Lyocell material for cigarette filter, and preparation method therefor
US-2018007952-A1 · Jan 11, 2018 · US
US11330836B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11330836-B2 |
| Application number | US-201916688838-A |
| Country | US |
| Kind code | B2 |
| Filing date | Nov 19, 2019 |
| Priority date | Jun 28, 2013 |
| Publication date | May 17, 2022 |
| Grant date | May 17, 2022 |
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A lyocell material for a cigarette filter and a method of manufacturing the same are disclose. The lyocell material which is biodegradable and eco-friendly can be manufactured by crimping lyocell multifilaments to obtain a crimped tow.
Opening claim text (preview).
The invention claimed is: 1. A lyocell material for a cigarette filter, manufactured by spinning a lyocell spinning dope comprising a cellulose pulp and an N-methylmorpholine-N-oxide (NMMO) aqueous solution to produce lyocell multifilaments which are then crimped, and the lyocell multifilaments are having 25-30 crimps per inch. 2. The lyocell material of claim 1 , wherein the lyocell spinning dope comprises 6˜16 wt % of the cellulose pulp and 84-94 wt % of the NMMO aqueous solution. 3. The lyocell material of claim 2 , wherein the cellulose pulp comprises 85-97 wt % of alpha-cellulose, and has a degree of polymerization (DPw) of 600-1700. 4. The lyocell material of claim 1 , manufactured by a method comprising the following steps: (S1) spinning a lyocell spinning dope comprising a cellulose pulp and an N-methylmorpholine-N-oxide (NMMO) aqueous solution; (S2) coagulating the lyocell spinning dope spun in the step (S1), thus obtaining lyocell multifilaments; (S3) water-washing the lyocell multifilaments obtained in the step (S2); (S4) oil-treating the lyocell multifilaments water-washed in the step (S3); and (S5) crimping the lyocell multifilaments oil-treated in the step (S4) using a stuffer box, thus obtaining a crimped tow having 25-30 crimps per inch, wherein coagulating in the step (S2) comprises a primary coagulation using air quenching (Q/A) including supplying cold air at a temperature of 4-15° C. and a wind velocity of 5-50 m/s to the spinning dope and a secondary coagulation including immersing the primarily coagulated spinning dope in a coagulation solution, wherein the cold air is supplied outwardly from an air cooling part positioned inside a donut-shaped spinneret, and wherein the step (S5) is performed by supplying steam having a pressure of 0.1-1.0 kgf/cm 2 to an interior of the stuffer box and pressing the lyocell multifilaments using a press roller at a pressure of 1.5-2.0 kgf/cm 2 to give the lyocell multifilaments having 25-30 crimps per inch. 5. The lyocell material of claim 4 , wherein the coagulation solution has a temperature of 30° C. or less.
Use of materials for tobacco smoke filters · CPC title
using stuffer boxes · CPC title
Producing crimped or curled fibres, filaments, yarns, or threads, giving them latent characteristics (yarns per se D02G3/00; during formation of artificial filaments, threads, or the like D01D5/22; general aspects of chemical treatment D06M) · CPC title
for cigars or cigarettes · CPC title
Biodegradable or disintegrable · CPC title
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