Aerogel structure body and method of manufacturing the same

Patent metadata

Field	Value
Publication number	US-11358366-B2
Application number	US-202117241828-A
Country	US
Kind code	B2
Filing date	Apr 27, 2021
Priority date	May 27, 2020
Publication date	Jun 14, 2022
Grant date	Jun 14, 2022

Abstract

An aerogel structure body includes a composite layer containing fibrous materials and aerogel, the aerogel being held between the fibrous materials, and an aerogel layer having a first surface on at least one surface of the composite layer and formed of the aerogel, in which the aerogel layer having a second surface opposite to the first surface, the second surface including a projection portion projecting from the second surface, and a density of the aerogel in the projection portion is 0.1% to 3.0% higher than a density of the aerogel in the aerogel layer (flat portion) other than the projection portion. Therefore, the aerogel structure body that is excellent in dimensional stability and heat insulating properties and that can be manufactured with high productivity and a method of manufacturing the same are provided.

First claim

What is claimed is:

1. An aerogel structure body comprising:
a composite layer containing fibrous materials and aerogel, wherein the aerogel is held between the fibrous materials and wherein the aerogel has a porous structure including particles of silica aerogel connected to each other; and
an aerogel layer having a first surface on at least one surface of the composite layer and formed of the aerogel,
wherein the aerogel layer has a second surface opposite to the first surface, and the second surface includes a projection portion projecting from the second surface,
a density of the aerogel in the projection portion is 0.1% to 3.0% higher than a density of the aerogel in the aerogel layer other than the projection portion,
a concentration of the aerogel in the projection portion is higher than a concentration of the aerogel in the aerogel layer other than the projection portion, and
a compression rate of the projection portion with respect to a pressure of 1.0 MPa or greater and 5.0 MPa or smaller applied to the projection portion is 0.1% to 20% lower than a compression rate of the aerogel layer other than the projection portion with respect to a pressure of 1.0 MPa or greater and 5.0 MPa or smaller applied to the aerogel layer other than the projection portion.

2. The aerogel structure body of claim 1 , wherein the projection portion has an elliptical shape in a plan view shape.

3. The aerogel structure body of claim 1 , wherein an average diameter of the fibrous materials is 0.1 μm or greater and 10 μm or smaller, and a porosity of the composite layer is 90% or greater.

4. The aerogel structure body of claim 1 , wherein the projection portion has a higher color tone than a portion other than the projection portion in the aerogel structure body.

5. The aerogel structure body of claim 1 ,
wherein the aerogel has a network structure in which the particles of silica aerogel are connected to each other by point contact.

6. The aerogel structure body of claim 1 , wherein the projection portion is visually perceived in a case where the aerogel structure body is exposed to light.

7. The aerogel structure body of claim 1 , wherein a thermal conductivity of the aerogel structure body is 0.02 W/(m·K) or greater and 0.06 W/(m·K) or smaller.

8. The aerogel structure body of claim 1 , wherein a compression rate of the aerogel structure body in a case of being pressurized at 5 MPa is 40% or less.

9. An aerogel structure body comprising:
a composite layer containing fibrous materials and aerogel, wherein the aerogel is held between the fibrous materials and wherein the aerogel has a porous structure including particles of silica aerogel connected to each other; and
an aerogel layer having a first surface on at least one surface of the composite layer and formed of the aerogel,
wherein the aerogel layer has a second surface opposite to the first surface, and the second surface includes a projection portion projecting from the second surface,
a concentration of the aerogel in the projection portion is higher than a concentration of the aerogel in the aerogel layer other than the projection portion, and
a compression rate of the projection portion with respect to a pressure of 1.0 MPa or greater and 5.0 MPa or smaller applied to the projection portion is 0.1% to 20% lower than a compression rate of the aerogel layer other than the projection portion with respect to a pressure of 1.0 MPa or greater and 5.0 MPa or smaller applied to the aerogel layer other than the projection portion.

10. The aerogel structure body of claim 9 , wherein the projection portion has an elliptical shape in a plan view shape.

11. The aerogel structure body of claim 9 , wherein the projection portion has a higher color tone than a portion other than the projection portion in the aerogel structure body.

12. The aerogel structure body of claim 9 , wherein the aerogel has a network structure in which the particles of silica aerogel are connected to each other by point contact.

13. The aerogel structure body of claim 9 , wherein the projection portion is visually perceived in a case where the aerogel structure body is exposed to light.

Assignees

• Panasonic Ip Man Co Ltd

Inventors

• Tsuruta Takashi
• IWASAKI Rikako

Classifications

• C01B33/1585 Primary

  Dehydration into aerogels · CPC title

• B32B2262/101

  Glass fibres · CPC title

• B32B2307/304

  Insulating · CPC title

• B32B5/18 Primary

  characterised by features of a layer {of} foamed material · CPC title

• B32B2266/057

  Silicon-containing material, e.g. glass · CPC title