Low resistance microfabricated filter

Patent metadata

Field	Value
Publication number	US-11413383-B2
Application number	US-202017092616-A
Country	US
Kind code	B2
Filing date	Nov 9, 2020
Priority date	May 16, 2012
Publication date	Aug 16, 2022
Grant date	Aug 16, 2022

Abstract

The present technology provides micro fabricated filtration devices, methods of making such devices, and uses for microfabricated filtration devices. The devices may allow diffusion to occur between two fluids with improved transport resistance characteristics as compared to conventional filtration devices. The devices may include a compound structure that includes a porous membrane overlying a support structure. The support structure may define a cavity and a plurality of recesses formed in a way that can allow modified convective flow of a first fluid to provide improved diffusive transport between the first fluid and a second fluid through the membrane.

First claim

What is claimed is:

1. A method of making a microfabricated filtration device, the method comprising:
depositing a dielectric layer over a semiconductor substrate;
forming a first layer of a membrane material on the dielectric layer and etching a pattern in the first membrane material layer;
forming a sacrificial dielectric layer over the patterned first membrane material layer and forming a second membrane material layer over the sacrificial dielectric layer;
forming a protective layer over the second membrane material layer;
etching the substrate with a first etchant process that produces a cavity that does not extend to the layers of membrane material;
etching the substrate with a second etchant process that forms a plurality of recesses through the remaining portion of the substrate and through the dielectric layer; and
etching the filtration device with a third etchant process that removes the sacrificial dielectric layer forming pores through the membrane material layers, which provides access to the recesses such that the combination of the pores, recesses, and the cavity produce apertures through the filtration device.

2. The method of claim 1 , wherein the first etchant process comprises a wet etchant.

3. The method of claim 2 , wherein the first etchant process is anisotropic.

4. The method of claim 2 , wherein the first etchant process is isotropic.

5. The method of claim 1 , wherein the first and second etchant processes comprise a reactive ion etch.

6. The method of claim 1 , wherein the membrane material comprises silicon or polysilicon membrane.

7. The method of claim 6 , wherein the pores have a width of less than 100 nm.

8. The method of claim 6 , wherein the pores have a width of less than 10 nm.

9. The method of claim 7 , wherein the plurality of recesses are rectangular and repeat along a width of the cavity and along a length of the cavity, the plurality of recesses each comprising a length of 500 μm or less.

10. The method of claim 8 , wherein the plurality of recesses comprise length by width measurements of 100 μm by 50 μm.

11. The method of claim 8 , wherein the plurality of recesses comprise length by width measurements of 250 μm by 50 μm.

12. The method of claim 1 , wherein the pores have a width of less than 100 nm.

13. The method of claim 1 , wherein the pores have a width of less than 10 nm.

14. The method of claim 1 , wherein the plurality of recesses are rectangular and repeat along a width of the cavity and along a length of the cavity, the plurality of recesses each comprising a length of 500 μm or less.

15. The method of claim 1 , wherein the plurality of recesses comprise length by width measurements of 100 μm by 50 μm.

16. The method of claim 1 , wherein the plurality of recesses comprise length by width measurements of 250 μm by 50 μm.

17. The method of claim 1 , wherein the protective layer comprises silicon nitride, silicon oxide, silicon oxynitride, or silicon carbide.

Assignees

• Univ California

Inventors

• Kant Rishi
• Roy Shuvo
• Chui Benjamin W
• Goldman Kenneth G

Classifications

• B01D39/1692 Primary

  Other shaped material, e.g. perforated or porous sheets · CPC title

• B01D61/027

  Nanofiltration · CPC title

• B01D67/0058

  by selective elimination of components, e.g. by leaching · CPC title

• B01D2325/26

  Electrical properties · CPC title

• B01D2315/14

  Batch-systems · CPC title