including temperature values, pressure values, time values, and density values to create baseline cement samples; and
analyzing the baseline cement samples using the plurality of sensors to generate the plurality of baseline three-dimensional mappings.

5. The method of claim 4 , wherein the temperature values are greater than or equal to 230° F. (110° C.), and wherein the plurality of baseline three-dimensional mappings describe strength and permeability characteristics for each of the baseline cement samples.

6. The method of claim 1 , wherein the at least one material characteristic comprises one or more mechanical properties selected from the group consisting of: a Young's modulus, a Poisson's ratio, strain to failure, compressive toughness, a compressive strength, and a tensile strength of the cement sample.

7. The method of claim 6 , wherein the one or more mechanical properties are time-dependent mechanical properties.

8. The method of claim 1 , further comprising:
determining that a cost of the cement mixture is less than a threshold cost value using information in a database;
determining that the cement mixture has a particular composition associated with the at least one material characteristic of the cement sample using the information in the database; and
in response to determining that (i) the cost of the cement mixture is less than the threshold cost value and (ii) the cement mixture has the particular composition associated with the at least one material characteristic, preparing the cement mixture to have the particular composition.

9. A system comprising:
a plurality of sensors configured to detect a plurality of characteristics of a cement sample obtained from a wellbore and transmit sensor signals representing the plurality of characteristics;
a processing device communicatively coupled to the plurality of sensors; and
a memory device comprising instructions that are executable by the processing device for causing the processing device to:
receive the sensor signals from the plurality of sensors;
generate a three-dimensional mapping of particles in the cement sample based on the sensor signals, the three-dimensional mapping representing three-dimensional spatial relationships between the particles in the cement sample;
compare the three-dimensional mapping to a plurality of baseline three-dimensional mappings in a database to identify at least one material characteristic of the cement sample; and
output information usable for preparing a cement mixture based on the at least one material characteristic of the cement sample from the wellbore.

10. The system of claim 9 , wherein:
the cement sample is a cement cutting from a casing shoe; and
the plurality of sensors include any combination of: a first sensor configured to perform X-Ray Computing Tomography on the cement sample, a second sensor configured to perform Focused Ion-Beam Scanning Electron Macroscopy with X-Ray Diffraction on the cement sample, a third sensor configured to perform X-Ray Fluorescence on the cement sample, a fourth sensor configured to perform Energy Dispersive Spectroscopy on the cement sample, or a fifth sensor configured to perform Nuclear Magnetic Resonance on the cement sample.

11. The system of claim 9 , wherein the at least one material characteristic comprises one or more physical properties selected from the group consisting of: a porosity of the cement sample, density of the cement sample, CSH content in the cement sample, degree of crystallinity, a volume fraction of a chemical component in the cement sample, a total surface area of a chemical component in the cement sample, a given geometric shape factor of a chemical component in the cement sample, and an amount of unreacted bulk blend component in the cement sample.

12. The system of claim 9 , the memory device further comprising instructions that are executable by the processing device for causing the processing device to generate the database by:
analyzing baseline cement samples prepared under a plurality of temperature values using the plurality of sensors to generate the plurality of baseline three-dimensional mappings.

13. The system of claim 12 , wherein the plurality of temperature values are greater than or equal to 230° F. (110° C.), and wherein the plurality of baseline three-dimensional mappings describe strength and permeability characteristics for each of the baseline cement samples.

14. The system of claim 9 , wherein the at least one material characteristic comprises one or more mechanical properties selected from the group consisting of: a Young's modulus, a Poisson's ratio, a compressive strength, strain to failure, compressive toughness, and a tensile strength of the cement sample.

15. The system of claim 14 , wherein the one or more mechanical properties are time-dependent mechanical properties.

16. The system of claim 9 , the memory device further comprising instructions that are executable by the processing device for causing the processing device to:
determine that a cost of the cement mixture is less than a threshold cost value using information in a database;
determine that the cement mixture has a particular composition associated with the at least one material characteristic of the cement sample using the information in the database; and
in response to determining that (i) the cost of the cement mixture is less than the threshold cost value and (ii) the cement mixture has the particular composition associated with the at least one material characteristic, configure the information to indicate that the cement mixtur

Assignees

• Halliburton Energy Services Inc

Inventors

• Pisklak Thomas Jason
• Lewis Jr Samuel Jason
• Singh John P
• Grader Abraham S
• Morgan Ronnie Glen
• Tan Brendon C

Classifications

• G01N23/223

  by irradiating the sample with X-rays or gamma-rays and by measuring X-ray fluorescence · CPC title

• E21B47/005 Primary

  Monitoring or checking of cementation quality or level · CPC title

• G01N24/081

  Making measurements of geologic samples, e.g. measurements of moisture, pH, porosity, permeability, tortuosity or viscosity · CPC title

• G01N33/383

  Concrete or cement · CPC title

• G01N23/046 Primary

  using tomography, e.g. computed tomography [CT] · CPC title