Method of making nanocrystalline metal flakes and nanocrystalline flakes made therefrom

Patent metadata

Field	Value
Publication number	US-11389871-B2
Application number	US-201916730212-A
Country	US
Kind code	B2
Filing date	Dec 30, 2019
Priority date	Dec 11, 2015
Publication date	Jul 19, 2022
Grant date	Jul 19, 2022

Abstract

A method of producing flakes containing nanostructures from a part made of a material. The method includes subjecting the part made of the material to peening by shots driven by ultrasonic energy for a period of time, wherein nano structures form on the surface of the part and, subsequently, damage to the part caused by continued peening of the part by the shots driven by ultrasonic energy results in separation of flakes containing nanostructures from the part made of the material. Nanocrystalline flakes containing fractured surfaces, microcracks, nanograins and nanolamellae. Sensors comprising nanocrystalline flakes containing fractured surfaces, microcracks, nanograins and nanolamellae.

First claim

The invention claimed is:

1. A nanocrystalline flake of a material, wherein the nanocrystalline flake contains one or more fractured surfaces, microcracks, and nanolamellae.

2. The nanocrystalline flake of claim 1 , wherein the nanocrystalline flake contains nanograins in the size range of 20-100 nm.

3. The nanocrystalline flake of claim 1 , wherein the nanolamellae have a thickness in the size range of 30-100 nm.

4. The nanocrystalline flake of claim 1 , wherein the material is a metal or an alloy.

5. A nanocrystalline flake of a material, wherein the nanocrystalline flake contains one or more fractured surfaces and microcracks and wherein the material is steel.

6. The nanocrystalline flake of claim 5 , wherein the steel is a stainless steel.

7. The nanocrystalline flake of claim 1 , wherein the material is one of magnesium, copper, nickel, iron, aluminum, titanium and cobalt.

8. The nanocrystalline flake of claim 1 , wherein the material is an alloy comprising one of copper, magnesium, nickel, iron, aluminum, titanium and cobalt.

9. A nanocrystalline flake of a material, wherein the nanocrystalline flake contains one or more fractured surfaces and microcracks, wherein the material is a refractory metal.

10. The nanocrystalline flake of claim 9 , wherein the refractory metal is one of niobium, tantalum, molybdenum and tungsten.

11. A nanocrystalline flake of a material, wherein the nanocrystalline flake contains one or more fractured surfaces and microcracks, wherein the material is an alloy comprising one of niobium, tantalum, molybdenum and tungsten.

12. A nanocrystalline flake of a material, wherein the nanocrystalline flake contains one or more fractured surfaces and microcracks, wherein the flake is in the size range of 10-1000 micrometers.

13. A nanocrystalline flake containing one or more fractured surfaces and microcracks, wherein the nanocrystalline flake is produced by a method comprising;
providing a part made of the material;
subjecting the part made of the material to peening by shots driven by ultrasonic energy for a period of time, wherein nanostructures form on the surface of the part and, subsequently, damage to the part caused by continued peening of the part by the shots driven by ultrasonic energy results in separation of flakes containing nanostructures from the part made of the material.

14. A sensor comprising flakes containing fractured surfaces, microcracks and nanostructures, wherein the nanostructures comprise nanograins and nanolamellae.

15. The sensor of claim 14 , the sensor is an electronic sensor.

Assignees

• Purdue Research Foundation

Inventors

• Han Qingyou
• Yin Fei
• Rakita Milan

Classifications

• B22F1/068

  Flake-like particles · CPC title

• B22F2304/10

  Micron size particles, i.e. above 1 micrometer up to 500 micrometer · CPC title

• B22F9/04 Primary

  starting from solid material, e.g. by crushing, grinding or milling ({C22C1/1084 takes precedence}; crushing, grinding or milling, in general, see the relevant subclasses, e.g. B02C) · CPC title

• B22F2998/10

  Processes characterised by the sequence of their steps · CPC title

• B22F2009/045

  by other means than ball or jet milling · CPC title