Additive layer method for application of slurry-based features

Patent metadata

Field	Value
Publication number	US-11351696-B2
Application number	US-201916278265-A
Country	US
Kind code	B2
Filing date	Feb 18, 2019
Priority date	Feb 19, 2018
Publication date	Jun 7, 2022
Grant date	Jun 7, 2022

Abstract

A system and method for forming a porous ceramic preform is provided. The method may include forming a stacked powder structure including a binder layer and a powder layer on the binder layer. The binder layer may be formed by depositing a binder with a spray nozzle on a substrate. The powder layer may be formed by depositing a powder on the binder layer. The porous ceramic preform may be formed by heating the stacked powder structure to pyrolyze the binder. The porous ceramic preform is configured to be infiltrated by a molten material. The substrate may comprise a ceramic fiber preform. After melt infiltration of the porous ceramic preform and the ceramic fiber preform, a densified ceramic feature having a predetermined geometry may be formed on a ceramic matrix composite (CMC) component.

First claim

What is claimed is:

1. A method comprising:
forming a stacked powder structure on a substrate comprising a previously formed ceramic fiber preform, the stacked powder structure comprising a binder layer and a powder layer on the binder layer, wherein forming the stacked powder structure comprises forming the binder layer by depositing a binder with a spray nozzle on the substrate and forming the powder layer on the binder layer by depositing a powder on the binder layer, the binder comprising at least one of phenolic resin, poly(furfuryl alcohol), and polycarbosilane, and the powder comprising silicon carbide; and
heating the stacked powder structure to pyrolyze the binder, and infiltrating the stacked powder structure and the previously formed ceramic fiber preform with molten silicon metal or silicon alloy, thereby forming a CMC component including a densified composite feature on the CMC component.

2. The method of claim 1 , further comprising:
removing an amount of the powder from the stacked powder structure prior to the heating.

3. The method of claim 1 , wherein the powder comprises fibers, and the method further comprises:
wherein the densified composite feature has a fiber-to-ceramic matrix material ratio of between 20% and 45%.

4. The method of claim 1 , wherein the spray nozzle comprises an array of nozzles for supplying the binder to selected regions of the substrate.

5. The method of claim 1 , further comprising controlling the spray nozzle to supply the binder to predetermined portions of the substrate.

6. The method of claim 1 , wherein the powder comprises a plurality of chopped fibers, each having a diameter in a range of between 5 microns and 10 microns, inclusively, and the chopped fibers have an aspect ratio between 4 and 20, inclusively.

7. The method of claim 1 , wherein the binder layer is a first binder layer and the powder layer is a first powder layer, and forming the stacked powder structure further comprises forming a second binder layer by depositing the binder on the first powder layer and forming a second powder layer by depositing the powder on the second binder layer.

8. The method of claim 1 , further comprising:
placing the substrate on a stage; and
lowering the stage before depositing the powder on the binder.

9. The method of claim 1 , wherein the powder further comprises a reactive additive.

10. The method of claim 9 , wherein the reactive additive comprises at least one of graphite, diamond, and carbon black.

11. The method of claim 9 , wherein the reactive additive comprises acicular particulate.

12. The method of claim 11 , wherein the acicular particulate comprises at least one of carbon fiber and graphene.

13. The method of claim 1 , wherein heating the stacked powder structure causes the binder to produce silicon carbide.

14. The method of claim 1 , wherein the powder comprises a unimodal particle size distribution.

15. The method of claim 1 , wherein the powder comprises a bimodal particle size distribution.

16. The method of claim 1 , wherein the previously formed ceramic fiber preform has been infiltrated by a slurry, the slurry comprising silicon carbide.

17. A method comprising:
forming a stacked powder structure on a substrate comprising a previously formed ceramic fiber preform, the stacked powder structure comprising a first binder layer, a first powder layer on the first binder layer, a second binder layer on the first powder layer, and a second powder layer on the second binder layer, wherein forming the stacked powder structure comprises forming the first binder layer by depositing a binder with a spray nozzle on the substrate, the binder comprising at least one of phenolic resin, poly(furfuryl alcohol), and polycarbosilane, forming the first powder layer on the first binder layer by depositing a powder on the first binder layer, forming the second binder layer on the first powder layer by depositing the binder with the spray nozzle on the first powder layer, and forming the second powder layer by depositing the powder on the second binder layer, the powder comprising fibers, including silicon carbide fibers wherein the fibers comprise chopped fibers having a diameter in a range of between 5 microns and 10 microns, inclusively, and the chopped fibers have an aspect ratio between 4 and 20, inclusively;
heating the stacked powder structure to pyrolyze the binder, and infiltrating the stacked powder structure and the previously formed ceramic fiber preform with molten silicon metal or silicon alloy, thereby forming a CMC component including a densified composite feature on the CMC component; and
wherein the densified composite feature has a fiber-to-matrix material ratio of between 20% and 45%.

18. The method of claim 17 , wherein the densified composite feature includes a seal land, labyrinth seal, strip seal, load pad, locating pad, and/or clocking feature.

Assignees

• Rolls Royce Corp
• Rolls Royce High Temperature Composites Inc

Inventors

• Nelson Scott
• Shuck Quinlan
• Landwehr Sean
• Shim Sungbo

Classifications

• B33Y40/20

  Post-treatment, e.g. curing, coating or polishing · CPC title

• B28B1/001 Primary

  Rapid manufacturing of 3D objects by additive depositing, agglomerating or laminating of material (selective deposition modelling of metallic powder B22F10/00; rapid manufacturing of 3D objects in general and in particular of plastics B29C64/00) · CPC title

• C04B2235/5248

  Carbon, e.g. graphite · CPC title

• C04B35/62281

  based on silicon carbide (C04B35/571 takes precedence) · CPC title

• B33Y10/00 Primary

  Processes of additive manufacturing · CPC title