Method for recovering germanium
US-2024342650-A1 · Oct 17, 2024 · US
US11370690B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11370690-B2 |
| Application number | US-201716763768-A |
| Country | US |
| Kind code | B2 |
| Filing date | Nov 17, 2017 |
| Priority date | Nov 17, 2017 |
| Publication date | Jun 28, 2022 |
| Grant date | Jun 28, 2022 |
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Official abstract text for this publication.
An apparatus for manufacturing glass preforms for optical fibers includes a reaction chamber surrounding a deposition region, a holding device for holding a target rod within said deposition region, one or a plurality of deposition burners positioned below said deposition region and configured to direct a high temperature flow of forming glass particles toward said target rod, a hood positioned opposite to the deposition burners with respect to said holding device and configured for discharging soot of un-deposited glass particles, said hood including at least one exhaust port provided at a first end portion thereof and side panels extending from a second end portion thereof toward said first end portion. At least a portion of the side panels of the hood is gas permeable.
Opening claim text (preview).
The invention claimed is: 1. An apparatus for manufacturing glass preforms for optical fibers comprising: a reaction chamber surrounding a deposition region; a holding device for holding a target rod within said deposition region; one or a plurality of deposition burners positioned below said deposition region and configured to direct a high temperature flow of forming glass particles toward said target rod; a hood positioned opposite to the deposition burners with respect to said deposition region and configured for discharging soot of un-deposited glass particles, said hood comprising at least one exhaust port provided at a first end portion thereof and side panels extending from a second end portion thereof toward said first end portion; wherein at least a portion of the side panels of the hood is gas permeable and wherein the apparatus comprises a control device for adjusting the degree of permeability of the gas permeable portion. 2. The apparatus according to claim 1 , wherein said gas permeable portion of the side panels is positioned between said second end portion and said first end portion and extends for an area of at least 50% of the overall area of the side panels. 3. The apparatus according to claim 1 , wherein said gas permeable portion comprises a first plurality of perforations on said side panels fluidly connecting an internal environment of the reaction chamber with an external environment of said reaction chamber. 4. The apparatus according to claim 3 , wherein said gas permeable portion has a perforation density, calculated as a ratio between perforated areas and a not perforated areas, comprised between 0.2% and 15%. 5. The apparatus according to claim 3 , wherein an area of each perforation of said first plurality of perforation is between 0.7 mm{circumflex over ( )}2 and 15 mm{circumflex over ( )}2. 6. The apparatus according to claim 1 , wherein said control device acts on said first plurality of perforations for partially closing the latter. 7. The apparatus according to claim 1 , wherein said control device comprises at least one plate having a second plurality of perforations and configured to move with continuity between a minimum permeability condition, wherein said second plurality of perforations are partially superposed to said first plurality of perforations to partially close the latter, and a maximum permeability condition, wherein said second plurality of perforations are fully superposed and centered to said first plurality of perforations to leave the latter fully opened. 8. The apparatus according to claim 7 , wherein the perforations of said second plurality of perforations present identical spacing, identical shape and identical area of the perforations of said first plurality of perforations. 9. The apparatus according to claim 1 , wherein said hood has a tapered shape. 10. The apparatus according to claim 1 , further comprising an exhaust fan positioned or acting on said exhaust port. 11. The apparatus according to claim 1 , wherein said gas permeable portion is realized by one or more air filters. 12. A method for manufacturing glass preforms for optical fibers comprising: providing a reaction chamber surrounding a deposition region; holding a target rod within said deposition region; directing a high temperature flow of forming glass particles toward said target rod; providing a hood comprising side panels and an exhaust port for discharging to outside said reaction chamber glass particles not adhered to said target rod; providing said side panels with gas permeable portions extending for an area of at least 50% of the overall area of said side panels; maintaining the pressure inside the reaction chamber lower than the pressure outside the reaction chamber; adjusting a degree of permeability of said gas permeable portions of the side panels. 13. The method according to claim 12 , comprising maintaining the pressure inside the reaction chamber at values comprised between 20 Pa and 200 Pa lower than the pressure outside the deposition chamber. 14. The method according to claim 12 , further comprising setting a flow rate (B) passing through the gas permeable portions of said side panels comprised between 5% and 20% of the overall flow rate (A) passing through the exhaust port. 15. The method according to claim 14 , wherein setting a flow rate (B) passing through the gas permeable portions of said side panels is performed by adjusting a degree of permeability of said gas permeable portions of the side panels. 16. The method according to claim 12 , wherein adjusting a degree of permeability comprises providing said gas permeable portions of the side panels with a first plurality of perforations and partially closing said first plurality of perforations. 17. The method according to claim 16 , wherein partially closing said first plurality of perforations comprises providing at least one plate having a second plurality of perforations and moving with continuity said at least one plate with respect to said side panels between a minimum permeability condition, wherein said second plurality of perforations are partially superposed and aligned to said first plurality of perforations, and a maximum permeability condition, wherein said second plurality of perforations are centered and aligned to said first plurality of perforations. 18. The method according to claim 16 , wherein providing a first plurality of perforations comprises providing said gas permeable portions with a perforation density, calculated as a ratio between perforated areas and not perforated areas, comprised between 0.2% and 15%. 19. A method for manufacturing glass preforms for optical fibers comprising: providing the apparatus of claim 1 wherein the reaction chamber of the apparatus surrounds a deposition region; holding a target rod within said deposition region; directing a high temperature flow of forming glass particles toward said target rod; providing the hood comprising side panels and an exhaust port for discharging to outside said reaction chamber glass particles not adhered to said target rod; providing said side panels with gas permeable portions extending for an area of at least 50% of the overall area of said side panels; maintaining the pressure inside the reaction chamber lower than the pressure outside the reaction chamber; adjusting a degree of permeability of said gas permeable portions of the side panels.
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