Extraction device and method for same

Patent metadata

Field	Value
Publication number	US-11364452-B2
Application number	US-201816754153-A
Country	US
Kind code	B2
Filing date	Oct 11, 2018
Priority date	Nov 13, 2017
Publication date	Jun 21, 2022
Grant date	Jun 21, 2022

Abstract

Provided is an extraction method for extracting an extract from a mixture using liquefied gas that can dissolve the extract, the method facilitating extraction operations and enabling low cost operation. An extraction device that extracts a component dissolved in liquefied gas from material to be treated using continuous phase changes in the liquefied gas is characterized by being provided with: a compressor that feeds gas under pressure; a heat exchanger for generating liquefied gas by the gas flowing in a high temperature side flow path; a treatment tank into which the material to be treated is loaded and the liquefied gas flows; and a retention tank provided in series or in parallel to the flow path downstream of the high temperature side flow path in the heat exchanger.

First claim

The invention claimed is:

1. An extraction device for extracting a component contained in an object to be treated, comprising:
a first compressor;
a first heat exchanger that changes a phase of the extractant from gas to liquid;
a second heat exchanger that changes the phase of the extractant from liquid to gas;
a closing valve disposed between the second heat exchanger and the first heat exchanger along a flow path;
a second compressor disposed between the closing valve and the first heat exchanger along the flow path that pumps an extractant;
a treatment tank in which the object to be treated is stored, and into which the extractant liquefied in the first heat exchanger flows;
a valve that is provided between the second heat exchanger and the treatment tank; and
a retention tank that is provided between the first heat exchanger and the treatment tank,
wherein the gas from the second heat exchanger passes via the flow path to the first heat exchanger by the second compressor via the closing valve.

2. The extraction device according to claim 1 , wherein the valve is closed to drive the first compressor before opening a collection valve for collecting an extract stored in the second heat exchanger.

3. The extraction device according to claim 1 ,
wherein the valve is closed to drive the second compressor before opening a collection valve for collecting an extract stored in the second heat exchanger.

4. The extraction device according to claim 1 , wherein the treatment tank is disposed in a vertical direction.

5. The extraction device according to claim 4 , further comprising:
a filter disposed in an upper portion in the treatment tank,
wherein a flow in the treatment tank is an upward flow during a steady operation of an extraction process.

6. The extraction device according to claim 5 , wherein the retention tank is installed below the first heat exchanger in the vertical direction.

7. The extraction device according to claim 6 , further comprising:
a pump which is downstream of the retention tank and upstream of the treatment tank.

8. The extraction device according to claim 7 , wherein the pump is installed below the first heat exchanger in the vertical direction.

9. The extraction device according to claim 8 , wherein the pump is installed below the retention tank in the vertical direction.

10. The extraction device according to claim 1 , wherein as the first compressor, a compressor that uses edible oil or silicone oil as a lubricant, or an oil-free compressor is used.

11. The extraction device according to claim 1 , wherein the extractant is any one of propane, normal butane, isobutane, neopentane, isopentane, dimethyl ether, and ethyl methyl ether, or a mixture of two or more thereof.

Assignees

• Hitachi Ltd

Inventors

• Sano Tadashi
• Miyasaka Toom
• Sekiya Sachio

Classifications

• B01D11/0219

  Fixed bed of solid material · CPC title

• B01D11/028

  Flow sheets · CPC title

• B01D11/02

  of solids · CPC title

• B01D11/0288

  Applications, solvents · CPC title

• B01D11/0296

  Condensation of solvent vapours (condensation in general B01D5/00) · CPC title