Processes for making a super-insulating core material for a vacuum insulated structure

Patent metadata

Field	Value
Publication number	US-11365843-B2
Application number	US-201716305254-A
Country	US
Kind code	B2
Filing date	Mar 7, 2017
Priority date	Mar 7, 2017
Publication date	Jun 21, 2022
Grant date	Jun 21, 2022

Abstract

A method for forming a super-insulating material for a vacuum insulated structure includes disposing glass spheres within a rotating drum. A plurality of interstitial spaces are defined between the glass spheres. A binder material is disposed within the rotating drum. The glass spheres and the at least one binder material are rotated within the rotating drum, wherein the binder material is mixed during a first mixing stage with the glass spheres. A first insulating material is disposed within the rotating drum. The binder material, the first insulating material and the glass spheres are mixed to define an insulating base. A second insulating material is disposed within the rotating drum. The secondary insulating material is mixed with the insulating base to define a homogenous form of the super-insulating material, wherein the first and second insulating materials occupy substantially all of the interstitial spaces.

First claim

What is claimed is:

1. A method for forming a super-insulating material for a vacuum insulated structure for an appliance, the method comprising steps of:
disposing glass spheres within a rotating drum, wherein a plurality of interstitial spaces are defined between the glass spheres;
disposing a resin-based binding material within the rotating drum;
mixing the glass spheres and the resin-based binding material during a first mixing stage to define an adhering base material, wherein the plurality of interstitial spaces between the glass spheres are partially occupied by the resin-based binding material;
disposing a first insulating material within the rotating drum;
mixing the adhering base material with the first insulating material to define an aggregate material;
crushing the aggregate material during a crushing stage to define an insulating base;
disposing a second insulating material within the rotating drum; and
mixing the second insulating material with the insulating base to define a homogenous form of the super-insulating material, wherein the first and second insulating materials substantially occupy substantially all of an interstitial volume defined by the plurality of interstitial spaces.

2. The method of claim 1 , wherein the resin-based binding material includes a resin-based material and a hardening agent.

3. The method of claim 1 , wherein the first insulating material is carbon black that adheres to the resin-based binding material.

4. The method of claim 1 , wherein the second insulating material is a silica-based material.

5. The method of claim 4 , wherein the silica-based material is at least one of precipitated silica and fumed silica.

6. The method of claim 1 , wherein the glass spheres are micro spheres.

7. The method of claim 1 , wherein the glass spheres are hollow glass spheres.

8. The method of claim 1 , wherein the step of mixing the adhering base material and the first insulating material includes second and third mixing stages.

9. The method of claim 8 , wherein the second mixing stage is a short-term mixing stage and the third mixing stage is a long-term mixing stage.

10. The method of claim 1 , further comprising:
mixing the aggregate material during an inspection mixing stage, wherein the inspection mixing stage exposes substantially each surface of the aggregate material to air within the rotating drum.

11. The method of claim 1 , wherein the homogenous form of the super-insulating material is defined by coated glass spheres that are each below a predetermined insulating particle size.

12. The method of claim 11 , wherein the super-insulating material is a pourable free flowing insulating material.

13. The method of claim 1 , further comprising the steps of:
disposing the super-insulating material into an insulating cavity of an insulating structure;
expressing gas from the insulating cavity to define an at least partial vacuum within the insulating cavity; and
sealing the insulating cavity to define the vacuum insulated structure.

14. The method of claim 13 , wherein the insulating structure is an insulating panel and wherein the vacuum insulated structure is a vacuum insulated panel.

15. The method of claim 13 , wherein the insulating structure is an appliance cabinet having an outer wrapper and an inner liner that are attached to define the insulating cavity therein, and wherein the vacuum insulated structure is a vacuum insulated cabinet.

16. A method for forming a super-insulating material for a vacuum insulated structure for an appliance, the method comprising steps of:
disposing glass spheres within a rotating drum, wherein a plurality of interstitial spaces are defined between the glass spheres;
disposing a resin-based binding material within the rotating drum;
mixing the glass spheres and the resin-based binding material during a first mixing stage to define an adhering base material, wherein the plurality of interstitial spaces of the glass spheres are partially occupied by the resin-based binding material;
disposing a first insulating material within the rotating drum;
mixing the adhering base material with the first insulating material to define an aggregate material;
mixing the aggregate material to define an inspection mixing stage that exposes substantially each surface of the aggregate material to air within the rotating drum; and
crushing the aggregate material during a crushing stage to define an insulating base.

17. The method of claim 16 , further comprising:
disposing a second insulating material within the rotating drum to be combined with the insulating base; and
mixing the second insulating material with the insulating base to define a homogenous form of the super-insulating material, wherein the first and second insulating materials substantially occupy substantially all of an interstitial volume defined by the plurality of interstitial spaces.

18. The method of claim 17 , wherein the resin-based binding material includes a resin-based material and a hardening agent, and wherein the first insulating material includes carbon black that adheres to the resin-based binding material, and wherein the second insulating material includes at least one of precipitated silica and fumed silica.

19. A method for forming a super-insulating material for a vacuum insulated structure for an appliance, the method comprising steps of:
disposing glass spheres and a resin-based binding material within a rotating drum, wherein a plurality of interstitial spaces are defined between the glass spheres;
mixing the glass spheres and the resin-based binding material during a first mixing stage to define an adhering base material, wherein interstitial spaces defined between the glass spheres are partially occupied by the resin-based binding material;
mixing the adhering base material with a first insulating material to define an aggregate material;
mixing the aggregate material to define an inspection mixing stage that exposes substantially each surface of the aggregate material to air within the rotating drum;
crushing the aggregate material during a crushing stage to define an insulating base; and
mixing a second insulating material with the insulating base to define a homogenous form of the super-insulating material.

20. The method of claim 19 , wherein the step of mixing the adhering base material and the first insulating material includes second and third mixing stages, and wherein the second mixing stage is a short-term mixing stage and the third mixing stage is a long-term mixing stage.

Assignees

• Whirlpool Co

Inventors

• Deka Lakshya J
• Ernat Nicole M

Classifications

• Y02B80/10

  Insulation, e.g. vacuum or aerogel insulation · CPC title

• Y02A30/242

  Slab shaped vacuum insulation · CPC title

• C04B2235/528

  Spheres · CPC title

• C04B24/34

  Natural resins, e.g. rosin {(C04B24/243 takes precedence)} · CPC title

• C04B14/062

  Microsilica, e.g. colloïdal silica (preparing microsilica slurries or suspensions C04B18/148) · CPC title