Cleaning and dewatering fine coal

Patent metadata

Field	Value
Publication number	US-11331676-B2
Application number	US-202016788617-A
Country	US
Kind code	B2
Filing date	Feb 12, 2020
Priority date	Feb 1, 2010
Publication date	May 17, 2022
Grant date	May 17, 2022

Abstract

Fine coal is cleaned of its mineral matter impurities and dewatered by mixing the aqueous slurry containing both with a hydrophobic liquid, subjecting the mixture to a phase separation. The resulting hydrophobic liquid phase contains coal particles free of surface moisture and droplets of water stabilized by coal particles, while the aqueous phase contains the mineral matter. By separating the entrained water droplets from the coal particles mechanically, a clean coal product of substantially reduced mineral matter and moisture contents is obtained. The spent hydrophobic liquid is separated from the clean coal product and recycled. The process can also be used to separate one type of hydrophilic particles from another by selectively hydrophobizing one.

First claim

What is claimed is:

1. A system for removing mineral matter from and dewatering fine coal comprised of particles of 1.0 mm in diameter and smaller wherein said fine coal includes mineral impurities, comprising:
a mixer for mixing a hydrophobic liquid with fine coal in an aqueous media, said mixer being configured to permit said mineral impurities to separate from said fine coal into said aqueous media, permitting said hydrophobic liquid to displace water from surfaces of said fine coal, and producing a mixture;
a phase separator for phase separating said mixture produced in said mixing step in which said hydrophobic liquid is atop said aqueous media, said phase separating step producing a first phase containing said hydrophobic liquid, fine coal, and entrained water, and a second phase containing said aqueous media and mineral impurities:
a mechanical separator for separating said entrained water from said fine coal and said hydrophobic liquid from said first phase by a mechanical process, wherein residual mineral impurities are dispersed in the entrained water droplets; and
a hydrophobic liquid recovery system for separating hydrophobic liquid from said fine coal to produce a fine coal product with reduced mineral impurities and moisture content.

2. The system of claim 1 wherein said phase separator is a settler.

3. The system of claim 1 wherein said mechanical separator is a size-size separator.

4. The system of claim 3 wherein said size-size separator includes a screen.

5. The system of claim 3 wherein said mechanical separator is a solid-liquid separator.

6. The system of claim 5 wherein said solid-liquid separator includes a filter.

7. The system of claim 5 wherein said solid-liquid separator includes a centrifuge.

8. The system of claim 1 wherein said hydrophobic liquid recovery system includes components configured to recover residual hydrophobic liquid adhering to the surface of said fine coal product.

9. The system of claim 1 further comprising a high shear dewatering apparatus.

10. The system of claim 9 wherein said high shear dewatering apparatus is selected from the group consisting of dynamic mixer, static mixer, rotating fan, fluidized bed, vibrating screen, and air jet.

11. The system of claim 1 further comprising a dry particle collector.

Assignees

• Virginia Tech Intellectual Properties Inc

Inventors

• Yoon Roe-Hoan
• Eraydin Mert Kerem

Classifications

• C10L5/366

  Powders · CPC title

• C10L9/10

  by using additives · CPC title

• B03B9/005 Primary

  specially adapted for coal · CPC title

• B03B1/04

  by additives · CPC title