Methods for removing hemicellulose
US-8986501-B2 · Mar 24, 2015 · US
US11337436B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11337436-B2 |
| Application number | US-201716470984-A |
| Country | US |
| Kind code | B2 |
| Filing date | Dec 12, 2017 |
| Priority date | Dec 23, 2016 |
| Publication date | May 24, 2022 |
| Grant date | May 24, 2022 |
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The present invention relates to a water-in-oil emulsion comprising 30-90 wt. % of a structured continuous fat phase and 10-70 wt. % of a dispersed aqueous phase, said structured continuous fat phase comprising:95-99.9 wt. % fat, said fat having a solid fat content at 20° C. (N20) of 5-50% and a liquid oil content at 20° C. that equals 100%-N20;particulate anhydrous non-defibrillated cell wall material from plant parenchymal tissue, said particulate anhydrous non-defibrillated cell wall material having a particle size of between 25 μm and 500 μm;wherein the particulate anhydrous non-defibrillated cell wall material is present in the structured continuous fat phase in a concentration of 0.2-10% by weight of the liquid oil.Incorporation of the aforementioned particulate cell wall material in the fat phase of the water-in-oil emulsion makes it possible to reduce the amount of high melting (hard stock) fat that is required in the production of the emulsion.
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The invention claimed is: 1. A water-in-oil emulsion comprising 30-90 wt. % of a structured continuous fat phase and 10-70 wt. % of a dispersed aqueous phase, said structured continuous fat phase comprising: 95-99.9 wt. % fat, said fat having a solid fat content at 20° C. (N 20 ) of 5-50% and a liquid oil content at 20° C. that equals 100%-N 20 ; particulate anhydrous non-defibrillated cell wall material from plant parenchymal tissue, said particulate anhydrous non-defibrillated cell wall material having a particle size of between 25 μm and 500 μm; wherein the particulate anhydrous non-defibrillated cell wall material is present in the structured continuous fat phase in a concentration of 0.2-10% by weight of the liquid oil, and wherein the dispersed aqueous phase contains at least 80 wt % water. 2. The emulsion according to claim 1 , wherein the particulate anhydrous non-defibrillated cell wall material is present in the structured continuous fat phase in a concentration of 0.1-5% by weight of the structured continuous fat phase. 3. The emulsion according to claim 1 , wherein the fat has a solid fat content at 35° C. (N 35 ) of 0-20%. 4. The emulsion according claim 1 , wherein the combination of the structured continuous fat phase and the dispersed aqueous phase constitutes at least 80 wt. % of the water-in-oil emulsion. 5. The emulsion according to claim 1 , wherein the emulsion has a Stevens hardness at 5° C. of at least 30 g. 6. The emulsion according to claim 1 , wherein the anhydrous non-defibrillated cell wall material contains galacturonic acid and glucose in a molar ratio of less than 0.60. 7. The emulsion according to claim 1 , wherein the particulate anhydrous non-defibrillated cell wall material originates from fruit, bulb, root, tuber, leave, and/or stem tissue. 8. The emulsion according to claim 1 , wherein the particulate anhydrous non-defibrillated cell wall material originates from one or more plant sources selected from carrot, aubergine, cucumber, sugar beet, apple, pear, leek, pumpkin, kiwi, strawberry, papaya, pine apple, prune, melon, apricot, grapes onion, tomato, potato, coconut. 9. A process of preparing a water-in-oil emulsion, said process comprising: preparing a pre-emulsion by mixing molten fat and aqueous liquid, said fat having a solid fat content at 20° C. (N 20 ) of 5-50% and a liquid oil content at 20° C. that equals 100%-N 20 ; cooling the pre-emulsion to a temperature that is at least 5° C. below the slip melting point of the fat; mixing the cooled pre-emulsion with particulate anhydrous non-defibrillated cell wall material from plant parenchymal tissue; wherein the particulate cell wall material has a bulk density of less than 50 g/l and 20 at least 90 wt. % of said particulate cell wall material has a particle size between 25 μm and 500 μm; and wherein the particulate cell wall material is mixed with the pre-emulsion in an amount of 0.1 to 10 parts by weight per 100 parts by weight of liquid oil, wherein the process yields a water-in-oil emulsion comprising: 30-90 wt. % of a structured continuous fat phase and 10-70 wt. % of a dispersed aqueous phase, said structured continuous fat phase comprising: 95-99.9 wt. % fat, said fat having a solid fat content at 20° C. (N 20 ) of 5-50% and a liquid oil content at 20° C. that equals 100%-N 20 ; particulate anhydrous non-defibrillated cell wall material from plant parenchymal tissue, said particulate anhydrous non-defibrillated cell wall material having a particle size of between 25 μm and 500 μm; wherein the particulate anhydrous non-defibrillated cell wall material is present in the structured continuous fat phase in a concentration of 0.2-10% by weight of the liquid oil, and wherein the dispersed aqueous phase contains at least 80 wt % water. 10. The process according to claim 9 , wherein the particulate cell wall material has a bulk density of less than 20 g/l. 11. The process according to claim 9 , wherein the particulate anhydrous non-defibrillated cell wall material when dispersed in demineralised water in a concentration of 3 wt. % produces a suspension having a conductivity of less than 200 μS/cm. 12. The process according to claim 9 , wherein the process comprises mixing 100 parts by weight of fat with 0.3-4 parts by weight of the particulate anhydrous non-defibrillated cell wall material.
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