High-temperature all-metal induction furnace, intended to melt samples of minerals and/or rocks for extracting gases under ultra-high vacuum

Patent metadata

Field	Value
Publication number	US-11421936-B2
Application number	US-201716336694-A
Country	US
Kind code	B2
Filing date	Sep 7, 2017
Priority date	Sep 27, 2016
Publication date	Aug 23, 2022
Grant date	Aug 23, 2022

Abstract

The application basically comprises supplying a high-temperature ultra-high vacuum furnace, the sole chamber of which is metal, in which an electrically conductive crucible, preferably made of tantalum, is placed onto an insulating support, preferably a ceramic, and is induction heated by a winding wound around the crucible. The insulating tube, preferably made of quartz, that is arranged between the induction winding and the crucible, advantageously acts as a surface on which the condensable species can condense. The quartz insulating tube especially allows the induction winding to be protected.

First claim

The invention claimed is:

1. A high-temperature ultrahigh-vacuum furnace, intended for the extraction of noble gases present in samples of minerals and/or rocks, comprising:
a metal chamber that is gastight comprising a first connection opening for connecting to a purification line for purifying the gases released in the chamber and/or to a gravity feed device for supplying a sample and, a second connection opening for connecting to a pump suitable for creating the ultrahigh vacuum inside the chamber,
a crucible made of electrically conductive material, suitable for containing at least one sample of minerals and/or rocks,
a support made of electrically insulating material, resting on a lower portion of the metal chamber, and supporting the crucible in the chamber,
at least one induction coil, powered from outside of the chamber through at least one insulated bushing passing through a wall of the chamber, and arranged around the crucible,
a tube made of electrically insulating material, resting on the lower portion of the metal chamber, arranged between the induction coil and the crucible supported by the support,
wherein the first connection opening is connected to a bypass part for connecting an upper portion of the chamber both to the purification line and to a storage carousel as a gravity feed device for supplying a sample.

2. The high-temperature ultrahigh-vacuum furnace as claimed in claim 1 , comprising a heat-transfer fluid cooling circuit integrated into lower and upper walls of the chamber.

3. The high-temperature ultrahigh-vacuum furnace as claimed in claim 1 , wherein the metal chamber consists of cylinders assembled together by welding and fastening flanges.

4. The high-temperature ultrahigh-vacuum furnace as claimed in claim 3 , wherein the cylinders and fastening flanges being made of stainless steel.

5. The high-temperature ultrahigh-vacuum furnace as claimed in claim 1 , wherein the distance between the induction coil and each of lower, upper and lateral inner walls is at least equal to 10 mm.

6. The high-temperature ultrahigh-vacuum furnace as claimed in claim 1 , wherein the conductive crucible is made of a material selected from tantalum (Ta), molybdenum (Mo), platinum (Pt), iron (Fe).

7. The high-temperature ultrahigh-vacuum furnace as claimed in claim 1 , wherein the electrically insulating support is made of a material selected from a ceramic, quartz.

8. The high-temperature ultrahigh-vacuum furnace as claimed claim 1 , wherein the electrically insulating tube is made of a material selected from quartz, glass-ceramic, vitreous carbon.

9. The high-temperature ultrahigh-vacuum furnace as claimed in claim 1 , wherein the lower end of the electrically insulating support is housed in a centering guide made in a lower inner wall of the chamber.

10. The high-temperature ultrahigh-vacuum furnace as claimed in claim 1 , wherein the lower end of the electrically insulating tube is housed in a centering guide made in a lower inner wall of the chamber.

11. The high-temperature ultrahigh-vacuum furnace as claimed in claim 1 , wherein an upper end of the electrically insulating tube is arranged as close as possible to an upper inner wall of the chamber.

Assignees

• Centre Nat Rech Scient

Inventors

• Zimmermann Laurent
• Blard Pierre-Henri

Classifications

• F27B14/10

  Crucibles · CPC title

• F27B5/06

  Details, accessories or equipment specially adapted for furnaces of these types · CPC title

• F27B17/02

  specially designed for laboratory use · CPC title

• F27B14/04 Primary

  adapted for treating the charge in vacuum or special atmosphere · CPC title

• F27D2007/066

  Vacuum · CPC title