Separation of kinetic hydrate inhibitors from an aqueous solution
US-2016376171-A1 · Dec 29, 2016 · US
US11377368B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11377368-B2 |
| Application number | US-202017108709-A |
| Country | US |
| Kind code | B2 |
| Filing date | Dec 1, 2020 |
| Priority date | Dec 5, 2019 |
| Publication date | Jul 5, 2022 |
| Grant date | Jul 5, 2022 |
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A method and an apparatus for producing and providing sterile water comprising an inlet for process water; a recuperator for preheating process water and for cooling down the sterile water; a heating circuit comprising a pump, a heater for heating preheated process water and a heat retention section for keeping heated process water hot; a temperature sensor for measuring a current temperature of the sterile water leaving the heat retention section; a flow control valve located downstream of the temperature sensor; and a bypass between the flow control valve and the heater. The flow control valve keeps a volume flow in the heating circuit constant, the recuperator cools down the sterile water of a first partial volume flow, when such a first partial volume flow of sterile water is taken from the heating circuit, the bypass returns into the heating circuit a second partial volume flow of sterile water.
Opening claim text (preview).
What is claimed is: 1. An apparatus for producing and providing sterile water, comprising: an inlet to introduce process water, wherein the inlet is fluidly connected to a recuperator; the recuperator located downstream of the inlet, wherein the recuperator is to preheat the process water by sterile water flowing in countercurrent and to provide preheated process water to a heating circuit, and wherein the recuperator is to cool down the sterile water by the process water flowing in countercurrent; and the heating circuit located downstream of the recuperator comprising a pump, downstream of the pump a heater to heat the preheated process water and to provide heated process water to a heat retention section, and downstream of the heater the heat retention section to keep the heated process water hot at a predetermined temperature for a predetermined period of time, so as to produce sterile water, wherein the heating circuit comprises: a temperature sensor located downstream of the heat retention section, wherein the temperature sensor is to measure a current temperature of the sterile water leaving the heat retention section; a flow control valve located downstream of the temperature sensor; and a bypass provided between the flow control valve and the heater, wherein the bypass is a conduit; and wherein the flow control valve is configured to keep a volume flow in the heating circuit constant, wherein the recuperator is configured to cool down the sterile water of a first partial volume flow when the first partial volume flow of sterile water is taken from the heating circuit, and wherein the bypass is configured to return into the heating circuit a second partial volume flow of sterile water, wherein the second partial volume flow corresponds to a difference between the volume flow and the first partial volume flow. 2. The apparatus of claim 1 , further comprising a cooler located downstream of the recuperator, wherein the cooler is to further cool down the sterile water. 3. The apparatus of claim 1 , further comprising one or a plurality of consumers for consuming cooled down sterile water. 4. The apparatus of claim 3 , further comprising a line located downstream of the one or the plurality of consumers, wherein the line is openable for line sanitization by passing the cooled down sterile water through the opened line. 5. The apparatus of claim 4 , wherein the line comprises a terminal vapor barrier. 6. The apparatus of claim 1 , wherein an overflow valve is located downstream of the pump and upstream of the heater. 7. The apparatus of claim 1 , wherein a pressure holding valve is provided within the bypass. 8. The apparatus of claim 1 , wherein the heating circuit further comprises a degassing and expansion vessel. 9. A method of operating an apparatus for producing and providing sterile water, comprising: feeding process water to the apparatus through an inlet of the apparatus; preheating the process water in a recuperator of the apparatus by sterile water flowing in countercurrent; heating the preheated process water in a heater of the apparatus; maintaining the heated process water in a heat retention section of the apparatus at a predetermined temperature for a predetermined period of time; controlling a constant volume flow in a heating circuit of the apparatus by a flow control valve of the apparatus to maintain a constant heat holding time in the heating circuit; cooling down a first partial volume flow of sterile water, which is taken from the heating circuit in the recuperator; and returning a second partial volume flow of sterile water into the heating circuit via a bypass of the apparatus, wherein the second partial volume flow of sterile water corresponds to a difference between the volume flow and the first partial volume flow. 10. The method of claim 9 , further comprising cooling down the sterile water in a cooler of the apparatus. 11. The method of claim 9 , further comprising conducting the cooled down sterile water to one or a plurality of consumers. 12. The method of claim 9 , wherein a pressure difference of 0.5 bar is provided across a pressure holding valve. 13. The method of claim 9 , wherein downstream of the flow control valve, providing one of: responsive to determining that sterile water is drawn off, a pressure of 3.5 bar; or responsive to determining that sterile water is not drawn off, a pressure of 4.0 bar. 14. The method of claim 9 , further comprising measuring a current temperature of the sterile water leaving the heat retention section.
by distillation or evaporation · CPC title
by heating (methods of steam generation F22B; preheating boiler feed-water or accumulating preheated boiler feed-water F22D) · CPC title
Disinfection · CPC title
Energy recuperation; Heat pumps · CPC title
Time · CPC title
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